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    POLYESTER HYDROGELS
    3.
    发明公开
    POLYESTER HYDROGELS 有权
    聚酯水凝胶

    公开(公告)号：EP3083753A1

    公开(公告)日：2016-10-26

    申请号：EP14825292.7

    申请日：2014-12-17

    Applicant: BASF SE

    Inventor： YAMAMOTO, Motonori ,  WISSEMEIER, Alexander ,  WEIGELT, Wolfgang ,  KELLER, Harald ,  SEUFERT, Michael ,  FERNANDEZ RAMIREZ, Gimmy Alex ,  SANZ-GOMEZ, Jorge ,  WIEDEMANN, Alexandra

    IPC: C08G63/676 ,  C08L67/06 ,  C08G63/52

    CPC classification number: C08G63/6888 ,  B01J20/262 ,  C05G3/04 ,  C08G63/52 ,  C08G63/676 ,  C08G63/916 ,  C08G2210/00 ,  C08G2310/00 ,  C09K17/18

    Abstract: The present invention relates to a polyester comprising units derived from monomers A, B and C, wherein the group of monomers A consists of (a1) monomers A1, or (a2) monomers A1 and monomers A2, with monomers A1 and monomers A2 being present in a molar ratio of at least 31:69, preferably at least 4:1, wherein the monomers A1 are selected from the group consisting of aromatic sulfonated dicarboxylic acid based monomers of general formulae (I), (II), (III) and (IV), and wherein the monomers A2 are selected from the group consisting of non-sulfonated aromatic dicarboxylic acid based monomers of general formulae (V), (VI) and (VII); and wherein the group of monomers B consists of (b1) monomers B1, or (b2) monomers B1 and monomers B2, with monomers B1 and monomers B2 being present in a molar ratio of at least 1:9, preferably at least 4:1, wherein the monomers B1 are selected from the group consisting of unsaturated dicarboxylic acid based monomers of general formula (VIII), and wherein the monomers B2 are selected from the group consisting of saturated dicarboxylic acid based monomers of general formula (IX); and wherein the group of monomers C consists of (c1) monomers C1, (c2) monomers C2, or (c3) monomers C1 and C2, wherein the monomers C1 are selected from the group consisting of ethylene glycol based monomers of general formula (X), and wherein the monomers C2 are selected from the group consisting of propylene glycol based monomers of general formula (XI), and wherein the molar ratio of the units derived from the group of monomers A to the units derived from the group of monomers B is from 9:1 to 1:2.4, and wherein the molar ratio of the units derived from the groups of monomers A and B to the units derived from the group of monomers C is from 1.3:1 to 1:1.3. The polyester of the invention is preferably cross-linked.

    Abstract translation: 本发明涉及包含衍生自单体A，B和C的单元的聚酯，其中单体A的组由单体A1或（a2）单体A1和单体A2组成，单体A1和单体A2存在 摩尔比为至少31:69，优选至少4:1，其中单体A1选自通式（I），（II），（III）和（II）的芳族磺化二羧酸基单体和 （IV），并且其中单体A2选自通式（V），（VI）和（VII）的非磺化芳族二羧酸基单体; 并且其中单体组B由（b1）单体B1或（b2）单体B1和单体B2组成，其中单体B1和单体B2以至少1:9，优选至少4:1的摩尔比存在 其中单体B1选自通式（VIII）的不饱和二羧酸基单体，并且其中单体B2选自通式（IX）的基于饱和二羧酸的单体; 并且其中单体组C由（c1）单体C1，（c2）单体C2或（c3）单体C1和C2组成，其中单体C1选自通式（X）的基于乙二醇的单体 ），并且其中单体C2选自通式（XI）的基于丙二醇的单体，并且其中衍生自单体A的单元的单元与衍生自单体B的单元的单元的摩尔比 为9:1至1:2.4，并且其中衍生自单体A和B的基团的单元与衍生自单体C的基团的单元的摩尔比为1.3:1至1:1.3。 本发明的聚酯优选交联。

    VEREINZELUNG EINER POLYARYLENETHERLÖSUNG
    6.
    发明公开
    VEREINZELUNG EINER POLYARYLENETHERLÖSUNG 审中-公开
    VEREINZELUNG EINERPOLYARYLENETHERLÖSUNG

    公开(公告)号：EP3022254A1

    公开(公告)日：2016-05-25

    申请号：EP14739821.8

    申请日：2014-07-16

    Applicant: BASF SE

    Inventor： ERBES, Jörg ,  MÜSSIG, Stefan ,  KORTEKAMP, Tobias ,  KRÜGER, Marco ,  STEFFEN, Markus ,  ULZHÖFER, Angela ,  SCHNEIDER, Cecile ,  WIEDEMANN, Alexandra ,  GRAMLICH, Simon

    IPC: C08J3/12 ,  C08J3/14 ,  C08G65/46 ,  C08G75/23

    CPC classification number: C08J3/14 ,  B29C48/04 ,  B29K2081/06 ,  C08G65/46 ,  C08G75/23 ,  C08J3/12 ,  C08J2381/06 ,  C08J2381/08

    Abstract: The invention relates to a method for producing polyarylene ether beads from a polyarylene ether solution, having the steps of i) separating the polyarylene ether solution in a separating device which is vibrated at a frequency ranging from 10 to 1400 Hz, thereby obtaining drops, and ii) transporting the drops into a precipitation bath, thereby forming polyarylene ether beads in the precipitation bath. The precipitation bath (A) contains at least one aprotic solvent (component (1)) and at least one protic solvent (component (2)), (B) has a temperature of 0 °C to T
    c , the critical temperature T
    c in [°C] being determined by the numerical equation T
    c = (77 - c)/0.58, in which c is the concentration of the component (1) in the precipitation bath in [wt.%], and (C) has the component (1) in concentrations of 5 wt.% to c
    c , the critical concentration c
    c in [wt.%] being determined by the numerical equation c
    c = 77 - 0.58 * T, in which T is the temperature in the precipitation bath in [°C], wherein the wt.% in each case is based on the sum of the wt.% of the component (1) and the component (2) in the precipitation bath.

    Abstract translation: 本发明涉及一种由聚芳醚溶液制备聚亚芳基醚珠粒的方法，包括以下步骤：i）将分散装置中的聚亚芳基醚溶液除以10-1400Hz的频率振动得到液滴，ii （A）包含至少一种非质子溶剂（组分（1））和至少一种质子溶剂（组分（2）），（B）具有至少一种质子溶剂 温度为0℃至Tc，其中[℃]中的临界温度Tc可以通过数学方程式Tc =（77-c）/0.58确定，其中c是组分（1）中的浓度 沉淀浴中的[重量％]和（C）的组分（1）的浓度为5重量％〜cc，其中临界浓度cc（重量％）可以通过数学式cc = 77-0.58 * T，其中T是沉淀浴中的温度[℃]，其中 重量百分比分别基于沉淀浴中组分（1）和组分（2）的重量百分比之和。

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