Phthalocyanine compounds, process for production thereof and electrophotographic photosensitive member using the compounds
    111.
    发明授权
    Phthalocyanine compounds, process for production thereof and electrophotographic photosensitive member using the compounds 有权
    酞菁化合物,其制备方法和使用该化合物的电子照相感光构件

    公开(公告)号:US06245472B1

    公开(公告)日:2001-06-12

    申请号:US09150836

    申请日:1998-09-10

    申请人: Masato Tanaka

    发明人: Masato Tanaka

    IPC分类号: G03G506

    摘要: Iodogallium phthalocyanine and bromogallium phthalocyanine having novel crystalline forms characterized by X-ray diffraction patterns according to CuK&agr; characteristic X-ray diffraction method and exhibiting excellent zirconium phthalocyanine can be obtained through appropriate selection of a reaction solvent, followed by milling or stirring in an appropriate solvent. For example, &agr;-chloronaphthalene is a suitable solvent for reaction between phthalonitrile and gallium triiodide or tribromide to provide iodogallium phthalocyanine or bromogallium phthalocyanine. Reaction of chlorogallium phthalocyanine or hydroxygallium phthalocyanine with hydroiodic (or hydrobromic) acid is also effective for providing a novel crystal form of iodo- (or bromo-)gallium phthalocyanine. Zirconium phthalocyanine exhibiting good electrophotographic performances can be obtained through a similar process.

    摘要翻译: 具有新型结晶形式的碘镓酞菁和溴镓酞菁可以通过适当选择反应溶剂,然后在合适的溶剂中研磨或搅拌而获得,其特征在于根据CuKalpha特征X射线衍射法的X射线衍射图并显示出优异的锆酞菁 。 例如,α-氯萘是适用于邻苯二腈和三碘化镓与三溴化镓反应的溶剂,以提供碘镓酞菁或溴镓酞菁。 氯镓酞菁或羟基镓酞菁与氢碘酸(或氢溴酸)的反应对于提供新的晶体形式的碘 - (或溴 - )镓酞菁也是有效的。 可以通过类似的方法获得表现出良好的电子照相性能的锆酞菁。

    Electrophotographic photosensitive member, process cartridge and
electrophotographic apparatus
    112.
    发明授权
    Electrophotographic photosensitive member, process cartridge and electrophotographic apparatus 有权
    电子照相感光构件,处理盒和电子照相设备

    公开(公告)号:US6040100A

    公开(公告)日:2000-03-21

    申请号:US261504

    申请日:1999-03-03

    IPC分类号: G03G5/06

    摘要: An electrophotographic photosensitive member is formed of a support, and a photosensitive layer disposed on the support. The photosensitive layer is characterized by containing an azo pigment having an organic group represented by formula (1) below: wherein A denotes a residue group of formula (1A) below: ##STR1## and k.sub.1, k.sub.2, Z.sub.1, Z.sub.2, D; R.sub.1 and R.sub.2 are defined in the text. The group of the formula (1) may provide at least one of up to 4 azo-substituents of the azo pigment having an entire structure represented by ##STR2## wherein Ar denotes an aromatic or heterocyclic core unit, Cp denotes a coupler residue group, and --(N.dbd.N--Cp) denotes such an azo-substituent. The photosensitive member can exhibit good electrophotographic performances including high and stable sensitivity on repetitive use.

    摘要翻译: 电子照相感光构件由支撑体和设置在支撑体上的感光层形成。 感光层的特征在于含有具有由下式(1)表示的有机基团的偶氮颜料:其中A表示下式(1A)的残基:和k1,k2,Z1,Z2,D; R1和R2在文中定义。 式(1)的基团可以提供具有由Ar表示芳族或杂环核心单元表示的整个结构的至多4个偶氮颜料的偶氮取代基中的至少一个,Cp表示成色剂残基,和 - ( N = N-Cp)表示这种偶氮取代基。 感光构件可以表现出良好的电子照相性能,包括对重复使用的高且稳定的灵敏度。

    Silyl thioalkene compound and method for the preparation thereof
    113.
    发明授权
    Silyl thioalkene compound and method for the preparation thereof 失效
    硅烷基硫代烯烃化合物及其制备方法

    公开(公告)号:US5977394A

    公开(公告)日:1999-11-02

    申请号:US261387

    申请日:1999-03-03

    CPC分类号: C07F7/1836 C07F7/12

    摘要: Disclosed is a silyl thioalkene compound, as a class of organosilicon compounds, represented by the general formulaR(--CSAr.dbd.CHSiX.sub.3).sub.n,in which the subscript n is 1 or 2, R is, when n is 1, a hydrogen atom or unsubstituted or substituted monovalent hydrocarbon group or, when n is 2, a divalent hydrocarbon group, Ar is an unsubstituted or nucleus-substituted aromatic monovalent aromatic hydrocarbon group and X is a halogen atom, a monovalent hydrocarbon group or hydrocarbyloxy group, having usefulness as an intermediate in the synthesis of various precision organic chemicals. The compound, of which X is a halogen atom X.sup.1, can be prepared, for example, by the reaction of an alkyne compound of the general formulaR(--C.tbd.CH).sub.n,with a silyl sulfide compound of the general formulaArS--SiX.sup.1.sub.3,in the presence of a platinum complex catalyst. The compound, of which X is a monovalent hydrocarbon group or a hydrocarbyloxy group, can be derived from the above obtained halogen-containing compound.

    摘要翻译: 公开了作为一类由通式R(-CSAr = CHSiX 3)n表示的有机硅化合物的甲硅烷基硫代烯烃化合物,其中下标n为1或2,当n为1时,R为氢原子或未取代的 或取代的一价烃基,或者n为2时为二价烃基,Ar为未取代的或核取代的芳香族一价芳香族烃基,X为卤素原子,一价烃基或烃氧基,作为中间体具有有用性 在合成各种精密有机化学品。 其中X为卤素原子X 1的化合物可以通过例如通式R(-C 3 CH CH)n的炔化合物与通式为ArS-SiX 13的甲硅烷基硫醚化合物反应来制备, 在铂络合物催化剂的存在下。 X为一价烃基或烃氧基的化合物可以由上述得到的含卤素化合物得到。

    Substrate treating apparatus
    114.
    发明授权
    Substrate treating apparatus 失效
    底物处理装置

    公开(公告)号:US5875804A

    公开(公告)日:1999-03-02

    申请号:US877008

    申请日:1997-06-16

    摘要: A substrate treating apparatus adapted for treating a substrate with treating fluid therein, the substrate treating apparatus includes a processing bath; a baffle plate with a plurality of holes disposed therein for dividing the processing bath into an upper region and a lower region, the holes allowing communication of the treating liquid between the upper region and the lower region. The baffle plate is composed of a material exhibiting a property that the contact angle of a bubble generated in the treating liquid with respect to the baffle plate is smaller than a predetermined value.

    摘要翻译: 一种基板处理装置,其特征在于,用于处理基板,处理流体,基板处理装置包括处理槽; 挡板,其中设置有多个孔,用于将处理槽分成上部区域和下部区域,所述孔允许处理液体在上部区域和下部区域之间连通。 挡板由表现出处理液中产生的气泡相对于挡板的接触角小于预定值的材料构成。

    Pattern recognition apparatus and method using fuzzy logic
    115.
    发明授权
    Pattern recognition apparatus and method using fuzzy logic 失效
    模糊识别装置及其使用模糊逻辑的方法

    公开(公告)号:US5479533A

    公开(公告)日:1995-12-26

    申请号:US223139

    申请日:1994-04-05

    申请人: Masato Tanaka

    发明人: Masato Tanaka

    IPC分类号: G06K9/64 G06K9/62

    CPC分类号: G06K9/6202

    摘要: Pattern recognition method and apparatus are provided which can recognize not only standard typewritten characters but also handwritten characters and various styles of fonts without the necessity of learning, formation of rules, and complicated algorithm for extracting characteristics of patterns which have been required to conventional pattern recognition apparatus. A signal representing a pattern to be recognized is inputted and converted into binary signals corresponding to the pattern. The binary signals are compared with predetermined reference patterns having indefinite boundaries. The reference patterns each are formed based on one or more multi-dimensional membership functions. A certainty factor of the pattern recognition is calculated from the comparison as the pattern recognition result.

    摘要翻译: 提供了不仅可以识别标准打字字符,而且还可以识别手写字符和各种风格的字体而不需要学习,形成规则的模式识别方法和装置,以及用于提取传统模式识别所需的模式特征的复杂算法 仪器。 表示要识别的图案的信号被输入并转换成对应于图案的二进制信号。 将二进制信号与具有无限边界的预定参考图案进行比较。 参考图案各自基于一个或多个多维隶属函数形成。 从比较中计算出模式识别的确定性因子作为模式识别结果。

    Silicon-containing pentacyclic compound, a silicon-containing ladder
polymer, and methods for producing the same
    117.
    发明授权
    Silicon-containing pentacyclic compound, a silicon-containing ladder polymer, and methods for producing the same 失效
    含硅五环化合物,含硅梯形聚合物及其制造方法

    公开(公告)号:US5449800A

    公开(公告)日:1995-09-12

    申请号:US363814

    申请日:1994-12-27

    CPC分类号: C08G77/60 C07F7/0809 C07F7/14

    摘要: There is disclosed a method for effectively producing a silicon-containing pentacyclic compound, wherein the method comprises reacting (a) a 1,2-bis(hydrosilyl)benzene with (b) a cyclic diyne in the presence of (c) a platinum compound. There is also disclosed a method for effectively producing a silicon-containing ladder polymer having a complete ladder structure, wherein the method comprises reacting (a) a 1,2,4,5-tetrakis(hydrosilyl)benzene with (b) a cyclic diyne in the presence of (c) a platinum compound.

    摘要翻译: 公开了一种有效生产含硅五环化合物的方法,其中所述方法包括在(c)铂化合物存在下使(a)1,2-双(氢化硅烷基)苯与(b)环状二炔反应 。 还公开了一种有效地制备具有完全梯形结构的含硅梯形聚合物的方法,其中所述方法包括使(a)1,2,4,5-四(氢化硅烷基)苯与(b)环状二炔 在(c)铂化合物的存在下。

    System for automatically adjusting parameters of a digital signal
reproducing apparatus
    118.
    发明授权
    System for automatically adjusting parameters of a digital signal reproducing apparatus 失效
    用于自动调整数字信号再现装置的参数的系统

    公开(公告)号:US5406429A

    公开(公告)日:1995-04-11

    申请号:US33557

    申请日:1993-03-18

    摘要: In a digital signal reproducing apparatus various adjustment jobs and measurement jobs can be automatically executed by a simple operation by providing a clock generator, an external waveform equalizer, an error detector, an edge detection circuit, and a DC following circuit in addition to a waveform equalizer by which a reproduced analog signal waveform is processed and then converted to a digital signal. The digital signal is equalized by a digital filter and sampled and the digital signal and extracted clocks are supplied. The reproducing level and the equalizer coefficients can be automatically adjusted and an error rate can be automatically measured. A pulse width modulation or bias recording can be automatically determined and a recording current can be automatically adjusted by the system and the inclination of magnetic heads and the distance between the heads can also be automatically measured.

    摘要翻译: 在数字信号再现装置中,除了波形之外,还可以通过简单的操作自动执行各种调整作业和测量作业,该方法通过提供时钟发生器,外部波形均衡器,误差检测器,边缘检测电路和DC跟随电路 均衡器,再现模拟信号波形被处理,然后转换成数字信号。 数字信号由数字滤波器均衡并进行采样,并提供数字信号和提取的时钟。 可以自动调整再现级别和均衡器系数,并可以自动测量错误率。 可以自动确定脉冲宽度调制或偏移记录,并且可以通过系统自动调整记录电流,并且还可以自动测量磁头的倾角和磁头之间的距离。

    Fuzzy data processing method and data smoothing filter
    119.
    发明授权
    Fuzzy data processing method and data smoothing filter 失效
    模糊数据处理方法和数据平滑滤波

    公开(公告)号:US5398303A

    公开(公告)日:1995-03-14

    申请号:US843751

    申请日:1992-02-28

    申请人: Masato Tanaka

    发明人: Masato Tanaka

    IPC分类号: G06F17/40 G06F9/44

    CPC分类号: G05B23/0221 Y10S706/90

    摘要: A unique data processing method and a fuzzy smoothing filter are disclosed which employ a three-dimensional elliptic membership function based on the fuzzy logic to remove noises from data including a sequence of measured points for evaluating the linearity of the measured points. The evaluation is carried out by superimposing the center of an ellipse represented by an elliptic membership function on a substantial central portion of inputted data, evaluating a factor representing the linearity of the inputted data by summing the degrees of membership derived at respective inputted data, calculating the ratio of the factor to a factor representing an ideal linearity of the inputted data, rotating the ellipse by a predetermined angular distance to derive the ratio at that position, repeating the rotating step until the peak is found, and determining the ratio when the peak is found as the linearity of the inputted data. The fuzzy smoothing filter is comprised of a data input for inputting data to be smoothed, a multi-dimensional membership function generator for calculating a degree of membership for the inputted data, a calculator for deriving an angle of the data and calculating the linearity of the data, smoothing processors coupled to receive the angle and the linearity of the data from the calculator for executing a smoothing operation in a plurality of modes, a selector for selecting one mode from among the plurality of smoothing modes, and a store for holding smoothing filter parameters supplied to the calculator and the selector.

    摘要翻译: 公开了一种独特的数据处理方法和模糊平滑滤波器,其采用基于模糊逻辑的三维椭圆隶属函数来从包括用于评估测量点的线性度的测量点序列的数据中去除噪声。 通过将由椭圆隶属函数表示的椭圆的中心重叠在输入数据的实质中心部分上来进行评估,通过对在各输入数据中导出的隶属度求和来计算表示输入数据的线性度的因子,计算 所述系数与表示所输入数据的理想线性度的因子的比率,将所述椭圆旋转预定角距离以导出所述位置处的比率,重复所述旋转步骤直到找到所述峰值,并且当所述峰值 被发现为输入数据的线性。 模糊平滑滤波器包括用于输入要平滑化的数据的数据输入,用于计算输入数据的隶属程度的多维隶属函数发生器,用于导出数据角度并计算数据的线性度的计算器 数据,平滑处理器,其被耦合以从所述计算器接收用于执行多个模式中的平滑操作的数据的角度和线性,用于从所述多个平滑模式中选择一个模式的选择器和用于保持平滑滤波器的存储器 提供给计算器和选择器的参数。

    Color developer for pressure-sensitive recording sheets
    120.
    发明授权
    Color developer for pressure-sensitive recording sheets 失效
    压敏记录纸的彩色显影剂

    公开(公告)号:US5393332A

    公开(公告)日:1995-02-28

    申请号:US164483

    申请日:1993-12-09

    IPC分类号: C07C51/15 C07C65/10 C09D11/00

    CPC分类号: C07C51/15

    摘要: Herein disclosed is a method for preparing a nuclear-substituted salicylic acid or a metal salt thereof represented by the following general formula (1): ##STR1## [wherein R.sub.1 and R.sub.2 each represents a t-butyl group, a t-amyl group, a t-octyl group, an isononyl group or an isododecyl group, provided that at least one of R.sub.1 and R.sub.2 represents an isononyl group or an isododecyl group; M represents a hydrogen atom or a metal atom; and n is the atomic valency of the metal atom M] which comprises the step of subjecting, to a Kolbe-Schmitt reaction, an alkali metal salt of a nuclear-substituted phenol represented by the following general formula (2): ##STR2## [wherein R.sub.1 and R.sub.2 are the same as those defined above] in which 100 to 50% of the alkali metal salt is potassium salt and 0 to 50% thereof is sodium salt, in a substantially water-insoluble solvent as a reaction medium. The method makes it possible to improve the yield of the specific nuclear-substituted salicylic acid and metal salts thereof and to provide such products having high purity without any post-treatment. The compounds can be used in color developers for pressure-sensitive recording sheets without any additional purification treatment.

    摘要翻译: 本文公开了一种由以下通式(1)表示的核取代的水杨酸或其金属盐的制备方法:其中R1和R2各自表示叔丁基,t- 戊基,叔辛基,异壬基或异十二烷基,条件是R 1和R 2中的至少一个表示异壬基或异十二烷基; M表示氢原子或金属原子; 并且n是金属原子M的原子价,其包括以下通式(2)表示的核取代苯酚的碱金属盐进行Kolbe-Schmitt反应的步骤:< IMAGE> 2)[其中R1和R2与上述定义相同],其中100〜50%的碱金属盐为钾盐,0〜50%为钠盐,在基本不溶于水的溶剂中作为反应介质 。 该方法可以提高特定的核取代的水杨酸及其金属盐的产率,并提供具有高纯度的这种产品,而不需要后处理。 这些化合物可以用于彩色显影剂,用于压敏记录片材,而无需任何额外的纯化处理。