摘要:
An electrolytic cell and system used for making nitrogen trifluoride consisting of a computer and an electrolytic cell having a body, an electrolyte, at least one anode chamber that produces an anode product gas, at least one cathode chamber, and one or more fluorine adjustment means to maintain fluorine or hydrogen in the anode product gas within a target amount by adjusting the concentration of fluorine in said anode product gas, and the process that controls the system.
摘要:
A process for cleaning a deposit from an interior surface of a processing chamber includes generating a plasma from a cleaning gas including SO2F2 and contacting the interior surface with the plasma for a time sufficient to convert the deposit into a volatile product, thereby cleaning the deposit from the interior surface, in which the process is conducted in the absence of SF6. The deposits, which may be removed by the process of the invention, include silicone, silicone oxide, silicone nitride, tungsten, copper and aluminum.
摘要翻译:用于从处理室的内表面清洗沉积物的方法包括从包括SO 2 F 2 N 2的清洁气体产生等离子体,并使内表面与等离子体接触 足以将沉积物转化成挥发性产物的时间,从而清除在不存在SF 6的情况下进行处理的内表面的沉积物。 可以通过本发明的方法除去的沉积物包括硅氧烷,硅氧烷,硅氮化物,钨,铜和铝。
摘要:
This invention describes an improvement in a process for purifying a nitrogen trifluoride (NF3) stream containing unreacted F2, HF, and nitrogen oxides from an NF3 reactor wherein the F2, and HF are removed and then the nitrogen oxides removed by adsorption. The improvement in the process resides in selectively removing the F2 from said NF3 stream without generating oxygen difluoride, removing HF and then removing said nitrogen oxides by adsorption. Further purification can be effected as desired.
摘要翻译:本发明描述了一种从NF 3纯化含有未反应的F 2 H 2,HF和氮氧化物的三氟化氮(NF 3 H 3)流的方法的改进, / SUB>反应器,其中除去F 2 H和HF,然后通过吸附除去氮氧化物。 该方法的改进在于从所述NF 3 N流中选择性除去F 2 O而不产生二氟化氧,除去HF,然后通过吸附除去所述氮氧化物。 可以根据需要进一步纯化。
摘要:
The invention relates to an improvement in apparatus and process for the formation of a complex of Lewis acidic or Lewis basic gases in a reactive liquid of opposite character and for the breaking (fragmentation) of said complex associated with the recovery of the Lewis gas therefrom. The improvement resides in forming finely divided droplets of reactive liquid and controlling the temperature, pressure and concentration of said Lewis gas of opposite character to provide for (a) the formation of said complex between said gas and reactive liquid or (b) the breaking of said complex and the recovery of the atomized droplets of reactive liquid.
摘要:
An economical means of safely “containing” or “packaging” commercial electrophilic fluorination agents whereby these agents are readily stored and transported in a package, typically without loss of “F+” activity, and in a form which is readily and directly useable, i.e., in solution or a slurry. Importantly, the solution/slurry medium provides a tremendous safety margin for storage and transportation since the solution medium has an enormous ability to absorb heat (due to the latent heat of vaporization of the liquid) relative to the contained active fluorination agent.
摘要:
An electrolytic cell and system used for making nitrogen trifluoride consisting of a computer and an electrolytic cell having a body, an electrolyte, at least one anode chamber that produces an anode product gas, at least one cathode chamber, and one or more fluorine adjustment means to maintain fluorine or hydrogen in the anode product gas within a target amount by adjusting the concentration of fluorine in said anode product gas, and the process that controls the system.
摘要:
The present invention is directed to improvements in storage and delivery systems that allow for rapid fill and delivery of gases reversibly stored in a nonvolatile liquid medium, improvements in delivery and purity of the delivered gas. The low pressure storage and delivery system for gas which comprises:a container having an interior portion containing a reactive Lewis basic or Lewis acidic reactive liquid medium that is reversibly reacted with a gas having opposing Lewis acidity or basicity; a system for transferring energy into or out of the reactive liquid medium; or, a product gas purifier (e.g. a gas/liquid separator); or both.
摘要:
The invention relates to an improvement in apparatus and process for the formation of a complex of Lewis acidic or Lewis basic gases in a reactive liquid of opposite character and for the breaking (fragmentation) of said complex associated with the recovery of the Lewis gas therefrom. The improvement resides in forming finely divided droplets of reactive liquid and controlling the temperature, pressure and concentration of said Lewis gas of opposite character to provide for (a) the formation of said complex between said gas and reactive liquid or (b) the breaking of said complex and the recovery of the atomized droplets of reactive liquid.