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    Isothiazolylazo dyes having aminophenyl and aminonaphthyl components
    3.
    发明授权
    Isothiazolylazo dyes having aminophenyl and aminonaphthyl components 失效
    具有氨基苯基氨基萘基组分的异噻唑基偶氮染料

    公开(公告)号：US4764600A

    公开(公告)日：1988-08-16

    申请号：US460793

    申请日：1983-01-25

    申请人： Udo Bergmann ,  Johannes P. Dix ,  Guenter Hansen ,  Ernst Schefczik ,  Guenther Seybold

    发明人： Udo Bergmann ,  Johannes P. Dix ,  Guenter Hansen ,  Ernst Schefczik ,  Guenther Seybold

    IPC分类号： C09B29/039 ,  C09B29/00 ,  C09B29/06 ,  C09B29/08 ,  C09B29/095 ,  C09B29/042 ,  C09B29/09 ,  D06P1/18 ,  D06P3/54

    CPC分类号： C09B29/0847 ,  C09B29/0081 ,  C09B29/06 ,  C09B29/0813 ,  C09B29/083 ,  C09B29/095 ,  Y10S534/02

    摘要： An isothiazolylazo dye of the formula I ##STR1## wherein R is an alkyl group or unsubstituted aryl or substituted aryl group selected from the group consisting of ##STR2## and K is a radical of the formula ##STR3## where B is C.sub.1 -C.sub.4 alkyl or a substituted amino radical selected from the group consisting of ##STR4## R.sup.1 is hydrogen, methyl, methoxy or ethoxy, R.sup.2 and R.sup.3 independently of one another are each unsubstituted C.sub.1 -C.sub.4 alkyl or substituted alkyl groups selected from the group of C.sub.1 -C.sub.4 alkyls which are substituted by chlorine, bromine, cyano, hydroxyl, C.sub.1 -C.sub.4 -alkoxy, benzyloxy, phenoxy, phenyl, C.sub.1 -C.sub.4 -alkylcarbonyloxy which is unsubstituted or substituted by C.sub.1 -C.sub.4 -alkoxy, phenoxy or phenyl, phenycarbonyloxy which is unsubstituted or substituted by chlorine, bromine, methoxy, ethoxy, methyl or ethyl, oxycarbonyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, C.sub.1 -C.sub.4 -alkoxycarbonyloxy, carbamyl, phenalkyloxycarbonyloxy, phenoxyalkyloxycarbonyloxy, C.sub.1 -C.sub.4 -alkoxyalkoxycarbonyloxy, phenylaminocarbonyloxy which is unsubstituted or substituted by chlorine, methoxy or methyl, C.sub.1 -C.sub.4 -alkoxyalkoxycarbonyl, phenylalkyloxycarbonyl or C.sub.1 -C.sub.4 -alkylaminocarbonyloxy which is unsubstituted or substituted by C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, chlorine or bromine; or R.sup.3 is hydrogen, R.sup.4 is a radical of the formula --A--OCO--Y--R, Z is hydrogen or methyl, X is hydrogen, methyl, methoxy, chlorine or an acylamino radical selected from the group consisting of A is C.sub.2 - or C.sub.3 -alkylene and Y is --O-- or --NH--. The dyes are very useful for dyeing cellulose esters and synthetic polyesters; the dyeings obtained are from yellow to blue, and very fast.

    摘要翻译： 式I的异噻唑基偶氮染料其中R为烷基或未取代的芳基或取代的芳基，所述芳基选自由下列组成的组：K IMAGE> TR＆lt; IMAGE＆gt;和K是式 > + TR 其中B是C1-C4烷基或选自由下列组成的组的取代的氨基：R 1是氢，甲基，甲氧基或乙氧基，R 2和R 3彼此独立地各自是未取代的 C 1 -C 4烷基或取代的烷基，其选自被氯，溴，氰基，羟基，C 1 -C 4 - 烷氧基，苄氧基，苯氧基，苯基，未被取代的C 1 -C 4 - 烷基羰基氧基取代的C 1 -C 4烷基 被C 1 -C 4 - 烷氧基，苯氧基或苯基取代，未被取代或被氯，溴，甲氧基，乙氧基，甲基或乙基，氧羰基，C 1 -C 4 - 烷氧基羰基，C 1 -C 4烷氧基羰基氧基，氨基甲酰基，苯氧基羰基氧基，苯氧基羰基氧基 ，C 1 -C 4 - 烷氧基烷氧基羰基氧基 未取代或被氯，甲氧基或甲基取代的苯氨基羰基氧基，未被取代或被C 1 -C 4 - 烷氧基，氯或溴取代的C 1 -C 4 - 烷氧基烷氧基羰基，苯基烷氧基羰基或C 1 -C 4烷基氨基羰氧基; 或R 3是氢，R 4是式-A-OCO-YR的基团，Z是氢或甲基，X是氢，甲基，甲氧基，氯或选自NHCHO，NHCOCH 3，NHCOC 2 H 5， NHCO芳基，NHCOCH2芳基，A是C2-或C3-亚烷基，Y是-O-或-NH-。 染料对染色纤维素酯和合成聚酯是非常有用的; 得到的染色从黄色到蓝色，非常快。

    Thiazole derivatives
    4.
    发明授权
    Thiazole derivatives 失效
    噻唑衍生物

    公开(公告)号：US4239894A

    公开(公告)日：1980-12-16

    申请号：US920638

    申请日：1978-06-29

    申请人： Guenther Seybold ,  Heinz Eilingsfeld

    发明人： Guenther Seybold ,  Heinz Eilingsfeld

    IPC分类号： C07D277/20 ,  C07D277/40

    CPC分类号： C07D277/20

    摘要： An organic compound of the general formula ##STR1## where R.sup.1 and R.sup.2 are cyano, formyl, substituted or unsubstituted alkanoyl or aroyl, a carboxylic acid ester group, substituted or unsubstituted carbamoyl or sulfamoyl, alkylsulfonyl, arylsulfonyl or alkylsulfinyl, orR.sup.1 and R.sup.2 together may be a cyclic radical,R.sup.2 may also be alkyl, aryl or hetaryl,R.sup.3 is hydrogen, substituted or unsubstituted alkyl, aryl or hetaryl,X is CH, CR.sup.5 or N,R.sup.4 is a radical of the formula ##STR2## R.sup.5 to R.sup.10 are substituents conventionally present in dyes. The compounds may be used as dyes for synthetic and natural fibers and give very fast dyeings.

    摘要翻译： 其中R 1和R 2为氰基，甲酰基，取代或未取代的烷酰基或芳酰基，羧酸酯基，取代或未取代的氨基甲酰基或氨磺酰基，烷基磺酰基，芳基磺酰基或烷基亚磺酰基，或R 1和R 2在一起的有机化合物 可以是环状基团，R 2也可以是烷基，芳基或杂芳基，R 3是氢，取代或未取代的烷基，芳基或杂芳基，X是CH，CR 5或N，R 4是下式的基团： R5至R10是染料中通常存在的取代基。 这些化合物可以用作合成和天然纤维的染料，并给出非常快的染色。

    Preparation of N,N-disubstituted 2-aminothiazoles
    6.
    发明授权
    Preparation of N,N-disubstituted 2-aminothiazoles 失效
    N，N-二取代的2-氨基噻唑的制备

    公开(公告)号：US4560751A

    公开(公告)日：1985-12-24

    申请号：US509428

    申请日：1983-06-30

    申请人： Guenther Seybold

    发明人： Guenther Seybold

    IPC分类号： C07D277/20 ,  C07D277/42 ,  C07D417/04 ,  C07D417/06

    CPC分类号： C07D417/04 ,  C07D277/42 ,  C07D417/06

    摘要： Compounds of the general formula I ##STR1## where R is unsubstituted or substituted alkyl, alkenyl, aryl or hetaryl and R.sup.1 and R.sup.2 independently of one another are each unsubstituted or substituted alkyl or aryl, or, together with the nitrogen, form a heterocyclic ring, are prepared by a process wherein a compound of the general formula II ##STR2## is reacted with a water-soluble monohaloacetate in an aqueous alkaline medium. They are very useful coupling components for the preparation of azo dyes.

    摘要翻译： 其中R是未取代或取代的烷基，链烯基，芳基或杂芳基和R 1和R 2彼此独立的通式I的化合物是未取代或取代的烷基或芳基，或者与氮一起形成杂环 环通过其中通式II II的化合物与水溶性单卤代乙酸酯在碱性水溶液中反应的方法制备。 它们是用于制备偶氮染料的非常有用的偶联组分。

    Monoazo dyes of the thiazole series having a heterocyclic substituent in the 4-position
    7.
    发明授权
    Monoazo dyes of the thiazole series having a heterocyclic substituent in the 4-position 失效
    在4位具有杂环取代基的噻唑系单偶氮染料

    公开(公告)号：US4340537A

    公开(公告)日：1982-07-20

    申请号：US124740

    申请日：1980-02-26

    申请人： Heinz Eilingsfeld ,  Guenter Hansen ,  Guenther Seybold

    发明人： Heinz Eilingsfeld ,  Guenter Hansen ,  Guenther Seybold

    IPC分类号： C09B29/36 ,  C07C107/04

    CPC分类号： C09B29/3691

    摘要： Dyes of the thiazole series, having the general formula I ##STR1## where D is the radical of an aromatic diazo component,R is a heterocyclic radical andR.sup.1 and R.sup.2 are hydrogen or unsubstituted or substituted hydrocarbon radicals, which may also together form a ring, which may or may not be heterocyclic.The dyes according to the invention are particularly suitable for dyeing synthetic polyesters.

    摘要翻译： 噻唑系的染料具有通式I I，其中D是芳族重氮组分的基团，R是杂环基团，R 1和R 2是氢或未取代或取代的烃基，其也可以一起形成 环，其可以是也可以不是杂环的。 根据本发明的染料特别适用于染色合成聚酯。

    Process for the production of 4,5-disubstituted thiazoles
    8.
    发明授权
    Process for the production of 4,5-disubstituted thiazoles 失效
    制备4,5-二取代噻唑的方法

    公开(公告)号：US4153607A

    公开(公告)日：1979-05-08

    申请号：US880883

    申请日：1978-02-24

    申请人： Heinz Eilingsfeld ,  Guenther Seybold

    发明人： Heinz Eilingsfeld ,  Guenther Seybold

    IPC分类号： C07D277/20 ,  C07D277/40 ,  C07D277/48 ,  C07D277/56 ,  C07D513/04 ,  C09B29/042 ,  C07D417/02

    CPC分类号： C07D513/04 ,  C07D277/56

    摘要： 4,5-Disubstituted thiazoles are manufactured by reacting 4-amino-5-cyano-thiazoles with hydrogen sulfide in the presence of basic compounds, followed by dehydrogenating cyclization. The new 3-amino-thiazolo-(4,5-c)-isothiazoles I, 4-amino-5-thiocarbamidothiazoles III and 4,5-disubstituted thiazoles IV obtainable by the process of the invention are valuable intermediates for the manufacture of azo dyes and of crop protection agents.

    摘要翻译： 通过在碱性化合物的存在下使4-氨基-5-氰基 - 噻唑与硫化氢反应，然后脱氢环化来制备4,5-二取代的噻唑。 通过本发明方法获得的新的3-氨基 - 噻唑并（4,5-c） - 异噻唑I，4-氨基-5-硫代氨基甲酰基噻唑III和4,5-二取代噻唑IV是制备偶氮的有价值的中间体 染料和作物保护剂。