公开(公告)号：US12043564B2

公开(公告)日：2024-07-23

申请号：US17872407

申请日：2022-07-25

申请人： SHIN-ETSU CHEMICAL CO., LTD.

发明人： Naoto Noda ,  Hitoshi Iinuma

IPC分类号： C03B37/014 ,  C03B37/016 ,  C03B37/07 ,  G02B1/04

CPC分类号： C03B37/01433 ,  C03B37/016 ,  C03B37/07 ,  G02B1/046

摘要： A manufacturing method of a porous glass base material for optical fiber includes: controlling a flow rate of a raw material liquid of an organic siloxane by a liquid mass flow controller; introducing raw material liquid to a raw material liquid nozzle of a vaporizer by a raw material liquid pipe; ejecting raw material liquid into the vaporizer; mixing raw material liquid and carrier gas to vaporize raw material liquid to form mixed gas; supplying mixed gas to a burner; combusting mixed gas together with a combustible gas and a combustion supporting gas in the burner to produce SiO2 particles; depositing SiO2 particles on a starting core base material to form the porous glass base material; and closing an open/close valve on a flow path of the raw material liquid pipe to stop supply of raw material liquid, while continuing to supply carrier gas, combustible gas, and combustion supporting gas.

公开(公告)号：US11897807B2

公开(公告)日：2024-02-13

申请号：US17872376

申请日：2022-07-25

申请人： SHIN-ETSU CHEMICAL CO., LTD.

发明人： Naoto Noda ,  Hitoshi Iinuma

IPC分类号： C03B37/014 ,  C03B37/016 ,  C03B37/07 ,  G02B1/04

CPC分类号： C03B37/01433 ,  C03B37/016 ,  C03B37/07 ,  G02B1/046

摘要： A porous glass base material manufacturing apparatus for an optical fiber includes: a liquid mass flow controller for controlling a flow rate of raw material liquid of an organic siloxane; a vaporizer for mixing raw material liquid and carrier gas to vaporize raw material liquid to form mixed gas; a raw material liquid nozzle for ejecting raw material liquid into the vaporizer; a carrier gas supply pipe for supplying carrier gas into the vaporizer; a raw material liquid pipe for introducing raw material liquid into the nozzle; a burner for combusting mixed gas with combustible gas and combustion supporting gas to produce SiO2 particles; a mixed gas pipe for supplying mixed gas to the burner; an open/close valve on a flow path of the raw material liquid pipe; and a purge gas supply pipe that joins the raw material liquid pipe between the valve and the raw material liquid nozzle.

公开(公告)号：US11807566B2

公开(公告)日：2023-11-07

申请号：US16464183

申请日：2018-03-16

申请人： SYNTHERA BIOMEDICAL PRIVATE LIMITED

发明人： Amol Vasudeo Chaudhari ,  Nilay Jayant Lakhkar

IPC分类号： C03B19/09 ,  C03C4/00 ,  C03C11/00 ,  C03C3/16 ,  B01J31/02 ,  C03B19/08 ,  C03B19/10 ,  C03B19/12 ,  C03B37/01 ,  C03B37/016 ,  C03C3/21 ,  C03C1/00

CPC分类号： C03B19/09 ,  B01J31/0237 ,  C03B19/08 ,  C03B19/1045 ,  C03B19/1065 ,  C03B19/12 ,  C03B37/011 ,  C03B37/016 ,  C03C1/006 ,  C03C3/21 ,  C03C4/0014 ,  C03C11/007 ,  C03C2203/10 ,  C03C2203/20 ,  C03C2203/36 ,  C03C2203/52

摘要： The invention discloses porous, bioactive glass and glass ceramic morsels or pellets to be used as tissue graft substitute materials and processes for obtaining the same wherein the bioactive glass and glass ceramic morsels or pellets are made up of natural agents like phosphate, calcium, sodium and other elements which are not alien to the human or animal body. The said preparation process encompasses various steps like quenching sintering, foaming, and sol-gel casting which render the glass morsels or pellets unique bioactivity and enhanced porosity which may facilitate tissue repair and augmentation during tissue graft replacement.

公开(公告)号：US20220363583A1

公开(公告)日：2022-11-17

申请号：US17872407

申请日：2022-07-25

申请人： SHIN-ETSU CHEMICAL CO., LTD.

发明人： Naoto NODA ,  Hitoshi IINUMA

IPC分类号： C03B37/014 ,  C03B37/016 ,  C03B37/07 ,  G02B1/04

摘要： A manufacturing method of a porous glass base material for optical fiber includes: controlling a flow rate of a raw material liquid of an organic siloxane by a liquid mass flow controller; introducing raw material liquid to a raw material liquid nozzle of a vaporizer by a raw material liquid pipe; ejecting raw material liquid into the vaporizer; mixing raw material liquid and carrier gas to vaporize raw material liquid to form mixed gas; supplying mixed gas to a burner; combusting mixed gas together with a combustible gas and a combustion supporting gas in the burner to produce SiO2 particles; depositing SiO2 particles on a starting core base material to form the porous glass base material; and closing an open/close valve on a flow path of the raw material liquid pipe to stop supply of raw material liquid, while continuing to supply carrier gas, combustible gas, and combustion supporting gas.

公开(公告)号：US09266765B2

公开(公告)日：2016-02-23

申请号：US14348260

申请日：2012-09-28

申请人： Commissariat a l'energie atomique et aux ene alt

发明人： Tarek Fathallah ,  Gilles Marchand

IPC分类号： B29C47/76 ,  C03B19/12 ,  C03B37/016 ,  C03C1/00 ,  C04B35/624 ,  C04B35/14 ,  C04B35/16 ,  B28B11/12 ,  B28B1/24 ,  B28B7/34

CPC分类号： C03B19/12 ,  B28B1/24 ,  B28B7/344 ,  B28B7/346 ,  B28B7/348 ,  B28B11/12 ,  C03B37/016 ,  C03B2201/02 ,  C03B2201/42 ,  C03C1/006 ,  C03C2203/26 ,  C04B35/14 ,  C04B35/16 ,  C04B35/624 ,  C04B2235/3232 ,  C04B2235/441 ,  C04B2235/6027 ,  C04B2235/606

摘要： A process for manufacturing an object made of a constituent material obtained from a sol-gel solution, the process including, successively: a) introducing the sol-gel solution into a mold of the object to be manufactured; b) gelling the sol-gel solution; c) drying the gel obtained in b) in the mold, by which the gel is converted into the constituent material of the object, wherein the mold includes a closed chamber and includes a material configured to allow evacuation of gases formed during b) and/or c).

摘要翻译： 一种制造由溶胶 - 凝胶溶液获得的构成材料制成的物体的方法，该方法包括：a）将溶胶 - 凝胶溶液引入待制造物体的模具中; b）凝胶溶胶凝胶溶液; c）将模具中b）中获得的凝胶干燥，通过该凝胶将凝胶转化成物体的构成材料，其中模具包括封闭室，并且包括被配置为允许排空在b）和/ 或c）。

公开(公告)号：US20150110452A1

公开(公告)日：2015-04-23

申请号：US14395698

申请日：2013-05-13

申请人： OFS FITEL, LLC ,  RAYTHEON COMPANY

发明人： David J. Digiovanni ,  Dennis J. Trevor ,  David A. Rockwell ,  Vladimir Shkunov

IPC分类号： G02B6/028 ,  C03B37/016 ,  C03B37/012 ,  C03B37/018

CPC分类号： G02B6/028 ,  C03B37/01268 ,  C03B37/01297 ,  C03B37/016 ,  C03B37/018 ,  C03B2201/06 ,  C03B2203/12 ,  C03B2203/22 ,  H01S3/0672 ,  H01S3/06729 ,  H01S3/06737 ,  H01S3/08045 ,  H01S3/1618 ,  H01S3/1698

摘要： High aspect ratio core optical fiber designs, which could be semi-guiding, including a core region having a first refractive index and a high aspect ratio elongated cross-section along a slow axis direction, are described. An internal cladding having a second refractive index sandwiches the core and acts as a fast-axis signal cladding. The core has an edge region at both of its short edges that is in contract with edge-cladding regions having a barbell shape. The refractive index of the core regions, the refractive index of the internal claddings, and the refractive index of the edge-cladding regions, are selected so as to maximize the optical power of a lowest-order mode propagating in the fiber core, and to minimize the optical power of the next-order modes in the fiber core. A process to fabricate such a high aspect ratio core fiber is also provided.

摘要翻译： 描述了可以是半导向的高纵横比纤芯光纤设计，包括沿慢轴方向具有第一折射率和高纵横比细长横截面的芯区域。 具有第二折射率的内部包层夹住芯并用作快轴信号包层。 芯具有在其短边缘处的边缘区域，其与具有杠铃形状的边缘包层区域收缩。 选择核心区域的折射率，内部包层的折射率和边缘包层区域的折射率，以使在纤维芯中传播的最低阶模的光功率最大化，并且 最小化光纤芯中下一阶模式的光功率。 还提供了制造这种高纵横比纤芯的方法。

公开(公告)号：US08861912B2

公开(公告)日：2014-10-14

申请号：US13476622

申请日：2012-05-21

申请人： Jeong I. Kim ,  Daniel Kominsky ,  Gary Pickrell ,  Ahmad Safaai-Jazi ,  Roger H Stolen ,  Anbo Wang

发明人： Jeong I. Kim ,  Daniel Kominsky ,  Gary Pickrell ,  Ahmad Safaai-Jazi ,  Roger H Stolen ,  Anbo Wang

IPC分类号： G02B6/032 ,  G02B6/02 ,  C03B37/027 ,  C03C13/04 ,  C03B37/016 ,  C03B37/012 ,  G01L1/24 ,  C03C11/00

CPC分类号： G02B6/02385 ,  C03B37/01297 ,  C03B37/016 ,  C03B37/02781 ,  C03B2203/14 ,  C03B2203/42 ,  C03C11/007 ,  C03C13/04 ,  G01L1/243 ,  G02B6/02295 ,  G02B6/02333 ,  G02B6/02338 ,  G02B6/02357 ,  G02B6/02366 ,  G02B6/032

摘要： A random array of holes is created in an optical fiber by gas generated during fiber drawing. The gas forms bubbles which are drawn into long, microscopic holes. The gas is created by a gas generating material such as silicon nitride. Silicon nitride oxidizes to produce nitrogen oxides when heated. The gas generating material can alternatively be silicon carbide or other nitrides or carbides. The random holes can provide cladding for optical confinement when located around a fiber core. The random holes can also be present in the fiber core. The fibers can be made of silica. The present random hole fibers are particularly useful as pressure sensors since they experience a large wavelength dependant increase in optical loss when pressure or force is applied.

摘要翻译： 在纤维拉伸中产生的气体在光纤中产生随机阵列的孔。 气体形成气泡，其被吸入长的微观孔中。 气体由诸如氮化硅的气体发生材料产生。 氮化硅在加热时氧化生成氮氧化物。 气体发生材料可以替代地是碳化硅或其它氮化物或碳化物。 当位于纤维芯周围时，随机孔可以提供用于光学限制的包层。 随机孔也可以存在于纤维芯中。 纤维可以由二氧化硅制成。 当前的随机孔纤维作为压力传感器是特别有用的，因为当施加压力或力时，它们经历大的波长依赖性的光学损失增加。

公开(公告)号：US20130223804A1

公开(公告)日：2013-08-29

申请号：US13476622

申请日：2012-05-21

申请人： Jeong I. KIM ,  Daniel KOMINSKY ,  Gary PICKRELL ,  Ahmad SAFAAI-JAZI ,  Roger H. STOLEN ,  Anbo WANG

发明人： Jeong I. KIM ,  Daniel KOMINSKY ,  Gary PICKRELL ,  Ahmad SAFAAI-JAZI ,  Roger H. STOLEN ,  Anbo WANG

IPC分类号： C03B37/016 ,  G02B6/02

CPC分类号： G02B6/02385 ,  C03B37/01297 ,  C03B37/016 ,  C03B37/02781 ,  C03B2203/14 ,  C03B2203/42 ,  C03C11/007 ,  C03C13/04 ,  G01L1/243 ,  G02B6/02295 ,  G02B6/02333 ,  G02B6/02338 ,  G02B6/02357 ,  G02B6/02366 ,  G02B6/032

摘要： A random array of holes is created in an optical fiber by gas generated during fiber drawing. The gas forms bubbles which are drawn into long, microscopic holes. The gas is created by a gas generating material such as silicon nitride. Silicon nitride oxidizes to produce nitrogen oxides when heated. The gas generating material can alternatively be silicon carbide or other nitrides or carbides. The random holes can provide cladding for optical confinement when located around a fiber core. The random holes can also be present in the fiber core. The fibers can be made of silica. The present random hole fibers are particularly useful as pressure sensors since they experience a large wavelength dependant increase in optical loss when pressure or force is applied.

公开(公告)号：US20070074540A1

公开(公告)日：2007-04-05

申请号：US11635440

申请日：2006-12-06

申请人： Gang Chen ,  Ronen Rapaport ,  Elsa Reichmanis ,  Shu Yang

发明人： Gang Chen ,  Ronen Rapaport ,  Elsa Reichmanis ,  Shu Yang

IPC分类号： C03B37/016

CPC分类号： C03B19/12 ,  C03B2201/58 ,  C03C11/00

摘要： Techniques for producing a glass structure having interconnected macroscopic pores, including providing a polymeric structure having interconnected macroscopic pores; providing polymerizable glass precursors; filling pores in the polymeric structure with the polymerizable glass precursors; polymerizing the polymerizable glass precursors to yield a filled polymeric structure; and decomposing the filled polymeric structure to produce a glass structure having interconnected macroscopic pores. Techniques for filling pores of such glass structure with a material having a high refractive index, and for then removing the glass structure. Structures can be produced having interconnected macroscopic pores and high refractive index contrasts, which can be used, for example, as photonic band gaps.

摘要翻译： 用于生产具有互连的宏观孔的玻璃结构的技术，包括提供具有互连的宏观孔的聚合物结构; 提供可聚合玻璃前体; 用可聚合玻璃前体填充聚合物结构中的孔; 聚合可聚合的玻璃前体以产生填充的聚合物结构; 并分解填充的聚合物结构以产生具有互连的宏观孔的玻璃结构。 用具有高折射率的材料填充这种玻璃结构的孔的技术，然后去除玻璃结构。 可以制造具有互连的宏观孔和高折射率对比度的结构，其可以用作例如光子带隙。

公开(公告)号：US20060086149A1

公开(公告)日：2006-04-27

申请号：US11216865

申请日：2005-08-31

申请人： Soon-Jae Kim ,  Keun-Deok Park ,  Jin-Han Kim

发明人： Soon-Jae Kim ,  Keun-Deok Park ,  Jin-Han Kim

IPC分类号： C03B37/075 ,  C03B37/016

CPC分类号： C03B37/016 ,  C03B2203/14 ,  C03B2203/42

摘要： An apparatus for manufacturing a photonic crystal fiber preform having a plurality of holes that extend in a lengthwise direction of the photonic crystal fiber perform is disclosed. The apparatus includes a housing for receiving a raw material for the photonic crystal fiber perform, a first support section arranged at an upper part of the housing; a second support section arranged at a lower part of the housing, and a plurality of pins supported by the first and second support sections. At least a portion of each pin is positioned in the housing. The apparatus also includes a vacuum pump for vacuumizing the interior of the housing; a first pipe connected to the lower part of the housing to introduce the raw material into the housing; and a first valve installed on the first pipe to open and close the first pipe.

摘要翻译： 公开了一种用于制造具有沿光子晶体光纤的长度方向延伸的多个孔的光子晶体光纤预制件的装置。 该装置包括用于接收用于光子晶体光纤的原材料的壳体，布置在壳体的上部的第一支撑部分; 布置在壳体的下部的第二支撑部分和由第一和第二支撑部分支撑的多个销。 每个销的至少一部分定位在壳体中。 该装置还包括一个真空泵，用于抽真空壳体的内部; 连接到所述壳体的下部以将所述原料引入所述壳体中的第一管; 以及安装在第一管上以打开和关闭第一管的第一阀。