METHODS OF MAKING PROPPANT PARTICLES FROM SLURRY DROPLETS AND METHODS OF USE
    3.
    发明申请
    METHODS OF MAKING PROPPANT PARTICLES FROM SLURRY DROPLETS AND METHODS OF USE 审中-公开
    从浆液中制备优选颗粒的方法和使用方法

    公开(公告)号:WO2016149133A1

    公开(公告)日:2016-09-22

    申请号:PCT/US2016/022155

    申请日:2016-03-11

    Abstract: A method for making proppant particles is provided. The method can include providing a slurry of ceramic raw material, the slurry containing a reactant including a polycarboxylic acid, and flowing the slurry through a nozzle in a gas while vibrating the slurry to form droplets. The method can also include receiving the droplets in a vessel containing a liquid having an upper surface in direct contact with the gas, the liquid containing a coagulation agent. The method can further include reacting the reactant with the coagulation agent to cause coagulation of the reactant in the droplets. The droplets can then be transferred from the liquid and dried to form green pellets. The method can include sintering the green pellets in a selected temperature range to form the proppant particles. In one or more exemplary embodiments, the reactant can be or include a PMA:PAA copolymer.

    Abstract translation: 提供了制造支撑剂颗粒的方法。 该方法可以包括提供陶瓷原料的浆料,所述浆料含有包含多元羧酸的反应物,并且使浆料在气体中流过喷嘴,同时振动浆料以形成液滴。 该方法还可以包括在容器中容纳液滴,所述容器含有与气体直接接触的上表面的液体,所述液体含有凝结剂。 该方法还可以包括使反应物与凝结剂反应以引起反应物在液滴中的凝结。 然后可以将液滴从液体中转移并干燥以形成生球团。 该方法可以包括在选定的温度范围内烧结生球团矿以形成支撑剂颗粒。 在一个或多个示例性实施方案中,反应物可以是或包括PMA:PAA共聚物。

    PROPPANT PARTICLES FORMED FROM SLURRY DROPLETS AND METHOD OF USE
    4.
    发明申请
    PROPPANT PARTICLES FORMED FROM SLURRY DROPLETS AND METHOD OF USE 审中-公开
    从浆液中形成的主要颗粒和使用方法

    公开(公告)号:WO2014039968A1

    公开(公告)日:2014-03-13

    申请号:PCT/US2013/058763

    申请日:2013-09-09

    CPC classification number: C09K8/80 B01J2/04 B01J2/18 C09K8/68

    Abstract: Proppant material for hydraulic fracturing is provided. The particles of the proppant are formed by drip casting. A slurry of finely divided ceramic particles is flowed through nozzles and formed into droplets under the influence of vibration. Uniform sized, smooth surface, spherical green particles are formed. The green particles are dried and sintered to form the proppant. The proppant is used in the process of hydraulic fracturing of wells.

    Abstract translation: 提供水力压裂支撑材料。 支撑剂的颗粒通过滴注形成。 精细分散的陶瓷颗粒的浆料通过喷嘴流动并在振动的影响下形成液滴。 形成均匀的大小,光滑的表面,形成球形绿色颗粒。 将绿色颗粒干燥并烧结以形成支撑剂。 支撑剂用于水井压裂过程中。

    PROPPANT PARTICLES FORMED FROM SLURRY DROPLETS AND METHODS OF USE
    6.
    发明申请
    PROPPANT PARTICLES FORMED FROM SLURRY DROPLETS AND METHODS OF USE 审中-公开
    从浆液中形成的主要颗粒和使用方法

    公开(公告)号:WO2016054022A1

    公开(公告)日:2016-04-07

    申请号:PCT/US2015/052912

    申请日:2015-09-29

    Abstract: Proppant particles formed from slurry droplets and methods of use are disclosed herein. The proppant particles can include a sintered ceramic material and can have a size of about 80 mesh to about 10 mesh and an average largest pore size of less than about 20 microns. The methods of use can include injecting a hydraulic fluid into a subterranean formation at a rate and pressure sufficient to open a fracture therein and injecting a fluid containing a proppant particle into the fracture, the proppant particle including a sintered ceramic material, a size of about 80 mesh to about 10 mesh, and an average largest pore size of less than about 20 microns.

    Abstract translation: 本文公开了由浆料液滴形成的支撑剂颗粒和使用方法。 支撑剂颗粒可以包括烧结陶瓷材料,并且可以具有约80目至约10目的尺寸和小于约20微米的平均最大孔径。 使用的方法可以包括以足以在其中打开断裂的速率和压力将液压流体注入到地层中,并将含有支撑剂颗粒的流体注入断裂中,支撑剂颗粒包括烧结陶瓷材料,尺寸约为 80目至约10目,平均最大孔径小于约20微米。

    TAGGED PROPPING AGENTS AND RELATED METHODS
    7.
    发明申请
    TAGGED PROPPING AGENTS AND RELATED METHODS 审中-公开
    标签推荐代理和相关方法

    公开(公告)号:WO2005103446A1

    公开(公告)日:2005-11-03

    申请号:PCT/US2004/041594

    申请日:2004-12-13

    CPC classification number: C09K8/80 C09K8/805 E21B43/267 E21B47/1015

    Abstract: A proppant composition comprises a non-radioactive, detectable tracer at least partially embedded in a ceramic composition. The composition may be prepared by agglomerating granules of the ceramic material and granules of the non-radioactive, detectable material to produce the particle by compression. Backflow of proppants in a fractured subterranean formation into which a plurality of particles of the proppant composition have been introduced may be tracked by analyzing a sample of the backflow by detecting for presence of the tracer in the sample.

    Abstract translation: 支撑剂组合物包含至少部分地嵌入陶瓷组合物中的非放射性,可检测的示踪剂。 组合物可以通过将陶瓷材料的颗粒和非放射性可检测材料的颗粒附聚在一起来制备,以通过压缩产生颗粒。 可以通过检测样品中示踪剂的存在来分析回流的样品来跟踪已经引入多个支撑剂组合物颗粒的断裂地下地层中的支撑剂的回流。

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