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1.发明授权Method for depositing zinc oxide at low temperatures and products formed thereby 有权低温沉积氧化锌的方法及由此形成的产品公开(公告)号：US08197914B2
公开(公告)日：2012-06-12
申请号：US11284193
申请日：2005-11-21
IPC分类号： H05H1/24
CPC分类号： C03C17/245 , C03C2217/216 , C03C2217/24 , C03C2217/241 , C03C2218/153 , C23C16/407
摘要： The present invention discloses plasma enhanced chemical vapor deposition (PECVD) process for depositing n-type and p-type zinc oxide-based transparent conducting oxides (TCOs) at low temperatures with excellent optical and electrical properties on glass and temperature sensitive materials such as plastics and polymers. Specifically, it discloses PECVD process for depositing n-type ZnO by doping it with B or F and p-type ZnO by doping it with nitrogen excellent optical and electrical properties on glass and temperature sensitive materials such as plastics and polymers for TCO application. The process utilizes a mixture of volatile zinc compound, argon and/or helium as a diluent gas, carbon dioxide as an oxidant, and a dopant or reactant to deposit the desired ZnO-based TCOs.
摘要翻译： 本发明公开了一种用于在低温下沉积n型和p型氧化锌基透明导电氧化物（TCO）的等离子体增强化学气相沉积（PECVD）工艺，在玻璃和温度敏感材料如塑料上具有优异的光学和电学性能 和聚合物。 具体地说，它公开了用于通过用B或F和p型ZnO掺杂以将氮掺杂在玻璃上的优异的光学和电学性质以及用于TCO应用的诸如塑料和聚合物的温度敏感材料来沉积n型ZnO的PECVD工艺。 该方法利用挥发性锌化合物，氩和/或氦气作为稀释气体，二氧化碳作为氧化剂和掺杂剂或反应物的混合物以沉积所需的ZnO基TCO。
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公开(公告)号：US07563308B2
公开(公告)日：2009-07-21
申请号：US11208723
申请日：2005-08-23
申请人： Daniel Joseph Tempel , Philip Bruce Henderson , Jeffrey Richard Brzozowski , Ronald Martin Pearlstein , Diwakar Garg
发明人： Daniel Joseph Tempel , Philip Bruce Henderson , Jeffrey Richard Brzozowski , Ronald Martin Pearlstein , Diwakar Garg
CPC分类号： C01B3/001 , C01B9/08 , C01B13/0285 , C01B25/06 , C01B32/80 , F17C11/00 , F17C11/005 , F17C11/007 , Y02E60/321 , Y02E60/324
摘要： A mixture and method for the storage and delivery of a gas are disclosed herein. In one aspect, there is provided a mixture comprising: an ionic liquid comprising an anion and a cation, at least a portion of the gas that is disposed within and reversibly chemically reacted with the ionic liquid, and optionally an unreacted gas. In another aspect, there is provided a method for delivering a gas from a mixture comprising an ionic liquid and one or more gases comprising: reacting at least a portion of the gas with the ionic liquid to provide the mixture comprising a chemically reacted gas and an ionic liquid and separating the chemically reacted gas from the mixture wherein the chemically reacted gas after the separating step has substantially the same chemical identity as the chemically reacted gas prior to the reacting step.
摘要翻译： 本文公开了用于储存和输送气体的混合物和方法。 在一个方面，提供了一种混合物，其包含：包含阴离子和阳离子的离子液体，所述气体的至少一部分设置在离子液体内并可逆地与离子液体化学反应，以及任选的未反应气体。 在另一方面，提供了一种从包含离子液体和一种或多种气体的混合物输送气体的方法，包括：使至少一部分气体与离子液体反应，以提供包含化学反应气体和 离子液体并且从混合物中分离化学反应的气体，其中分离步骤之后的化学反应气体在反应步骤之前具有与化学反应气体基本上相同的化学同一性。
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公开(公告)号：US08202446B2
公开(公告)日：2012-06-19
申请号：US12493751
申请日：2009-06-29
申请人： Daniel Joseph Tempel , Philip Bruce Henderson , Jeffrey Richard Brzozowski , Ronald Martin Pearlstein , Diwakar Garg
发明人： Daniel Joseph Tempel , Philip Bruce Henderson , Jeffrey Richard Brzozowski , Ronald Martin Pearlstein , Diwakar Garg
CPC分类号： C01B3/001 , C01B9/08 , C01B13/0285 , C01B25/06 , C01B32/80 , F17C11/00 , F17C11/005 , F17C11/007 , Y02E60/321 , Y02E60/324
摘要： A mixture and method for the storage and delivery of a gas are disclosed herein. In one aspect, there is provided a mixture comprising: an ionic liquid comprising an anion and a cation, at least a portion of the gas that is disposed within and reversibly chemically reacted with the ionic liquid, and optionally an unreacted gas. In another aspect, there is provided a method for delivering a gas from a mixture comprising an ionic liquid and one or more gases comprising: reacting at least a portion of the gas with the ionic liquid to provide the mixture comprising a chemically reacted gas and an ionic liquid and separating the chemically reacted gas from the mixture wherein the chemically reacted gas after the separating step has substantially the same chemical identity as the chemically reacted gas prior to the reacting step.
摘要翻译： 本文公开了用于储存和输送气体的混合物和方法。 在一个方面，提供了一种混合物，其包含：包含阴离子和阳离子的离子液体，所述气体的至少一部分设置在离子液体内并可逆地与离子液体化学反应，以及任选的未反应气体。 在另一方面，提供了一种从包含离子液体和一种或多种气体的混合物输送气体的方法，包括：使至少一部分气体与离子液体反应，以提供包含化学反应气体和 离子液体并且从混合物中分离化学反应的气体，其中分离步骤之后的化学反应气体在反应步骤之前具有与化学反应气体基本上相同的化学同一性。
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4.发明授权Contact methods for formation of Lewis gas/liquid systems and recovery of Lewis gas therefrom 有权用于形成路易斯气体/液体体系的接触方法和从其中回收路易斯气体公开(公告)号：US07736420B2
公开(公告)日：2010-06-15
申请号：US11437326
申请日：2006-05-19
申请人： Wayne Thomas McDermott , Philip Bruce Henderson , Daniel Joseph Tempel , Ronald Martin Pearlstein , James Joseph Hart , Rosaleen Patricia Morris-Oskanian , Diwakar Garg
发明人： Wayne Thomas McDermott , Philip Bruce Henderson , Daniel Joseph Tempel , Ronald Martin Pearlstein , James Joseph Hart , Rosaleen Patricia Morris-Oskanian , Diwakar Garg
IPC分类号： B01D53/14
CPC分类号： B01D53/1493 , B01D53/1456 , B01D2258/0216 , C01B7/0706 , C01B7/093 , C01B7/135 , C01B7/191 , C01B9/00 , C01B17/16 , C01B19/04 , C01C1/003 , C01C3/06 , F17C11/00
摘要： The invention relates to an improvement in apparatus and process for the formation of a complex of Lewis acidic or Lewis basic gases in a reactive liquid of opposite character and for the breaking (fragmentation) of said complex associated with the recovery of the Lewis gas therefrom. The improvement resides in forming finely divided droplets of reactive liquid and controlling the temperature, pressure and concentration of said Lewis gas of opposite character to provide for (a) the formation of said complex between said gas and reactive liquid or (b) the breaking of said complex and the recovery of the atomized droplets of reactive liquid.
摘要翻译： 本发明涉及在相反特征的反应性液体中形成路易斯酸性或路易斯碱性气体的复合物的装置和方法的改进，以及所述络合物与从其中回收的路易斯气体相关的破碎（碎裂）。 改进在于形成精细分离的反应液体的液滴并控制相反特性的所述Lewis气体的温度，压力和浓度以提供（a）在所述气体和反应性液体之间形成所述络合物，或（b） 说复合物和反应液体的雾化液滴的回收。
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公开(公告)号：US20090272938A1
公开(公告)日：2009-11-05
申请号：US12493751
申请日：2009-06-29
申请人： Daniel Joseph Tempel , Philip Bruce Henderson , Jeffrey Richard Brzozowski , Ronald Martin Pearlstein , Diwakar Garg
发明人： Daniel Joseph Tempel , Philip Bruce Henderson , Jeffrey Richard Brzozowski , Ronald Martin Pearlstein , Diwakar Garg
IPC分类号： H01J7/18
CPC分类号： C01B3/001 , C01B9/08 , C01B13/0285 , C01B25/06 , C01B32/80 , F17C11/00 , F17C11/005 , F17C11/007 , Y02E60/321 , Y02E60/324
摘要： A mixture and method for the storage and delivery of a gas are disclosed herein. In one aspect, there is provided a mixture comprising: an ionic liquid comprising an anion and a cation, at least a portion of the gas that is disposed within and reversibly chemically reacted with the ionic liquid, and optionally an unreacted gas. In another aspect, there is provided a method for delivering a gas from a mixture comprising an ionic liquid and one or more gases comprising: reacting at least a portion of the gas with the ionic liquid to provide the mixture comprising a chemically reacted gas and an ionic liquid and separating the chemically reacted gas from the mixture wherein the chemically reacted gas after the separating step has substantially the same chemical identity as the chemically reacted gas prior to the reacting step.
摘要翻译： 本文公开了用于储存和输送气体的混合物和方法。 在一个方面，提供了一种混合物，其包含：包含阴离子和阳离子的离子液体，所述气体的至少一部分设置在离子液体内并可逆地与离子液体化学反应，以及任选的未反应气体。 在另一方面，提供了一种从包含离子液体和一种或多种气体的混合物输送气体的方法，包括：使至少一部分气体与离子液体反应，以提供包含化学反应气体和 离子液体并且从混合物中分离化学反应的气体，其中分离步骤之后的化学反应气体在反应步骤之前具有与化学反应气体基本上相同的化学同一性。
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6.发明申请Contact methods for formation of Lewis gas/liquid systems and recovery of Lewis gas therefrom 有权用于形成路易斯气体/液体体系的接触方法和从其中回收路易斯气体公开(公告)号：US20070287812A1
公开(公告)日：2007-12-13
申请号：US11437326
申请日：2006-05-19
申请人： Wayne Thomas McDermott , Philip Bruce Henderson , Daniel Joseph Tempel , Ronald Martin Pearlstein , James Joseph Hart , Rosaleen Patricia Morris-Oskanian , Diwakar Garg
发明人： Wayne Thomas McDermott , Philip Bruce Henderson , Daniel Joseph Tempel , Ronald Martin Pearlstein , James Joseph Hart , Rosaleen Patricia Morris-Oskanian , Diwakar Garg
IPC分类号： C08F2/00
CPC分类号： B01D53/1493 , B01D53/1456 , B01D2258/0216 , C01B7/0706 , C01B7/093 , C01B7/135 , C01B7/191 , C01B9/00 , C01B17/16 , C01B19/04 , C01C1/003 , C01C3/06 , F17C11/00
摘要： The invention relates to an improvement in apparatus and process for the formation of a complex of Lewis acidic or Lewis basic gases in a reactive liquid of opposite character and for the breaking (fragmentation) of said complex associated with the recovery of the Lewis gas therefrom. The improvement resides in forming finely divided droplets of reactive liquid and controlling the temperature, pressure and concentration of said Lewis gas of opposite character to provide for (a) the formation of said complex between said gas and reactive liquid or (b) the breaking of said complex and the recovery of the atomized droplets of reactive liquid.
摘要翻译： 本发明涉及在相反特征的反应性液体中形成路易斯酸性或路易斯碱性气体的复合物的装置和方法的改进，以及所述络合物与从其中回收的路易斯气体相关的破碎（碎裂）。 改进在于形成精细分离的反应液体的液滴并控制相反特性的所述Lewis气体的温度，压力和浓度以提供（a）在所述气体和反应性液体之间形成所述络合物，或（b） 说复合物和反应液体的雾化液滴的回收。
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公开(公告)号：US07307772B2
公开(公告)日：2007-12-11
申请号：US11518802
申请日：2006-09-11
CPC分类号： G02F1/1523 , G02F1/153
摘要： A method of producing an electrochromic device, includes the steps of: providing a first electron conducting layer on a substrate, providing a working electrode in communication with the first electron conducting layer, providing an ion conducting layer in communication with the working electrode, providing an ion storage electrode in communication with the ion conducting layer, and providing a second electron conducting layer in communication with the ion storage electrode, wherein at least one and less than all of the providing steps include(s) plasma chemical vapor deposition. An electrochromic device produced by the method of the invention is disclosed, as is an apparatus adapted to perform the method of the invention, including plasma CVD devices and vacuum sputtering devices.
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公开(公告)号：US07106488B2
公开(公告)日：2006-09-12
申请号：US10806743
申请日：2004-03-23
CPC分类号： G02F1/1523 , G02F1/153
摘要： A method of producing an electrochromic device, includes the steps of: providing a first electron conducting layer on a substrate, providing a working electrode in communication with the first electron conducting layer, providing an ion conducting layer in communication with the working electrode, providing an ion storage electrode in communication with the ion conducting layer, and providing a second electron conducting layer in communication with the ion storage electrode, wherein at least one and less than all of the providing steps include(s) plasma chemical vapor deposition. An electrochromic device produced by the method of the invention is disclosed, as is an apparatus adapted to perform the method of the invention, including plasma CVD devices and vacuum sputtering devices.
摘要翻译： 一种制造电致变色器件的方法，包括以下步骤：在衬底上提供第一电子传导层，提供与第一电子传导层连通的工作电极，提供与工作电极连通的离子传导层， 离子存储电极与离子传导层连通，并提供与离子存储电极连通的第二电子传导层，其中至少一个并且小于所有提供步骤包括等离子体化学气相沉积。 公开了通过本发明的方法制造的电致变色装置，以及适于执行本发明方法的装置，包括等离子体CVD装置和真空溅射装置。
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9.发明申请Method for depositing zinc oxide at low temperatures and products formed thereby 有权低温沉积氧化锌的方法及由此形成的产品公开(公告)号：US20070116986A1
公开(公告)日：2007-05-24
申请号：US11284193
申请日：2005-11-21
申请人： Diwakar Garg , Philip Henderson , Daniel Tempel , Thomas Jackson , Jie Sun
发明人： Diwakar Garg , Philip Henderson , Daniel Tempel , Thomas Jackson , Jie Sun
CPC分类号： C03C17/245 , C03C2217/216 , C03C2217/24 , C03C2217/241 , C03C2218/153 , C23C16/407
摘要： The present invention discloses plasma enhanced chemical vapor deposition (PECVD) process for depositing n-type and p-type zinc oxide-based transparent conducting oxides (TCOs) at low temperatures with excellent optical and electrical properties on glass and temperature sensitive materials such as plastics and polymers. Specifically, it discloses PECVD process for depositing n-type ZnO by doping it with B or F and p-type ZnO by doping it with nitrogen excellent optical and electrical properties on glass and temperature sensitive materials such as plastics and polymers for TCO application. The process utilizes a mixture of volatile zinc compound, argon and/or helium as a diluent gas, carbon dioxide as an oxidant, and a dopant or reactant to deposit the desired ZnO-based TCOs.
摘要翻译： 本发明公开了一种用于在低温下沉积n型和p型氧化锌基透明导电氧化物（TCO）的等离子体增强化学气相沉积（PECVD）工艺，在玻璃和温度敏感材料如塑料上具有优异的光学和电学性能 和聚合物。 具体地说，它公开了用于通过用B或F和p型ZnO掺杂以将氮掺杂在玻璃上的优异的光学和电学性质以及用于TCO应用的诸如塑料和聚合物的温度敏感材料来沉积n型ZnO的PECVD工艺。 该方法利用挥发性锌化合物，氩和/或氦气作为稀释气体，二氧化碳作为氧化剂和掺杂剂或反应物的混合物以沉积所需的ZnO基TCO。
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公开(公告)号：US07824655B2
公开(公告)日：2010-11-02
申请号：US11339060
申请日：2006-01-25
CPC分类号： C01B3/38 , C01B3/46 , C01B2203/0233 , C01B2203/0425 , C01B2203/0475 , Y02P20/52
摘要： In a process for producing a hydrogen-containing gas, a hydrocarbon feed gas and steam are introduced into a reaction vessel containing a complex metal oxide and steam-hydrocarbon reforming catalyst thereby forming a combustible gas mixture comprising hydrogen. A regeneration gas comprising greater than 0.1 volume % oxygen up to and including 2 volume % oxygen is introduced into the reaction vessel to displace at least a portion of the combustible gas mixture from the reaction vessel. Subsequently, additional regeneration gases may be introduced into the reaction vessel. Numerous means for providing various regeneration gases are presented.
摘要翻译： 在制造含氢气体的方法中，将烃进料气体和蒸汽引入含有复合金属氧化物和蒸汽 - 烃重整催化剂的反应容器中，从而形成包含氢气的可燃气体混合物。 将包括大于0.1体积％氧气的再生气体引入反应容器中以将至少一部分可燃气体混合物从反应容器中置换。 随后，可以向反应容器中引入另外的再生气体。 提出了许多用于提供各种再生气体的方法。
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