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    Process for producing aromatic sulfide polymers
    1.
    发明授权
    Process for producing aromatic sulfide polymers 失效
    生产芳香族硫化物聚合物的方法

    公开(公告)号：US4495332A

    公开(公告)日：1985-01-22

    申请号：US517837

    申请日：1983-07-27

    申请人： Zenya Shiiki ,  Yo Iizuka ,  Yukichika Kawakami

    发明人： Zenya Shiiki ,  Yo Iizuka ,  Yukichika Kawakami

    IPC分类号： C08F2/16 ,  C08G75/02

    CPC分类号： C08G75/0254

    摘要： A process for obtaining aromatic sulfide polymer which has a markedly high molecular weight and can be readily formed into films, fibers, and other structures. The process comprises heating, in an aprotic solvent to a temperature of 100.degree. to 250.degree. C., (i) a dihaloaromatic compound and (ii) substantially anhydrous fine powder of the sulfide of an alkali or alkaline earth metal in the presence of (iii) substantially anhydrous fine powder of the carbonate of an alkali or alkaline earth metal, or of a mixture thereof with a hygroscopic inorganic salt and (iv) a strictly controlled very small amount of water dissolved in or solvated with the solvent.

    摘要翻译： 一种获得具有显着高分子量并可容易地形成薄膜，纤维和其它结构的芳香族硫化物聚合物的方法。 该方法包括在非质子溶剂中加热至100-250℃的温度，（i）二卤代芳族化合物和（ii）碱金属或碱土金属的硫化物的基本上无水的细粉末，在（ iii）碱性或碱土金属碳酸盐或其吸湿性无机盐的混合物的基本上无水的细粉末和（iv）严格控制的非常少量的溶于溶剂或溶剂化的水。

    Polyarylene thioether composition for molding
    2.
    发明授权
    Polyarylene thioether composition for molding 失效
    聚亚芳基硫醚组合物用于成型

    公开(公告)号：US4956499A

    公开(公告)日：1990-09-11

    申请号：US175250

    申请日：1988-03-30

    申请人： Makoto Fukuda ,  Sirou Suzuki ,  Toshio Hosokawa ,  Yo Iizuka ,  Yukichika Kawakami ,  Zenya Shiiki

    发明人： Makoto Fukuda ,  Sirou Suzuki ,  Toshio Hosokawa ,  Yo Iizuka ,  Yukichika Kawakami ,  Zenya Shiiki

    IPC分类号： C08L81/02

    CPC分类号： C08L81/02

    摘要： Disclosed herein are (1) a composition which is prepared by combining 0.2 to 90 parts by weight of a cross-linked polyarylene thioether having a melt viscosity of 5.times.10.sup.5 to 1.times.10.sup.9 poise, which becomes gel under melting, with 100 parts by weight of a resin consisting of polyarylene thioether, which has a repeating unit of ##STR1## as the main constituent, having a melt viscosity of 10 to 5.times.10.sup.4 poise and (2) a composition of polyarylene thioether for molding, which is prepared by combining not more than 400 parts by weight of a fibrous filler and/or an inorganic filler with 100 parts by weight of the above-mentioned composition (1), is excellent in an antiflash property, is high in a mechanical strength and a thermal stability and is easily processed on melt molding and can easily recycle its molded scraps.

    Process for producing aromatic sulfide polymer with alkaline earth metal oxide dehydrating agent
    3.
    发明授权
    Process for producing aromatic sulfide polymer with alkaline earth metal oxide dehydrating agent 失效
    用碱土金属氧化物脱水剂生产芳香族硫化物聚合物的方法

    公开(公告)号：US4537953A

    公开(公告)日：1985-08-27

    申请号：US647733

    申请日：1984-09-06

    申请人： Yukichika Kawakami ,  Zenya Shiiki ,  Yo Iizuka

    发明人： Yukichika Kawakami ,  Zenya Shiiki ,  Yo Iizuka

    IPC分类号： C08G75/02 ,  C08G75/06 ,  C08G75/16

    CPC分类号： C08G75/0254

    摘要： The improvement in a process for producing an aromatic sulfide polymer from (A) hydrous sulfide of an alkali or alkaline earth metal and (B) a dihalo-aromatic compound is disclosed. The improvement is concerned with how the hydrous sulfide is dehydrated and comprises dehydrating the hydrous sulfide by the action thereon of (C) an alkaline earth metal oxide before substantial formation of the aromatic sulfide polymer.

    摘要翻译： 公开了一种由（A）碱金属或碱土金属的含水硫化物和（B）二卤代芳族化合物制备芳族硫醚聚合物的方法的改进。 改进之处在于硫化氢如何脱水，并且包括在大量形成芳族硫醚聚合物之前通过（C）碱土金属氧化物的作用使含水硫化氢脱水。

    Process for producing aromatic sulfide polymer with anhydrous amorphous vitreous complex dehalogenation agent
    4.
    发明授权
    Process for producing aromatic sulfide polymer with anhydrous amorphous vitreous complex dehalogenation agent 失效
    用无水无定形玻璃体络合物脱卤剂生产芳香族硫化物聚合物的方法

    公开(公告)号：US4514558A

    公开(公告)日：1985-04-30

    申请号：US560988

    申请日：1983-12-13

    申请人： Zenya Shiiki ,  Yo Iizuka ,  Yukichika Kawakami

    发明人： Zenya Shiiki ,  Yo Iizuka ,  Yukichika Kawakami

    IPC分类号： C08G75/02 ,  C08G75/06 ,  C08G75/16

    CPC分类号： C08G75/025

    摘要： A process for obtaining an aromatic sulfide polymer which has a markedly high molecular weight and can be readily formed into films, fibers, and other structures. The process comprises heating, to a temperature of 100.degree. to 270.degree. C. in an organic solvent under the coexistence of a very small amount of water, a dihaloaromatic compound and a substantially anhydrous amorphous vitreous compound composed of (i) S.sup.2- anions and other inorganic salt-forming anions and (ii) ions of an alkali metal and/or an alkaline earth metal.

    摘要翻译： 一种获得具有显着高分子量并可容易地形成薄膜，纤维和其它结构的芳族硫化物聚合物的方法。 该方法包括在非常少量的水，二卤代芳族化合物和基本上无水的无定形玻璃质混合物的共存下，在有机溶剂中加热至100至270℃，所述无定形玻璃化合物由（i）S2-阴离子和 其它无机成盐阴离子和（ⅱ）碱金属和/或碱土金属的离子。

    Controlled release formulations using intelligent polymers
    7.
    发明申请
    Controlled release formulations using intelligent polymers 审中-公开
    使用智能聚合物的控制释放配方

    公开(公告)号：US20050214368A1

    公开(公告)日：2005-09-29

    申请号：US11109067

    申请日：2005-04-19

    申请人： Yukichika Kawakami ,  Nobuo Sato ,  Mitsuru Hoshino ,  Toshitaka Kouyama ,  Zenya Shiiki

    发明人： Yukichika Kawakami ,  Nobuo Sato ,  Mitsuru Hoshino ,  Toshitaka Kouyama ,  Zenya Shiiki

    IPC分类号： A61K9/14 ,  A61K9/20 ,  A61K9/22 ,  A61K9/28 ,  A61K31/716

    CPC分类号： A61K9/2846 ,  A61K9/2054 ,  A61K9/2077 ,  A61K31/716

    摘要： A controlled release pharmaceutical composition comprises (a) at least one pharmaceutically active substance having a water contact angle (θ) such that cos θ is between +0.9848 and −0.9848, (b) a first intelligent polymer component; and (c) a second intelligent polymer component having opposite wettability characteristics to the first intelligent polymer component, the first and second polymer components being present in a ratio in the range of about 1:100 to about 100:1 by weight. The polymer components are effective for controlled release of the pharmaceutically active substance from the composition.

    摘要翻译： 控释药物组合物包含（a）至少一种具有水接触角（θ）的药物活性物质，使得cosθ在+ 0.9848和-0.9848之间，（b）第一智能聚合物组分; 和（c）具有与第一智能聚合物组分相反润湿特性的第二智能聚合物组分，第一和第二聚合物组分以约1:100至约100:1重量比的比例存在。 聚合物组分对于从组合物中控制释放药物活性物质是有效的。

    Production process for injection-molded product of polyglycolic acid
    8.
    发明授权
    Production process for injection-molded product of polyglycolic acid 有权
    聚乙醇酸注射成型产品的生产工艺

    公开(公告)号：US06183679B2

    公开(公告)日：2001-02-06

    申请号：US09504604

    申请日：2000-02-15

    申请人： Yukichika Kawakami ,  Nobuo Sato ,  Mitsuru Hoshino ,  Toshitaka Kouyama ,  Zenya Shiiki

    发明人： Yukichika Kawakami ,  Nobuo Sato ,  Mitsuru Hoshino ,  Toshitaka Kouyama ,  Zenya Shiiki

    IPC分类号： B29C4500

    CPC分类号： C08G63/08 ,  B29C45/0001 ,  C08L67/04

    摘要： The invention provides an injection-molded product of polyglycolic acid obtainable by molding a thermoplastic resin material at an injection temperature ranging from the melting point, Tm of the polymer to 255° C., wherein the thermoplastic resin material comprises polyglycolic acid having a repeating unit represented by the following formula (1): and the following physical properties: (a) the melt viscosity, &eegr;* [as measured at a temperature of (the melting point, Tm of the polymer+20° C.) and a shear rate of 1,000/sec] being 30-10,000 Pa·s; (b) the melting point, Tm being at least 150° C.; (c) the melt enthalpy, &Dgr;Hm being at least 20 J/g; and (d) the density being at least 1.50 g/cm3 as measured in an unoriented, crystallized form, and a production process thereof.

    摘要翻译： 本发明提供一种聚乙醇酸的注射成型品，其通过在从聚合物的熔点Tm至255℃的注射温度下模制热塑性树脂材料而得到，其中热塑性树脂材料包含具有重复单元的聚乙醇酸 由下式（1）表示：和（a）熔体粘度eta * [在（熔点，聚合物的Tm + 20℃）的温度和剪切速率 1,000 /秒]为30-10,000Pa.s;（b）熔点Tm为至少150℃;（c）熔体焓DELTAHm为至少20J / g; 和（d）以非取向的结晶形式测量的密度为至少1.50g / cm 3，及其制造方法。

    Aromatic thioether ketone/thioether sulfone copolymer and production process thereof
    10.
    发明授权
    Aromatic thioether ketone/thioether sulfone copolymer and production process thereof 失效
    芳香族硫醚酮/硫醚砜共聚物及其制备方法

    公开(公告)号：US5369191A

    公开(公告)日：1994-11-29

    申请号：US3034

    申请日：1993-01-12

    申请人： Yukichika Kawakami ,  Zenya Shiiki

    发明人： Yukichika Kawakami ,  Zenya Shiiki

    IPC分类号： C08G75/02 ,  D01F6/76 ,  C08G75/14 ,  C08L81/04

    CPC分类号： C08G75/0254 ,  C08G75/0236 ,  D01F6/76 ,  Y10S525/906

    摘要： Disclosed herein are an aromatic thioether ketone/thioether sulfone random copolymer comprising phenylene thioether ketone recurring units (I) and phenylene thioether sulfone recurring units (II), (a) the compositional ratio (I:II) of the recurring units (I) to the recurring units (II) ranging from 98:2 to 65:35, (b) the solution viscosity (.eta..sub.inh) being at least 0.3 dl/g, (c) the melt crystallization time (f) being at least 3 minutes, (d) the melting point (Tm) being 300.degree.-350.degree. C., (e) the glass transition temperature being at least 125.degree. C., (f) the retention (400.degree. C./20 min) of melt crystallization enthalpy (.DELTA.Hmc) being at least 60%, and (g) the average particle size being at least 0.1 mm, and the production process thereof.

    摘要翻译： 本文公开了包含亚苯基硫醚酮重复单元（I）和亚苯基硫醚砜重复单元（II）的芳香族硫醚酮/硫醚砜无规共聚物，（a）重复单元（I）至（II）的组成比（I：II） 重复单元（II）的范围为98:2至65:35，（b）溶液粘度（eta inh）为至少0.3dl / g，（c）熔融结晶时间（f）为至少3分钟， （d）熔点（Tm）为300〜-350℃，（e）玻璃化转变温度为至少125℃，（f）熔融结晶的保留时间（400℃/ 20分钟） 焓（DELTA Hmc）为至少60％，（g）平均粒径为0.1mm以上，及其制造方法。