公开(公告)号：WO2013082343A1

公开(公告)日：2013-06-06

申请号：PCT/US2012/067171

申请日：2012-11-30

Applicant: CORNING INCORPORATED ,  HAMILTON, James Patrick ,  HRDINA, Kenneth Edward

Inventor： HAMILTON, James Patrick ,  HRDINA, Kenneth Edward

IPC: C03C23/00 ,  C03C21/00

CPC classification number: C03C23/008 ,  C03C21/006 ,  H01L31/03923 ,  H01L31/03925 ,  Y02E10/541

Abstract: A method of leaching alkali ions from a glass substrate to form a glass substrate having an intrinsic alkali barrier layer including providing a glass substrate comprising alkali metal ions, alkaline earth metal ions, or a combination thereof and contacting the surfaces of the substrate with a solution comprising a hydrogen bearing species such that at least a portion of the hydrogen bearing species replaces at least a portion of the alkali metal ions, alkaline earth metal ions, or the combination thereof in the at least one surface to form the glass substrate having the intrinsic alkali barrier layer.

Abstract translation: 一种从玻璃基板浸出碱离子以形成具有本征碱性阻挡层的玻璃基板的方法，该方法包括提供包括碱金属离子，碱土金属离子或其组合的玻璃基板，并使基板的表面与溶液接触 包括含氢物质，使得至少一部分含氢物质在至少一个表面中替换至少一部分碱金属离子，碱土金属离子或其组合，以形成具有本征态的玻璃基底 碱阻隔层。

公开(公告)号：WO2018118964A1

公开(公告)日：2018-06-28

申请号：PCT/US2017/067376

申请日：2017-12-19

Applicant: CORNING INCORPORATED ,  BADDING, Michael Edward ,  BOMBA, Richard Dominic ,  BROWN, Jacqueline Leslie ,  BOUTON, William Joseph ,  HRDINA, Kenneth Edward ,  KETCHAM, Thomas Dale ,  MERZ, Gary Edward ,  MILLER, Eric Lee ,  SHASHIDHAR, Nagaraja ,  ST. JULIEN, Dell Joseph ,  SONG, Zhen ,  TANNER, Cameron Wayne ,  WALSH, Conor James

Inventor： BADDING, Michael Edward ,  BOMBA, Richard Dominic ,  BROWN, Jacqueline Leslie ,  BOUTON, William Joseph ,  HRDINA, Kenneth Edward ,  KETCHAM, Thomas Dale ,  MERZ, Gary Edward ,  MILLER, Eric Lee ,  SHASHIDHAR, Nagaraja ,  ST. JULIEN, Dell Joseph ,  SONG, Zhen ,  TANNER, Cameron Wayne ,  WALSH, Conor James

IPC: C09J7/21 ,  C09J7/30 ,  C09J1/00

Abstract: A system is provided for sintering thin, wide, and/or long tape materials such as in a roll to roll process. The system is arranged to control sintering and limit deformation of the tape during sintering to produce sintered material.

公开(公告)号：WO2013116420A1

公开(公告)日：2013-08-08

申请号：PCT/US2013/023980

申请日：2013-01-31

Applicant: CORNING INCORPORATED ,  ALLEN, Douglas Clippinger ,  HRDINA, Kenneth Edward ,  ROSCH, William Rogers

Inventor： ALLEN, Douglas Clippinger ,  HRDINA, Kenneth Edward ,  ROSCH, William Rogers

IPC: C03C21/00

CPC classification number: C03C21/002

Abstract: The present disclosure is directed to a method for producing constancy of the ion-exchanged product stress profile through adjustment of ion-exchange conditions by taking account of the influence of salt bath poisoning on the baths useful lifetime. The present disclosure is directed to a method of ion-exchange in which the salt bath temperature and salt bath time are adjusted as a function of the amount of alkali metal ions that exchange in the bath. That is, temperature and time are adjusted as a function of salt bath poisoning. Temperature is set to its highest value and time to its shortest value in the starting un-poisoned salt bath, those values chosen to hit target values of surface compressive stress and exchange depth of layer. Temperature is then reduced and time lengthened as salt bath poisoning proceeds, those changes chosen to maintain the same surface compressive stress and exchange depth of layer.

Abstract translation: 本公开涉及一种通过考虑盐浴中毒对浴的使用寿命的影响来调节离子交换条件来产生离子交换产物应力分布的恒定性的方法。 本公开涉及一种离子交换方法，其中盐浴温度和盐浴时间作为在浴中交换的碱金属离子的量的函数来调节。 也就是说，温度和时间被调整为盐浴中毒的功能。 在起始的无毒盐浴中将温度设定为其最小值和时间到其最短值，这些值被选择以达到表面压应力的目标值和层的交换深度。 随着盐浴中毒的进行，温度降低，时间延长，这些变化被选择为保持相同的表面压应力和层的交换深度。

公开(公告)号：WO2014085529A1

公开(公告)日：2014-06-05

申请号：PCT/US2013/072146

申请日：2013-11-27

Applicant: CORNING INCORPORATED ,  ANNAMALAI, Sezhian ,  DURAN, Carlos, Alberto ,  HRDINA, Kenneth, Edward

Inventor： ANNAMALAI, Sezhian ,  DURAN, Carlos, Alberto ,  HRDINA, Kenneth, Edward

IPC: C03C3/06 ,  C03B19/14 ,  C03C4/00

CPC classification number: G03F1/22 ,  C03B19/12 ,  C03B19/1461 ,  C03B2201/075 ,  C03B2201/12 ,  C03B2201/20 ,  C03B2201/23 ,  C03B2201/32 ,  C03B2201/40 ,  C03B2201/42 ,  C03C3/06 ,  C03C4/0085 ,  C03C2201/12 ,  C03C2201/23 ,  C03C2201/32 ,  C03C2201/40 ,  C03C2201/42 ,  C03C2203/44 ,  C03C2203/54

Abstract: The present disclosure is directed to a doped silica-titania glass, DST glass, consisting essentially of 0.1 wt.% to 5 wt.% halogen, 50 ppm-wt. to 6 wt.% of one or more oxides of Al, Ta and Nb, 3 wt.% to 10 wt.% TiO 2 and the remainder SiO 2 . In an embodiment the halogen content can be in the range of 0.2 wt.% to 3 wt.% along with 50 ppm-wt. to 6 wt.% one or more oxides of Al, Ta and Nb, 3 wt.% to 10 wt.% TiO 2 and the remainder SiO 2 . In an embodiment the DST glass has an OH concentration of less than 100 ppm. In another embodiment the OH concentration is less than 50 ppm. The DST glass has a Active temperature T f of less than 875°C. In an embodiment T f is less than 825°C. In another embodiment T f is less than 775°C.

Abstract translation: 本公开涉及掺杂的二氧化硅 - 二氧化钛玻璃DST玻璃，其基本上由0.1重量％至5重量％的卤素组成，50重量ppm。 至6重量％的一种或多种Al，Ta和Nb的氧化物，3重量％至10重量％的TiO 2，余量为SiO 2。 在一个实施方案中，卤素含量可以在0.2重量％至3重量％的范围内以及50ppm重量的范围内。 至6重量％的一种或多种Al，Ta和Nb的氧化物，3重量％至10重量％的TiO 2，余量为SiO 2。 在一个实施方案中，DST玻璃的OH浓度小于100ppm。 在另一个实施方案中，OH浓度小于50ppm。 DST玻璃的活性温度Tf小于875℃。 在一个实施方案中，Tf小于825℃。 在另一个实施方案中，Tf小于775℃。

公开(公告)号：WO2014036116A1

公开(公告)日：2014-03-06

申请号：PCT/US2013/057041

申请日：2013-08-28

Applicant: CORNING INCORPORATED ,  ANNAMALAI, Sezhian ,  DAWES, Steven Bruce ,  HRDINA, Kenneth Edward

Inventor： ANNAMALAI, Sezhian ,  DAWES, Steven Bruce ,  HRDINA, Kenneth Edward

IPC: C03C3/06 ,  C03C3/076 ,  C03C3/095 ,  C03C3/097 ,  C03C4/00

CPC classification number: C03C3/097 ,  C03B19/12 ,  C03B2201/075 ,  C03B2201/23 ,  C03B2201/40 ,  C03B2201/42 ,  C03C3/06 ,  C03C3/076 ,  C03C3/095 ,  C03C4/0085 ,  C03C2201/23 ,  C03C2201/40 ,  C03C2201/42 ,  C03C2203/34 ,  C03C2203/42 ,  C03C2203/50

Abstract: This disclosure is directed to a silica-titania-niobia glass and to a method for making the glass. The composition of the silica-titania-niobia (SiO 2 -TiO 2 -Nb 2 O 5 ) glass, determined as the oxides, is Nb 2 O 5 in an amount in the range of 0.005 wt.% to 1.2 wt.% TiO 2 , in an amount in the range of 5 wt.% to 10 wt.%, and the remainder of glass is SiO 2 . In the method, the STN glass precursor is consolidated into a glass by heating to a temperature of 1600°C to 1700°C in flowing helium for 6 hours to 10 hours. When this temperature is reached, the helium flow can be replaced by argon for the remainder of the time. Subsequently the glass is cooled to approximately 1050°C, and then from 1050°C to 700°C followed by turning off the furnace and cooling the glass to room temperature at the natural cooling rate of the furnace.

Abstract translation: 本公开涉及二氧化硅 - 二氧化钛 - 铌玻璃和制造该玻璃的方法。 确定为氧化物的二氧化硅 - 二氧化钛 - 氧化铌（SiO2-TiO2-Nb2O5）玻璃的组成为0.005重量％至1.2重量％TiO 2的量的Nb 2 O 5，其量为 5重量％至10重量％，玻璃的其余部分为SiO 2。 在该方法中，通过在流动氦中加热至1600℃至1700℃的温度6小时至10小时，将STN玻璃前体固结成玻璃。 当达到这个温度时，氦气流可以在一段时间内用氩气代替。 随后将玻璃冷却至约1050℃，然后冷却至1050℃至700℃，随后关闭炉，并以炉的自然冷却速率将玻璃冷却至室温。

公开(公告)号：WO2013082246A1

公开(公告)日：2013-06-06

申请号：PCT/US2012/066993

申请日：2012-11-29

Applicant: CORNING INCORPORATED ,  FIACCO, Richard, Michael ,  HRDINA, Kenneth, Edward ,  ASHTON-PATTON, Melissann

Inventor： FIACCO, Richard, Michael ,  HRDINA, Kenneth, Edward ,  ASHTON-PATTON, Melissann

IPC: H01L31/00 ,  C03C3/00 ,  C03C3/06

CPC classification number: H01L31/03923 ,  C03C17/06 ,  C03C17/22 ,  C03C23/008 ,  C03C23/009 ,  C03C2217/26 ,  C03C2217/289 ,  H01L31/0392 ,  H01L31/03925 ,  Y02E10/541

Abstract: A method of moving alkali metal ions in a glass substrate to form a glass substrate having an intrinsic alkali metal barrier layer or an enhanced alkali metal layer by applying voltage to at least one of the surfaces of the substrate such that at least a portion of the alkali metal ions, alkaline earth metal ions, or the combination thereof in the at least one surface move into the thickness of the glass substrate.

Abstract translation: 一种使玻璃基板中的碱金属离子移动以通过向基板的至少一个表面施加电压以形成具有本征碱金属阻挡层或增强的碱金属层的玻璃基板的方法，使得至少一部分 碱金属离子，碱土金属离子或其至少一个表面的组合移动到玻璃基底的厚度中。