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    SULPHONIUM SALT INITIATORS
    2.
    发明公开
    SULPHONIUM SALT INITIATORS 有权
    硫磺盐引发剂

    公开(公告)号：EP2197840A1

    公开(公告)日：2010-06-23

    申请号：EP08804850.9

    申请日：2008-09-29

    Applicant: BASF SE

    Inventor： HAYOZ, Pascal ,  YAMATO, Hitoshi

    IPC: C07C381/12 ,  C09D5/03 ,  C09D5/08 ,  G03F7/004

    CPC classification number: G03F7/0045 ,  B33Y70/00 ,  C07C321/28 ,  C07C381/12 ,  C09D4/00 ,  C09D11/101 ,  G03F7/0007 ,  G03F7/031 ,  G03F7/038 ,  G03F7/0382 ,  G03F7/0392 ,  Y10S430/122 ,  Y10S430/123

    Abstract: Compounds of the formula (I), wherein X is a single bond, CRaRb O, S, NRC, NCORC, CO, SO or SO2; L, L1, L2, L3, L4, L5, L6, L7 and L8 are for example hydrogen, R1 or COT; T denotes T1 or O-T2; T1 and T2 for example are hydrogen, C1-C20alkyl, C3-C12cycloalkyl, C2-C20alkenyl, C5- C12cycloalkenyl, C6-C14aryl, C3-C12heteroaryl, C1-C20alkyl substituted by one or more D, C2- C20alkyl interrupted by one or more E, C2-C20alkyl substituted by one or more D and inter- rupted by one or more E or Q; R1, R2, R3, R4, Ra, Rb and Rc are T1; D is for example R5, OR5, SR5 or Q1; E is for example O, S, COO or Q2; R5 and R6 for example are hydrogen, C1- C12alkyl or phenyl; Q is for example C6-C12bicycloalkyl, C6-C12bicycloalkenyl or C6- C12tricycloalkyl; Q1 is for example, C6-C14aryl or C3-C12heteroaryl; Q2 is for example C6- C14arylene or C3-C12heteroarylene; Y is an anion; and M is a cation; provided that at least one of L, L1, L2, L3, L4, L5, L6, L7 and L8 is other than hydrogen; and provided that (i) at least one of T1 or T2 is a group Q; or (ii) at least one D is a group Q1; or (iii) at least one E is a group Q2; are suitable as photolatent catalysts.

    Abstract translation: 其中X是单键，CRaRbO，S，NRC，NCORC，CO，SO或SO 2的式（I）化合物; L，L 1，L 2，L 3，L 4，L 5，L 6，L 7和L 8是例如氢，R 1或COT; T表示T1或O-T2; T 1和T 2例如是氢，C 1 -C 20烷基，C 3 -C 12环烷基，C 2 -C 20烯基，C 5 -C 12环烯基，C 6 -C 14芳基，C 3 -C 12杂芳基，被一个或多个D取代的C 1 -C 20烷基， E，被一个或多个D取代并被一个或多个E或Q中断的C2-C20烷基; R1，R2，R3，R4，Ra，Rb和Rc是T1; D例如是R5，OR5，SR5或Q1; E例如是O，S，COO或Q2; 例如R5和R6是氢，C1-C12烷基或苯基; Q为例如C 6 -C 12双环烷基，C 6 -C 12双环烯基或C 6 -C 12三环烷基; Q1是例如C6-C14芳基或C3-C12杂芳基; Q2是例如C 6 -C 14亚芳基或C 3 -C 12杂亚芳基; Y是阴离子; M是阳离子; 条件是L，L1，L2，L3，L4，L5，L6，L7和L8中的至少一个不是氢; 并且（i）T1或T2中的至少一个是Q组; 或（ii）至少一个D是基团Q1; 或（iii）至少一个E是基团Q2; 适合作为潜光催化剂。

    OXIME DERIVATIVES AND THE USE THEREOF AS LATENT ACIDS
    6.
    发明授权
    OXIME DERIVATIVES AND THE USE THEREOF AS LATENT ACIDS 有权
    肟衍生物及其用途为递延酸

    公开(公告)号：EP1320785B1

    公开(公告)日：2010-02-17

    申请号：EP01985295.3

    申请日：2001-09-18

    Applicant: BASF SE

    Inventor： YAMATO, Hitoshi ,  ASAKURA, TOSHIKAGE ,  MATSUMOTO, Akira ,  OHWA, Masaki

    IPC: G03F7/004 ,  G03F7/038 ,  G03F7/039 ,  C07C309/63

    CPC classification number: G03F7/0392 ,  B33Y70/00 ,  G03F7/0045 ,  G03F7/0382

    Abstract: New oxime sulfonate compounds of formula (I, II, III, IV, V, VI and VII) wherein R1 is for example C1-C18 alkylsulfonyl, R2 is halogen or C1-C10 haloalkyl; R3 is for example unsubstituted or substituted phenylenedisulfonyl, diphenylenedisulfonyl, or oxydiphenylenedisulfonyl; Ar1 is for example a direct bond, C1-C12 alkylene; -O-C-bond or a O-Si-bond which cleaves upon the action of an acid; A1, A2, A3, A4, A5, A6, A7, A8, A9, A10, A11 and A12 are for example a direct bond, -O-, or S-, or are C1-C12 alkylene or phenylene unsubstituted or substituted; Y1 is C1-C12 alkylene which is for example subsituted by OR4, or SR7; Y2 is e.g. a trivalent radical of C1-C12 alkylene; Y3 is e.g. a tetravalent radical of C1-C12 alkylene; X is halogen; Ar'1 is for example C1-C12 alkyl which is unsubstituted or substituted; Ar'1 is for example phenylene; provided that at least one of the radicals Ar'1, Ar'1, is substituted by 1 to 3 groups of (VIII), (IX), (X), (XI), (XII) and/or (XIII); M+ is e.g. (XIV); L- is for example halogen; R¿15?, R16, R17 and R18 are e.g. hydrogen or phenyl; R19, R20, R21, R22 and R23 are e.g. phenyl; are especially suitable for the preparation of photoresists.

    6H-PYRROLO[3,2-B:4,5-B']BIS[1,4]BENZOTHIAZINE-6-CARBOXYLIC ACID ESTERS AS ORGANIC SEMICONDUCTOR MATERIALS FOR USE IN ELECTRONIC DEVICES
    7.
    发明公开
    6H-PYRROLO[3,2-B:4,5-B']BIS[1,4]BENZOTHIAZINE-6-CARBOXYLIC ACID ESTERS AS ORGANIC SEMICONDUCTOR MATERIALS FOR USE IN ELECTRONIC DEVICES 审中-公开
    6H-PYRROLO [3,2-B：4,5-B'] BIS [1,4]苯并吖嗪-6-羧酸酯用作电子器件

    公开(公告)号：EP3233868A1

    公开(公告)日：2017-10-25

    申请号：EP15810633.6

    申请日：2015-12-16

    Applicant: BASF SE

    Inventor： YAMATO, Hitoshi ,  TSUDA, Takuya ,  WU, Chao ,  WEITZ, Thomas ,  EUSTACHI, Michael ,  HEMGESBERG, Maximilian

    IPC: C07D513/14

    CPC classification number: H01L51/0071 ,  C07D513/14 ,  H01L51/0562

    Abstract: The present invention provides compounds of formula (I) wherein X is O, S or NR10,wherein R10 is H, C1-30-alkyl, substituted C1-30-alkyl, C2-30-alkenyl, substituted C2-30-alkenyl, C2-30-alkynyl, substituted C2-30-alkynyl or C(0)-OR11, R1 and R11 are independently from each other selected from the group consisting of C1-30-alkyl, substituted C1-30-alkyl, C2-30-alkenyl, substituted C2-30-alkenyl, C2-30-alkynyl, substituted C2-30-alkynyl, C5-8-cycloalkyl, substituted C5-8-cycloalkyl, C5-8-cycloalkenyl, and substituted C5-8-cycloalkenyl, and an electronic device comprising the compounds as semiconducting material.

    Abstract translation: 本发明提供了式（I）的化合物，其中X是O，S或NR 10，其中R 10是H，C 1-30烷基，取代的C 1-30烷基，C 2-30链烯基，取代的C 2-30-链烯基，C 2-30炔基，取代的C 2-30炔基或C（O）-OR 11，R 1和R 11彼此独立地选自C 1-30 - 烷基，取代的C 1-30烷基，C 2-30烯基，取代的C 2-30烯基，C 2-30炔基，取代的C 2-30炔基，C 5-8 - 环烷基，取代的C 5 -8-环烷基，C 5-8 - 环烯基和取代的C 5-8 - 环烯基的化合物，以及包含所述化合物作为半导体材料的电子器件。

    LATENT ACIDS AND THEIR USE
    9.
    发明公开
    LATENT ACIDS AND THEIR USE 审中-公开
    LATENTESÄURENUND IHRE VERWENDUNG

    公开(公告)号：EP2539316A1

    公开(公告)日：2013-01-02

    申请号：EP11702482.8

    申请日：2011-02-10

    Applicant: BASF SE

    Inventor： YAMATO, Hitoshi ,  ASAKURA, Toshikage ,  MATSUMOTO, Akira ,  TANAKA, Keita ,  NISHIMAE, Yuichi

    IPC: C07C309/08 ,  C07C309/12 ,  C07C311/53 ,  C07C333/06 ,  C07C381/12 ,  C07C25/18 ,  G03F7/004 ,  G03F7/039 ,  C07D209/00 ,  C07D241/00 ,  C07D265/00 ,  C07D311/00 ,  C07D235/00

    CPC classification number: C07C381/12 ,  C07C25/18 ,  C07C309/08 ,  C07C309/12 ,  C07C311/53 ,  C07C333/06 ,  C07C2601/14 ,  C07C2602/42 ,  C07C2603/74 ,  C07D207/28 ,  C07D233/38 ,  C07D241/08 ,  C07D295/205 ,  C07D295/215 ,  C07D493/08 ,  G03F7/0045 ,  G03F7/0046 ,  G03F7/0382 ,  G03F7/0392

    Abstract: The invention pertains to a compound generating an acid of the formula (I) or (II), for instance corresponding sulfonium and iodonium salts, as well as corresponding sulfonyloximes, Formula (I) and Formula (II), wherein X is CH
    2 or CO; Y is O, NR
    4 , S, O(CO), O(CO)O, O(CO)NR
    4 , OSO
    2 , O(CS), or O(CS)NR
    4 ; R
    1 is for example C
    1 -C
    18 alkyl, C
    1 -C
    10 haloalkyl, C
    2 -C
    12 alkenyl, C
    4 -C
    30 cycloalkenyl, phenyl-C
    1 -C
    3 -alkyl, C
    3 -C
    30 cycloalkyl, C
    3 -C
    30 cycloalkyl-C
    1 -C
    18 alkyl, interrupted C
    2 -C
    18 alkyl, interrupted C
    3 -C
    30 cycloalkyl, interrupted C
    3 -C
    30 cycloalkyl-C
    1 -C
    18 alkyl, interrupted C
    4 -C
    30 cycloalkenyl, phenyl, naphthyl, anthracyl, phenanthryl, biphenylyl, fluorenyl or heteroaryl, all unsubstituted or are substituted; or R
    1 is NR
    12 R
    13 ; R
    2 and R
    3 are for example C
    3 -C
    30 cycloalkylene, C
    3 -C
    30 cycloalkyl-C
    1 -C
    18 alkylene, C
    1 -C
    18 alkylene, C
    1 -C
    10 haloalkylene, C
    2 -C
    12 alkenylene, C
    4 -C
    30 cycloalkenylene, phenylene, naphthylene, anthracylene, phenanthrylene, biphenylene or heteroarylene; all unsubstituted or substituted; R
    4 is for example C
    3 -C
    30 cycloalkyl, C
    3 -C
    30 cycloalkyl-C
    1 -C
    18 alkyl, C
    1 -C
    18 alkyl, C
    1 -C
    10 haloalkyl, C
    2 -C
    12 alkenyl, C
    4 -C
    30 cycloalkenyl, phenyl-C
    1 -C
    3 -alkyl; R
    12 and R
    13 are for example C
    3 -C
    30 cycloalkyl, C
    3 -C
    30 cycloalkyl-C
    1 -C
    18 alkyl, C
    1 -C
    18 alkyl, C
    1 -C
    10 haloalkyl, C
    2 -C
    12 alkenyl, C
    4 -C
    30 cycloalkenyl, phenyl-C
    1 -C
    3 -alkyl, Ar, (CO)R
    15 , (CO)OR
    15 or SO
    2 R
    15 ; and Ar is phenyl, biphenylyl, fluorenyl, naphthyl, anthracyl, phenanthryl or heteroaryl, all unsubstituted or substituted.

    Abstract translation: 本发明涉及产生式（I）或（II）的酸的化合物，例如相应的锍盐和碘鎓盐，以及相应的磺酰肟，式（I）和式（II），其中X是CH 2或CO ; Y是O，NR4，S，O（CO），O（CO）O，O（CO）NR4，OSO2，O（CS）或O（CS）NR4; R1是例如C1-C18烷基，C1-C10卤代烷基，C2-C12链烯基，C4-C30环烯基，苯基-C1-C3-烷基，C3-C30环烷基，C3-C30环烷基-C1-C18烷基，间断的C 2 -C 18烷基，间断的C 3 -C 30环烷基， 间断的C 3 -C 30环烷基-C 1 -C 18烷基，间断的C 4 -C 30环烯基，苯基，萘基，蒽基，菲基，联苯基，芴基或杂芳基，全部未取代或被取代; 或R1为NR12R13; R 2和R 3例如为C 3 -C 30亚环烷基，C 3 -C 30环烷基-C 1 -C 18亚烷基，C 1 -C 18亚烷基，C 1 -C 10卤代亚烷基，C 2 -C 12亚烯基，C 4 -C 30亚环烯基，亚苯基，亚萘基，亚蒽基，亚菲基，亚联苯基或亚杂芳基。 全部未取代或取代; R4是例如C 3 -C 30环烷基，C 3 -C 30环烷基-C 1 -C 18烷基，C 1 -C 18烷基，C 1 -C 10卤代烷基，C 2 -C 12链烯基，C 4 -C 30环烯基，苯基-C 1 -C 3烷基; R 12和R 13例如为C 3 -C 30环烷基，C 3 -C 30环烷基-C 1 -C 18烷基，C 1 -C 18烷基，C 1 -C 10卤代烷基，C 2 -C 12烯基，C 4 -C 30环烯基，苯基-C 1 -C 3烷基，Ar，（CO）R 15（ CO）OR15或SO2R15; 并且Ar是苯基，联苯基，芴基，萘基，蒽基，菲基或杂芳基，全部是未取代或取代的。

    SULFONIUM DERIVATIVES AND THE USE THEREOF AS LATENT ACIDS
    10.
    发明公开
    SULFONIUM DERIVATIVES AND THE USE THEREOF AS LATENT ACIDS 审中-公开
    锍衍生物和它们作为递延ACIDS

    公开(公告)号：EP2288599A1

    公开(公告)日：2011-03-02

    申请号：EP09761637.9

    申请日：2009-06-02

    Applicant: BASF SE

    Inventor： NISHIMAE, Yuichi ,  ASAKURA, Toshikage ,  YAMATO, Hitoshi

    IPC: C07D327/08 ,  C07D339/08 ,  G03F7/00

    CPC classification number: C07D339/08 ,  C07D327/08

    Abstract: Compounds of the formula (I), wherein R
    1 , R
    2 and R
    3 for example are hydrogen, halogen, CN, C
    1 -C
    18 alkyl, C
    1 -C
    10 haloalkyl, (CO)R
    8 , (CO)OR
    4 , or (CO)NR
    5 R
    6 ; Y is O, S or CO; D
    2 , D
    3 and D
    4 for example are a direct bond, O, S, NR
    7 , CO, O(CO), (CO)O, S(CO), (CO)S, NR
    7 (CO), (CO)NR
    7 , SO, SO
    2 , or OSO
    2 , C
    1 -C
    18 alkylene, C
    3 -C
    30 cycloalkylene, C
    2 -C
    12 alkenylene, C
    4 -C
    30 cycloalkenylene, Ar
    1 ; Ar
    1 , Ar
    2 and Ar
    3 are for example phenylene, R
    4 , R
    5 , R
    6 , R
    7 and R
    8 are for example hydrogen, C
    3 -C
    30 cycloalkyl, C
    1 -C
    18 alkyl, C
    1 -C
    10 haloalkyl, C
    2 -C
    12 alkenyl, C
    4 -C
    30 cycloalkenyl, phenyl-C
    1 C
    3 -alkyl; X
    - is Formulae (IA), (IB) or (IC); R
    10 is for example C
    1 -C
    18 alkyl, C
    1 -C
    10 haloalkyl, camphoryl, phenyl-C
    1 -C
    3 alkyl, C
    3 -C
    30 cycloalkyl; and R
    11 , R
    12 , R
    13 , R
    14 and R
    15 are for example C
    1 -C
    10 haloalkyl; are useful as polymerizable photolatent acids.

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