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    Isothiazolylazo dyes having aminophenyl and aminonaphthyl components
    1.
    发明授权
    Isothiazolylazo dyes having aminophenyl and aminonaphthyl components 失效
    具有氨基苯基氨基萘基组分的异噻唑基偶氮染料

    公开(公告)号：US4764600A

    公开(公告)日：1988-08-16

    申请号：US460793

    申请日：1983-01-25

    申请人： Udo Bergmann ,  Johannes P. Dix ,  Guenter Hansen ,  Ernst Schefczik ,  Guenther Seybold

    发明人： Udo Bergmann ,  Johannes P. Dix ,  Guenter Hansen ,  Ernst Schefczik ,  Guenther Seybold

    IPC分类号： C09B29/039 ,  C09B29/00 ,  C09B29/06 ,  C09B29/08 ,  C09B29/095 ,  C09B29/042 ,  C09B29/09 ,  D06P1/18 ,  D06P3/54

    CPC分类号： C09B29/0847 ,  C09B29/0081 ,  C09B29/06 ,  C09B29/0813 ,  C09B29/083 ,  C09B29/095 ,  Y10S534/02

    摘要： An isothiazolylazo dye of the formula I ##STR1## wherein R is an alkyl group or unsubstituted aryl or substituted aryl group selected from the group consisting of ##STR2## and K is a radical of the formula ##STR3## where B is C.sub.1 -C.sub.4 alkyl or a substituted amino radical selected from the group consisting of ##STR4## R.sup.1 is hydrogen, methyl, methoxy or ethoxy, R.sup.2 and R.sup.3 independently of one another are each unsubstituted C.sub.1 -C.sub.4 alkyl or substituted alkyl groups selected from the group of C.sub.1 -C.sub.4 alkyls which are substituted by chlorine, bromine, cyano, hydroxyl, C.sub.1 -C.sub.4 -alkoxy, benzyloxy, phenoxy, phenyl, C.sub.1 -C.sub.4 -alkylcarbonyloxy which is unsubstituted or substituted by C.sub.1 -C.sub.4 -alkoxy, phenoxy or phenyl, phenycarbonyloxy which is unsubstituted or substituted by chlorine, bromine, methoxy, ethoxy, methyl or ethyl, oxycarbonyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, C.sub.1 -C.sub.4 -alkoxycarbonyloxy, carbamyl, phenalkyloxycarbonyloxy, phenoxyalkyloxycarbonyloxy, C.sub.1 -C.sub.4 -alkoxyalkoxycarbonyloxy, phenylaminocarbonyloxy which is unsubstituted or substituted by chlorine, methoxy or methyl, C.sub.1 -C.sub.4 -alkoxyalkoxycarbonyl, phenylalkyloxycarbonyl or C.sub.1 -C.sub.4 -alkylaminocarbonyloxy which is unsubstituted or substituted by C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, chlorine or bromine; or R.sup.3 is hydrogen, R.sup.4 is a radical of the formula --A--OCO--Y--R, Z is hydrogen or methyl, X is hydrogen, methyl, methoxy, chlorine or an acylamino radical selected from the group consisting of A is C.sub.2 - or C.sub.3 -alkylene and Y is --O-- or --NH--. The dyes are very useful for dyeing cellulose esters and synthetic polyesters; the dyeings obtained are from yellow to blue, and very fast.

    摘要翻译： 式I的异噻唑基偶氮染料其中R为烷基或未取代的芳基或取代的芳基，所述芳基选自由下列组成的组：K IMAGE> TR＆lt; IMAGE＆gt;和K是式 > + TR 其中B是C1-C4烷基或选自由下列组成的组的取代的氨基：R 1是氢，甲基，甲氧基或乙氧基，R 2和R 3彼此独立地各自是未取代的 C 1 -C 4烷基或取代的烷基，其选自被氯，溴，氰基，羟基，C 1 -C 4 - 烷氧基，苄氧基，苯氧基，苯基，未被取代的C 1 -C 4 - 烷基羰基氧基取代的C 1 -C 4烷基 被C 1 -C 4 - 烷氧基，苯氧基或苯基取代，未被取代或被氯，溴，甲氧基，乙氧基，甲基或乙基，氧羰基，C 1 -C 4 - 烷氧基羰基，C 1 -C 4烷氧基羰基氧基，氨基甲酰基，苯氧基羰基氧基，苯氧基羰基氧基 ，C 1 -C 4 - 烷氧基烷氧基羰基氧基 未取代或被氯，甲氧基或甲基取代的苯氨基羰基氧基，未被取代或被C 1 -C 4 - 烷氧基，氯或溴取代的C 1 -C 4 - 烷氧基烷氧基羰基，苯基烷氧基羰基或C 1 -C 4烷基氨基羰氧基; 或R 3是氢，R 4是式-A-OCO-YR的基团，Z是氢或甲基，X是氢，甲基，甲氧基，氯或选自NHCHO，NHCOCH 3，NHCOC 2 H 5， NHCO芳基，NHCOCH2芳基，A是C2-或C3-亚烷基，Y是-O-或-NH-。 染料对染色纤维素酯和合成聚酯是非常有用的; 得到的染色从黄色到蓝色，非常快。

    3-(.beta.-aminoethyl)-4-cyano-isothiazolylazo dyes
    3.
    发明授权
    3-(.beta.-aminoethyl)-4-cyano-isothiazolylazo dyes 失效
    3-（β-氨基乙基）-4-氰基 - 异噻唑偶氮染料

    公开(公告)号：US4619992A

    公开(公告)日：1986-10-28

    申请号：US710993

    申请日：1985-03-12

    申请人： Udo Bergmann ,  Johannes P. Dix ,  Guenter Hansen ,  Ernst Schefczik

    发明人： Udo Bergmann ,  Johannes P. Dix ,  Guenter Hansen ,  Ernst Schefczik

    IPC分类号： C09B29/042 ,  C09B29/00 ,  C09B29/36 ,  C09B29/039 ,  D06P1/18 ,  D06P3/54

    CPC分类号： C09B29/0081

    摘要： A compound of the formula: ##STR1## where R is hydrogen, C.sub.1 -C.sub.4 -alkyl, phenyl, chlorophenyl, methylphenyl, methoxyphenyl or nitrophenyl; R.sup.1 is allyl, C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -alkyl substituted by C.sub.1 -C.sub.8 -alkoxy, phenoxy, phenyl or C.sub.1 -C.sub.8 -alkanoyloxy, cyclopentyl, cyclohexyl, methylcyclohexyl, norbornyl, phenyl or phenyl substituted by chlorine, methyl or alkoxy; R.sup.2 is C.sub.1 -C.sub.10 -alkanoyl, C.sub.1 -C.sub.10 -alkanoyl substituted by alkoxy or phenoxy, cyclohexanoyl, benzoyl, benzoyl substituted by chlorine, methyl or methoxy, C.sub.1 -C.sub.8 -alkoxycarbonyl, aminocarbonyl, phenylaminocarbonyl, CH.sub.3 NHCO, C.sub.2 H.sub.5 NHCO, C.sub.3 H.sub.7 NHCO, C.sub.4 H.sub.9 NHCO, (CH.sub.3).sub.2 NCO, CH.sub.3 SO.sub.2, C.sub.6 H.sub.5 SO.sub.2 or p--CH.sub.3 --C.sub.6 H.sub.4 --SO.sub.2 ; or R.sup.1 and R.sup.2, together with the nitrogen atom, form a ring system, and K is a radical of a coupling component. The isothiazolylylazo compound of the invention is useful for the dyeing of the polyesters, nylon, and cellulose esters.

    摘要翻译： 其中R是氢，C 1 -C 4 - 烷基，苯基，氯苯基，甲基苯基，甲氧基苯基或硝基苯基的下式的化合物： R1是烯丙基，C1-C8-烷基，被C1-C8-烷氧基，苯氧基，苯基或C1-C8-烷酰氧基取代的C1-C8-烷基，环戊基，环己基，甲基环己基，降冰片基，苯基或被氯，甲基或 烷氧基 R2是C1-C10烷酰基，被烷氧基或苯氧基取代的C1-C10烷酰基，环己酰基，苯甲酰基，被氯，甲基或甲氧基取代的苯甲酰基，C1-C8-烷氧基羰基，氨基羰基，苯基氨基羰基，CH3NHCO，C2H5NHCO，C3H7NHCO，C4H9NHCO， （CH3）2NCO，CH3SO2，C6H5SO2或对-CH3-C6H4-SO2; 或R 1和R 2与氮原子一起形成环系，K是偶合组分的基团。 本发明的异噻唑立噻唑化合物可用于聚酯，尼龙和纤维素酯的染色。

    Preparation of concentrated solutions of cationic dyes as mono-carboxylates in glycol ether
    5.
    发明授权
    Preparation of concentrated solutions of cationic dyes as mono-carboxylates in glycol ether 失效
    在乙二醇醚中制备阳离子染料作为单羧酸盐的浓缩溶液

    公开(公告)号：US4976744A

    公开(公告)日：1990-12-11

    申请号：US406244

    申请日：1989-09-12

    申请人： Johannes P. Dix ,  Guenter Hansen ,  Hellmut Kast

    发明人： Johannes P. Dix ,  Guenter Hansen ,  Hellmut Kast

    IPC分类号： C09B67/32

    CPC分类号： C09B67/0075 ,  Y10S8/927

    摘要： Concentrated solutions of cationic dyes are prepared by treating the cationic dyes, which contain as the counterions the anions customarily present during their preparation, with alkali metal salts of monocarboxylic acids and with or without complexing agents in an aqueous glycol ether medium, and separating off the organic phase, which contains the dyes in the form of their monocarboxylic acid salts.

    摘要翻译： 阳离子染料的浓缩溶液通过在阳离子染料中处理阳离子染料，所述阳离子染料在其制备过程中通常含有阴离子与阴离子一起含有一元羧酸的碱金属盐，并且在含水二醇醚介质中含有或不与络合剂反应， 有机相，其含有其一元羧酸盐形式的染料。