Process to obtain polyglycolyl urea from aromatic diglycinates for electric conductor insulation
    2.
    发明申请
    Process to obtain polyglycolyl urea from aromatic diglycinates for electric conductor insulation 审中-公开
    从芳族二乙酸酯获得聚乙烯基脲用于导电绝缘的方法

    公开(公告)号:US20010047076A1

    公开(公告)日:2001-11-29

    申请号:US09750483

    申请日:2000-12-28

    CPC classification number: C08G18/3821

    Abstract: A process for obtaining polyglycolyl urea from aromatic diglycinate, to insulate electric conductors without forming HCN polluting residues, characterized because a mixture of methylene bromopropionate and methylenedianiline in aliphatic solvent reacts in presence of a catalizer; the solvent is separated through distillation, filtration of the mother waters and purification through washing with water and addition to the resulting product of cresylic acid and methylene dilisocyanate under stirring, up to a temperature, of 60null C., and addition of a triethylenediamino catalizer, heating at a temperature of up to 185null C. and it is then distilled at a temperature of up to 200null C., obtaining a polyglycolyl urea hydantoin resin.

    Abstract translation: 一种从芳族二乙二醇酸获得聚乙烯酰脲的方法,使电导体绝缘而不形成HCN污染残留物,其特征在于在脂肪族溶剂中亚甲基溴丙酸酯和亚甲基二苯胺的混合物在催化剂存在下反应; 通过蒸馏分离溶剂,过滤母体水并通过用水洗涤纯化,并在搅拌下加入到产物甲酸和亚甲基二异氰酸酯的产物中,直至温度为60℃,并加入三乙烯二胺催化剂 在高达185℃的温度下加热,然后在高达200℃的温度下蒸馏,得到聚乙烯酰脲乙内酰脲树脂。

    Method for isolating polyphenylene ether polymer resins from solution
    3.
    发明申请
    Method for isolating polyphenylene ether polymer resins from solution 失效
    从溶液中分离聚苯醚聚合物树脂的方法

    公开(公告)号:US20030111186A1

    公开(公告)日:2003-06-19

    申请号:US10005934

    申请日:2001-11-12

    CPC classification number: B01D1/225 C08G65/48

    Abstract: A method of removing substantially all solvent from a solution containing a polyphenylene ether polymer resin with little by-product formation (less than 250 ppm) is provided. The method employs a wiped thin film evaporator with a cylindrical heating chamber operating under conditions that satisfy the relationships defined by Equations I and II. 5.3*1024RLnull exp(null24123/T)/m

    Abstract translation: 提供了从含有少量副产物形成的聚苯醚聚合物树脂(小于250ppm)的溶液中除去基本上所有溶剂的方法。 该方法采用具有圆柱形加热室的擦拭薄膜蒸发器,其工作条件满足方程式I和II定义的关系。 5.3 * 1024RLdelta exp(-24123 / T)/ m

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