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    Metallophosphate type IM-6 crystalized solid and the preparation method thereof
    1.
    发明授权
    Metallophosphate type IM-6 crystalized solid and the preparation method thereof 有权
    金属磷酸盐型IM-6结晶固体及其制备方法

    公开(公告)号：US07033559B2

    公开(公告)日：2006-04-25

    申请号：US10508210

    申请日：2003-03-11

    申请人： Ludovic Josien ,  Angélique Simon-Masseron ,  Volker Gramlich ,  Joël Patarin ,  Loïc Rouleau

    发明人： Ludovic Josien ,  Angélique Simon-Masseron ,  Volker Gramlich ,  Joël Patarin ,  Loïc Rouleau

    IPC分类号： C01B39/54

    CPC分类号： C01B37/002 ,  C01P2002/72 ,  Y10S423/30

    摘要： The invention relates to a metallophosphate-type crystallized solid, referred to by the name IM-6, which exhibits an X-ray diffraction diagram as given below. This metallophosphate-type solid can be partially substituted by an element X and optionally by an element Y. Said metallophosphate exhibits a chemical composition, expressed on an anhydrous base, defined by the formula RS,(GgPpXxYy)O2, where G represents one or more trivalent element(s), R represents one or more organic compound(s), X represents one or more divalent element(s), Y represents one or more tetravalent element(s), and in which s≦0.2, g≦0.5, p≦0.5, x≦0.4, y≦0.3, with g+p+x+y=1.

    摘要翻译： 本发明涉及名称为IM-6的金属磷酸盐型结晶固体，其表现出如下所示的X射线衍射图。 该金属磷酸盐型固体可以部分地被元素X和任选地被元素Y取代。所述金属磷酸盐表现出由无水碱表示的化学组成，由式R 3定义（G < 其中G表示一个或者两个或者两个或多个，其中G表示一个或者两个， 更多的三价元素，R表示一种或多种有机化合物，X表示一种或多种二价元素，Y表示一种或多种四价元素，其中s <= 0.2， = 0.5，p <= 0.5，x <= 0.4，y <= 0.3，其中g + p + x + y = 1。

    Crystallized IM-8 solid of metallophosphate type and process for the preparation thereof
    2.
    发明授权
    Crystallized IM-8 solid of metallophosphate type and process for the preparation thereof 有权
    结晶的金属磷酸盐型IM-8固体及其制备方法

    公开(公告)号：US06998101B2

    公开(公告)日：2006-02-14

    申请号：US10831128

    申请日：2004-04-26

    申请人： Ludovic Josien ,  Angélique Simon-Masseron ,  Joël Patarin ,  Loïc Rouleau

    发明人： Ludovic Josien ,  Angélique Simon-Masseron ,  Joël Patarin ,  Loïc Rouleau

    IPC分类号： C01B37/00

    CPC分类号： C01B37/002 ,  Y10S423/30

    摘要： A crystallized solid of metallophosphate type, referred to by the designation IM-8 can be partially substituted by an element X and optionally by an element Y. The metallophosphate is of a chemical composition, expressed on an anhydrous basis is defined by the formula Rs(GgPpXxYy)O2 in which G represents one or more trivalent elements, R represents one or more organic compounds, X represents one or more divalent elements, and Y represents one or more tetravalent elements, and in which s≦0.2, g≦0.5, p≦0.5, x≦0.4 and y≦0.3 with g+p+x+y=1. The crystallized solid is useful as an adsorbent.

    摘要翻译： 由名称为IM-8的金属磷酸盐结晶的固体可以被元素X和任选的元素Y部分地取代。金属磷酸盐是以无水为基础的化学组成，由式R' （G）p x x 其中G表示一个或多个三价元素，R表示一种或多种有机化合物，X表示一种或多种二价元素，Y表示一种或多种四价元素，其中s <= 0.2，g < 0.5，p <= 0.5，x <= 0.4，y <= 0.3，其中g + p + x + y = 1。 结晶的固体可用作吸附剂。

    Process for preparing EU-1 zeolite
    3.
    发明授权
    Process for preparing EU-1 zeolite 有权
    制备EU-1沸石的方法

    公开(公告)号：US08557220B2

    公开(公告)日：2013-10-15

    申请号：US12601199

    申请日：2008-04-14

    申请人： Simone Goergen ,  Loïc Rouleau ,  Joël Patarin

    发明人： Simone Goergen ,  Loïc Rouleau ,  Joël Patarin

    IPC分类号： C01B33/36 ,  C01B39/36 ,  C01B39/00 ,  C01F7/00

    CPC分类号： C01B39/48 ,  B01J29/7023

    摘要： The invention concerns a process for preparing an EU-1 zeolite having a XO2/Y2O3 ratio in the range 10 to 100, comprising the following steps: a) mixing, in an aqueous medium, at least one source of at least one oxide XO2, X being selected from silicon and/or germanium, at least one source of at least one oxide Y2O3, Y being selected from aluminium, iron, gallium and boron, and at least one organic template Q; b) drying the reaction mixture derived from step a) at a temperature of less than 200° C.; c) hydrothermal treatment of the dried reaction mixture derived from step b) in an autoclave, said dried reaction mixture not being in contact with a liquid phase at the bottom of the autoclave.

    摘要翻译： 本发明涉及一种制备XO2 / Y2O3比例在10至100范围内的EU-1沸石的方法，包括以下步骤：a）在水性介质中混合至少一种氧化物XO 2的源， X选自硅和/或锗，至少一种氧化物Y 2 O 3，Y选自铝，铁，镓和硼的至少一种源和至少一种有机模板Q; b）在低于200℃的温度下干燥衍生自步骤a）的反应混合物; c）在高压釜中对来自步骤b）的干燥反应混合物进行水热处理，所述干燥的反应混合物不与高压釜底部的液相接触。

    NOVEL PROCESS FOR PREPARING EU-1 ZEOLITE
    4.
    发明申请
    NOVEL PROCESS FOR PREPARING EU-1 ZEOLITE 有权
    制备EU-1沸石的新工艺

    公开(公告)号：US20100178241A1

    公开(公告)日：2010-07-15

    申请号：US12601199

    申请日：2008-04-14

    申请人： Simone Goergen ,  Loïc Rouleau ,  Joël Patarin

    发明人： Simone Goergen ,  Loïc Rouleau ,  Joël Patarin

    IPC分类号： C01B39/02

    CPC分类号： C01B39/48 ,  B01J29/7023

    摘要： The invention concerns a process for preparing an EU-1 zeolite having a XO2/Y2O3 ratio in the range 10 to 100, comprising the following steps: a) mixing, in an aqueous medium, at least one source of at least one oxide XO2, X being selected from silicon and/or germanium, at least one source of at least one oxide Y2O3, Y being selected from aluminium, iron, gallium and boron, and at least one organic template Q; b) drying the reaction mixture derived from step a) at a temperature of less than 200° C.; c) hydrothermal treatment of the dried reaction mixture derived from step b) in an autoclave, said dried reaction mixture not being in contact with a liquid phase at the bottom of the autoclave.

    摘要翻译： 本发明涉及一种制备XO2 / Y2O3比例在10至100范围内的EU-1沸石的方法，包括以下步骤：a）在水性介质中混合至少一种氧化物XO 2的源， X选自硅和/或锗，至少一种氧化物Y 2 O 3，Y选自铝，铁，镓和硼的至少一种源和至少一种有机模板Q; b）在低于200℃的温度下干燥衍生自步骤a）的反应混合物; c）在高压釜中对来自步骤b）的干燥反应混合物进行水热处理，所述干燥的反应混合物不与高压釜底部的液相接触。

    Process for preparation of an EUO-structural-type zeolite, the zeolite that is obtained and its use as catalyst for isomerization of C8-aromatic compounds
    7.
    发明授权
    Process for preparation of an EUO-structural-type zeolite, the zeolite that is obtained and its use as catalyst for isomerization of C8-aromatic compounds 有权
    制备EUO结构型沸石的方法，所获得的沸石及其作为C8-芳族化合物异构化催化剂的用途

    公开(公告)号：US06616910B2

    公开(公告)日：2003-09-09

    申请号：US09849483

    申请日：2001-05-07

    申请人： Loïc Rouleau ,  Frédéric Kolenda ,  Elisabeth Merlen ,  Fabio Alario

    发明人： Loïc Rouleau ,  Frédéric Kolenda ,  Elisabeth Merlen ,  Fabio Alario

    IPC分类号： C01B3904

    CPC分类号： B01J29/7023 ,  B01J29/7446 ,  C01B39/06 ,  C01B39/48

    摘要： This invention relates to a process for synthesis of an EUO-structural-type zeolite that comprises at least one element X that is selected from among silicon and germanium and at least one element T that is selected from among aluminum, iron, gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese, whereby said process is carried out in the presence of an organic structuring agent that is derived from dibenzyldimethylammonium (DBDMA) or its precursors and in the presence of nuclei of at least one zeolitic material of the same structure as the zeolite that is to be synthesized. The zeolite that is thus obtained has an X/T ratio of between 5 and 50. It is used in particular as a catalyst, for example in a process for isomerization of aromatic compounds with 8 carbon atoms per molecule.

    摘要翻译： 本发明涉及一种合成EUO结构型沸石的方法，该方法包括选自硅和锗中的至少一种元素X和至少一种元素T，其选自铝，铁，镓，硼， 钛，钒，锆，钼，砷，锑，铬和锰，由此所述方法在衍生自二苄基二甲基铵（DBDMA）或其前体的有机结构剂存在下，并且在至少存在核的存在下进行 一种沸石材料与待合成的沸石具有相同的结构。 由此获得的沸石的X / T比为5〜50。特别是作为催化剂使用，例如在每分子具有8个碳原子的芳族化合物异构化的方法中。

    Process for preparing a zeolite with structure type MTT using specific template precursors
    8.
    发明授权
    Process for preparing a zeolite with structure type MTT using specific template precursors 有权
    使用特定模板前体制备具有MTT结构类型的沸石的方法

    公开(公告)号：US06548040B1

    公开(公告)日：2003-04-15

    申请号：US09672053

    申请日：2000-09-29

    申请人： Loïc Rouleau ,  Frédéric Kolenda ,  Eric Benazzi

    发明人： Loïc Rouleau ,  Frédéric Kolenda ,  Eric Benazzi

    IPC分类号： C01B3948

    CPC分类号： B01J20/18 ,  B01J29/04 ,  C01B39/48 ,  C10G45/64 ,  Y10S423/36

    摘要： The present invention concerns a process for synthesising a zeolite with structure type MTT comprising at least one element X selected from silicon and germanium and at least one element T selected from aluminium, iron gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese, comprising reacting an aqueous mixture comprising at least one source of at least one element X, at least one source of at least one element T, and at least one precursor of an organic compound comprising at least one alkylated polymethylene &agr;-&ohgr; diammonium derivative, characterized in that at least one precursor is selected from monoamines. The present invention also concerns the use of the zeolite obtained as a catalyst in a process for converting hydrocarbon-containing feeds, as an adsorbent to control pollution and as a molecular sieve for separation.

    摘要翻译： 本发明涉及合成具有结构类型MTT的沸石的方法，该方法包括至少一种选自硅和锗的元素X和至少一种选自铝，铁镓，硼，钛，钒，锆，钼，砷， 锑，铬和锰，包括使包含至少一种元素X的至少一种源，至少一种元素T的至少一种源的至少一种含有至少一种烷基化聚亚甲基α - 大豆二铵衍生物，其特征在于至少一种前体选自单胺。 本发明还涉及在用于转化含烃原料作为吸附剂以控制污染和分离分子筛的方法中作为催化剂获得的沸石的用途。