CELLULOSE ACETATE, AND METHOD AND DEVICE FOR PRODUCING CELLULOSE ACETATE

    公开(公告)号:US20210017296A1

    公开(公告)日:2021-01-21

    申请号:US17060649

    申请日:2020-10-01

    IPC分类号: C08B3/06

    摘要: An object is to provide a cellulose acetate remarkably good in hue even when a low-quality pulp is used.
    A method for producing the cellulose acetate includes a step (1) of crushing a wood pulp, a step (2) of bringing the crushed wood pulp into contact with acetic acid to subject the pulp to pretreat the wood pulp, a step (3) of causing the wood pulp to react with acetic anhydride after the pretreatment to acetylate the pulp, a step (4) of hydrolyzing the cellulose acetate, which is yielded by the acetylation, and a step (5) of precipitating the cellulose acetate, an acetylation degree of which is adjusted by the hydrolysis. In the hydrolyzing step (4), in a hydrolysis reaction system, a concentration of oxygen is set to 3% or less.

    Preparation of modified cellulose and its derivatives

    公开(公告)号:US10813377B2

    公开(公告)日:2020-10-27

    申请号:US15771829

    申请日:2016-10-28

    发明人: Wiechang Jin

    摘要: This invention discloses methods for producing modified cellulose, modified nanocellulose, modified nanocellulose functionalized with other functional species, and derivatives thereof. The present invention also provides cellulose, nanocellulose, and their derivatives that are safe to use inside an animal or human body and are biocompatible without costly purification. These cellulose or nanocellulose materials can be used in many different applications, including carrier for pharmaceutical active agents and other medical devices.

    Method of making silver-containing dispersions

    公开(公告)号:US10444618B2

    公开(公告)日:2019-10-15

    申请号:US15713777

    申请日:2017-09-25

    摘要: A method is used to prepare silver nanoparticles in the form of a silver nanoparticle cellulosic polymeric composite. A cellulosic polymer, organic solvent having a boiling point at atmospheric pressure of 100° C. to 500° C. and a Hansen parameter (δTPolymer) equal to or greater than that of the cellulosic polymer, and a nitrogenous base are mixed to form a premix solution. Upon heating the premix solution to a temperature of at least 75° C., a solution of reducible silver ions is added that is equimolar or less in relation to the nitrogenous base. The weight ratio of reducible silver ions to the cellulosic polymer is 5:1 to 50:1. The resulting silver nanoparticle composite is cooled, isolated, and re-dispersed in an organic solvent, providing a non-aqueous silver-containing dispersion comprising the silver nanoparticle cellulosic polymeric composite.

    METHODS FOR PRODUCING A MANURE-DERIVED BIOPLASTIC AND BIOPRODUCTS

    公开(公告)号:US20190276562A1

    公开(公告)日:2019-09-12

    申请号:US16302924

    申请日:2017-05-17

    申请人: Jalila ESSAIDI

    发明人: Jalila ESSAIDI

    IPC分类号: C08B3/06 C08B16/00

    摘要: The invention relates to the separation of manure in fractions and the treatment of said fractions in order to retrieve useful components to produce manure-derived bioplastic and other manure-derived bioproducts. The invention further relates to a method for producing composite (bio)plastic, and to a method for producing fibre from regenerated manure-derived cellulose. The methods include the steps of: flocculation treatment and a filtration treatment; pulping the manure-derived solid fractions; acetylation of the manure-derived dissolving-grade cellulose pulp with acetic anhydride and a catalyst; extracting fermentable components from the different fractions of the manure to produce monocarboxylic acids for use in the monocarboxylic acid carrier solution. Furthermore methods are disclosed for forming composite bioplastics with resin binding agents; and for spinning yarn from cellulose pulp.