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    Copolyetherimides
    1.
    发明授权
    Copolyetherimides 有权
    共聚酰亚胺

    公开(公告)号：US06849706B1

    公开(公告)日：2005-02-01

    申请号：US10647888

    申请日：2003-08-25

    申请人： Daniel Joseph Brunelle ,  Havva Yagci Acar ,  Farid Fouad Khouri ,  William David Richards

    发明人： Daniel Joseph Brunelle ,  Havva Yagci Acar ,  Farid Fouad Khouri ,  William David Richards

    IPC分类号： C08G73/12 ,  C08G73/00

    CPC分类号： C08G73/123 ,  C08G73/124 ,  C08G73/125

    摘要： Copolyetherimides comprise phthalimide structural units comprising both 3- and 4-linkages, wherein the designations 3-linkage and 4-linkage refer to the isomeric positions on the phthalimide ring in the totality of phthalimide-comprising structural units in the copolymer. The products have excellent properties, including high glass transition and heat distortion temperatures, high ductility and good melt flow properties, and low polydispersity.

    摘要翻译： 共聚酰亚胺包括包含3-和4-键的邻苯二甲酰亚胺结构单元，其中3-键和4-键的名称是指共聚物中邻苯二甲酰亚胺包含的结构单元总共在邻苯二甲酰亚胺环上的异构位置。 该产品具有优异的性能，包括高玻璃化转变和热变形温度，高延展性和良好的熔体流动性能，以及低的多分散性。

    Phase transfer catalyzed method for preparation of polyetherimides
    2.
    发明授权
    Phase transfer catalyzed method for preparation of polyetherimides 有权
    相转移催化聚醚酰亚胺的制备方法

    公开(公告)号：US07714095B2

    公开(公告)日：2010-05-11

    申请号：US11363681

    申请日：2006-02-28

    申请人： Daniel Joseph Brunelle ,  Havva Yagci Acar ,  Farid Fouad Khouri ,  Thomas Link Guggenheim ,  David Winfield Woodruff ,  Norman Enoch Johnson

    发明人： Daniel Joseph Brunelle ,  Havva Yagci Acar ,  Farid Fouad Khouri ,  Thomas Link Guggenheim ,  David Winfield Woodruff ,  Norman Enoch Johnson

    IPC分类号： C08G73/00 ,  C08G73/10 ,  C08G8/02 ,  C08G14/00

    CPC分类号： C08G73/12 ,  C08G73/121 ,  C08G73/124

    摘要： Polyether polymers, such as polyetherimides, are prepared by the reaction of a dihydroxy-substituted aromatic hydrocarbon alkali metal salt, such as bisphenol A disodium salt, with a bis(N-(chlorophthalimido))aromatic compound, such as 1,3- and/or 1,4-bis(N-(4-chlorophthalimido))benzene, in a solvent such as o-dichlorobenzene and in the presence of a phase transfer catalyst such as a hexaalkylguanidinium chloride. Several embodiments may be employed to improve the method. They comprise employing substantially dry reagents, employing a high solids level in solvent, beginning with an excess of bis(N-(chlorophthalimido))-aromatic compound and incrementally adding alkali metal salt, employing alkali metal salt of small particle size, and using reagents of high purity.

    摘要翻译： 聚醚聚合物如聚醚酰亚胺通过二羟基取代的芳族烃碱金属盐如双酚A二钠盐与双（N-（氯代邻苯二甲酰亚胺基））芳族化合物如1,3-和 /或1,4-双（N-（4-氯邻苯二甲酰亚氨基））苯，在溶剂如邻二氯苯中，并在相转移催化剂如六烷基氯化the存在下进行。 可以采用几个实施例来改进该方法。 它们包括使用基本上干的试剂，在溶剂中使用高固体含量，从过量的双（N-（氯代邻苯二甲酰亚胺基）） - 芳族化合物开始，并逐渐加入碱金属盐，使用小粒径的碱金属盐，并使用试剂 的高纯度。

    High heat polyethersulfone compositions
    4.
    发明授权
    High heat polyethersulfone compositions 有权
    高热聚醚砜组合物

    公开(公告)号：US07273919B1

    公开(公告)日：2007-09-25

    申请号：US11286181

    申请日：2005-11-21

    申请人： Daniel Steiger ,  Farid Fouad Khouri ,  Daniel Joseph Brunelle ,  Amy Beth Koren

    发明人： Daniel Steiger ,  Farid Fouad Khouri ,  Daniel Joseph Brunelle ,  Amy Beth Koren

    IPC分类号： C08G75/00 ,  C08G61/02 ,  C08G65/38 ,  C08G65/40

    CPC分类号： C08G75/23

    摘要： High heat polyethersulfone compositions are provided which possess unexpectedly high glass transition temperatures. The polyethersulfone compositions comprise structural units derived from phthalimide bisphenols such as 3,3-bis(4 -hydroxyphenyl)-N-phenylphthalimide, and structural units derived from at least one biphenyl-bissulfone such as 4,4′-bis((4-chlorophenyl)sulfonyl)-1,1′-biphenyl. The novel polyethersulfone compositions may further comprise structural units derived from one or more biphenols such as 4,4′-biphenol, bisphenols such as BPA, or other electrophilic sulfone monomers, such as bis(4-chlorophenyl)sulfone. In one embodiment, the polyethersulfone composition of the present invention comprises structural groups derived exclusively from 3,3-bis(4-hydroxyphenyl)-N-phenylphthalimide, and 4,4′-bis((4-chlorophenyl)sulfonyl)-1,1′-biphenyl and exhibits a single glass transition of greater than 300° C.

    摘要翻译： 提供了具有出人意料的高玻璃化转变温度的高热聚醚砜组合物。 聚醚砜组合物包含衍生自邻苯二甲酰亚胺双酚的结构单元，例如3,3-双（4-羟基苯基）-N-苯基邻苯二甲酰亚胺，以及衍生自至少一种联苯基 - 砜的结构单元，例如4,4'-双（（4- 氯苯基）磺酰基）-1,1'-联苯。 新型聚醚砜组合物还可以包含衍生自一种或多种双酚的结构单元，例如4,4'-联苯酚，双酚如BPA或其它亲电子砜单体如双（4-氯苯基）砜。 在一个实施方案中，本发明的聚醚砜组合物包含仅由3,3-双（4-羟基苯基）-N-苯基邻苯二甲酰亚胺衍生的结构基团和4,4'-双（（4-氯苯基）磺酰基） 1'-联苯并且表现出大于300℃的单一玻璃化转变。

    Polyetherimide compositions, methods of manufacture, and articles formed therefrom
    7.
    发明授权
    Polyetherimide compositions, methods of manufacture, and articles formed therefrom 有权
    聚醚酰亚胺组合物，制造方法和由其形成的制品

    公开(公告)号：US09127127B2

    公开(公告)日：2015-09-08

    申请号：US13649443

    申请日：2012-10-11

    申请人： Thomas Link Guggenheim ,  Roy Ray Odle ,  Farid Fouad Khouri

    发明人： Thomas Link Guggenheim ,  Roy Ray Odle ,  Farid Fouad Khouri

    IPC分类号： C08G73/10

    CPC分类号： C08G73/1021 ,  C08G73/1046 ,  C08G73/1053 ,  C08G73/1071

    摘要： A method for the manufacture of a polyetherimide composition includes catalyzing the reaction of a dianhydride and an organic diamine with a catalyst selected from guanadinium salts, pyridinium salts, imidazolium salts, tetra(C6-24)aryl ammonium salts, tetra(C7-24 arylalkylene) ammonium salts, dialkyl heterocycloaliphatic ammonium salts, bis-alkyl quaternary ammonium salts, (C7-24arylalkylene)(C1-16alkyl) phosphonium salts, (C6-24aryl)(C1-16alkyl)phosphonium salts, phosphazenium salts and combinations thereof, optionally in the presence of a solvent.

    摘要翻译： 制备聚醚酰亚胺组合物的方法包括用选自胍盐，吡啶鎓盐，咪唑鎓盐，四（C 6-24）芳基铵盐，四（C 7-24芳基亚烷基）烷基的催化剂催化二酐和有机二胺的反应 ）铵盐，二烷基杂环脂族铵盐，双烷基季铵盐，（C 7-24芳基亚烷基）（C 1-6烷基）鏻盐，（C 6-24芳基）（C 1-6烷基）鏻盐，磷氮烯基鏻盐及其组合， 溶剂的存在。