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    Process for preparing a Ziegler-Natta catalyst
    131.
    发明授权
    Process for preparing a Ziegler-Natta catalyst 失效
    齐格勒 - 纳塔催化剂的制备方法

    公开(公告)号：US06818584B2

    公开(公告)日：2004-11-16

    申请号：US10182371

    申请日：2002-07-29

    Applicant: Thomas Garoff ,  Solveig Johansson ,  Paivi Waldvogel

    Inventor： Thomas Garoff ,  Solveig Johansson ,  Paivi Waldvogel

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/6548 ,  C08F4/6555 ,  C08F4/6546

    Abstract: Especially homogeneous supported Ziegler-Natta catalysts may be prepared in a simple one reaction vessel process from a magnesium hydrocarbyloxy starting material which is soluble in a hydrocarbon solvent. The process comprises: (I) reacting a magnesium hydrocarbyloxy compound with a chlorine-containing compound in a non-polar hydrocarbon solvent in which said magnesium hydrocarbyloxy compound is soluble whereby to produce a solution (A); and then either: (II) contacting the solution (A) with a chlorine containing tetravalent titanium compound to produce a solution (B); (III) impregnating solution (B) into a porous particulate support; or (II) impregnating solution (A) into a porous particulate support; and (III) contacting the solid support with a chlorine containing tetravalent titanium compound; or (II) impregnating solution (A) into a porous particulate support pretreated with a chlorine containing tetravalent titanium compound.

    Abstract translation: 特别均匀的齐格勒 - 纳塔催化剂可以在简单的一种反应容器方法中由可溶于烃溶剂的镁烃氧基起始原料制备。 该方法包括：（I）使镁烃氧基化合物与含氯化合物在其中所述镁烃氧基化合物可溶的非极性烃溶剂中反应，从而产生溶液（A）; 然后：（II）使溶液（A）与含氯的四价钛化合物接触以产生溶液（B）; （III）浸渍溶液（B）加入到多孔颗粒载体中; 或（II）浸渍溶液（A）进入多孔颗粒载体; 和（III）使固体载体与含氯四价钛化合物接触; 或（II）浸渍溶液（A）加入用含氯四价钛化合物预处理的多孔颗粒载体中。

    Triple-decker catalysts based on delocalized dianionic ligands
    133.
    发明授权
    Triple-decker catalysts based on delocalized dianionic ligands 失效
    基于离域二离子配体的三层催化剂

    公开(公告)号：US06812183B1

    公开(公告)日：2004-11-02

    申请号：US10421062

    申请日：2003-04-23

    Applicant: Sandor Nagy ,  Joel A. Mutchler

    Inventor： Sandor Nagy ,  Joel A. Mutchler

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/65912 ,  C08F4/6592

    Abstract: Catalysts useful for polymerizing olefins are disclosed. The catalysts comprise an activator and a triple-decker bimetallic complex. The complex includes two Group 3-10 transition metals and a delocalized dianionic ligand that is pi-bonded to each of the metals. The behavior of the catalysts can be modified by choice of each metal, by the choice of the dianionic ligand, or by choice of the ancillary ligands. The invention provides a new way to make a large variety of catalyst systems.

    Abstract translation: 公开了可用于聚合烯烃的催化剂。 催化剂包括活化剂和三层双金属络合物。 络合物包括两个3-10族过渡金属和与每种金属π键合的离域二离子配位体。 可以通过选择每种金属，通过选择二阴离子配体或通过选择辅助配体来修饰催化剂的行为。 本发明提供了一种制造各种催化剂体系的新方法。

    Catalyst system for ethylene polymerizations
    135.
    发明授权
    Catalyst system for ethylene polymerizations 失效
    用于乙烯聚合的催化剂体系

    公开(公告)号：US06794326B1

    公开(公告)日：2004-09-21

    申请号：US09673121

    申请日：2000-11-27

    Applicant: Arild Follestad ,  Klaus-Joachim Jens ,  Richard Blom ,  Ivar Martin Dahl

    Inventor： Arild Follestad ,  Klaus-Joachim Jens ,  Richard Blom ,  Ivar Martin Dahl

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/63925 ,  C08F4/63904 ,  C08F4/76

    Abstract: A catalyst system for the polymerization of ethylene, comprising a particulate inorganic oxide supporting a chromium oxide being in a reduced oxidation state and a metallocene compound having the formula Cp2ZrR′R″, wherein each Cp, being equal or different, is an unsubstituted or substituted cyclopentadienyl compound, and R′ and R′, independent of each other, are selected from the group comprising alkyls having 1 to 6 carbon atoms, unsubstituted or substituted benzyl, and phenoxy substituted with alkyls having 1 to 6 carbon atoms; or R′ or R″ may be a halide. The catalyst system is prepared by a method comprising the steps of calcining the support, joining onto the surface of the support a chronium-organic compound, subjecting the obtained catalyst precursor to oxidizing conditions to obtain the chromium in an oxidized state, reducing the oxidized chromium to obtain a main part thereof in a bivalent oxidation state, and contacting the reduced catalyst with the metallocene compound.

    Abstract translation: 一种用于乙烯聚合的催化剂体系，其包含负载氧化还原氧化物的颗粒状无机氧化物和具有式Cp2ZrR'R“的茂金属化合物，其中每个Cp相同或不同，为未取代或未取代的 取代的环戊二烯基化合物，R'和R'彼此独立地选自含有1至6个碳原子的烷基，未取代或取代的苄基和被具有1至6个碳原子的烷基取代的苯氧基; 或R'或R“可以是卤素。 催化剂体系通过以下步骤制备：煅烧载体，在载体的表面上连接有机化合物，使得到的催化剂前体经历氧化条件以获得氧化态的铬，还原氧化铬 以二价氧化态获得其主要成分，并使还原催化剂与金属茂化合物接触。

    Photocatalytic material and photocatalytic article
    136.
    发明授权
    Photocatalytic material and photocatalytic article 有权
    光催化材料和光催化制品

    公开(公告)号：US06794065B1

    公开(公告)日：2004-09-21

    申请号：US10048933

    申请日：2002-02-05

    Applicant: Takeshi Morikawa ,  Ryoji Asahi ,  Takeshi Ohwaki ,  Yasunori Taga

    Inventor： Takeshi Morikawa ,  Ryoji Asahi ,  Takeshi Ohwaki ,  Yasunori Taga

    IPC: B01J3100

    CPC classification number: B01J21/063 ,  B01J27/24 ,  B01J35/002 ,  B01J35/004 ,  B01J37/0238 ,  B01J37/34 ,  B01J37/341 ,  B01J37/346 ,  B01J37/349 ,  C01G23/04 ,  C01P2002/54 ,  C01P2002/77 ,  C01P2004/84

    Abstract: A photocatalytic material having titanium oxide crystals and anions X incorporated therein, which is prepared by at least one of a method comprising substituting anions X for some of the oxygen sites of titanium oxide crystals, a method comprising doping anions X between lattices of a titanium crystal and a method comprising doping grain boundaries of titanium oxide, or a combination of these method. The photocatalytic material has acquired a new energy level formed in a band gap of titanium oxide, which results in its exhibition of a photocatalytic activity by absorbing visible lights. The photocatalytic material can thus exhibit a satisfactory photocatalytic activity under sunlight and also in a room with a fluorescent lamp.

    Abstract translation: 一种具有钛氧化物晶体和阴离子X的光催化材料，其通过以下方法制备，所述方法包括用阴离子X取代氧化钛晶体的一些氧部位的方法，包括在钛晶体的晶格之间掺杂阴离子X的方法 以及包含掺杂二氧化钛的晶界的方法，或这些方法的组合。 光催化材料已经获得了在氧化钛带隙中形成的新能级，从而通过吸收可见光来展现光催化活性。 因此，光催化材料在阳光下以及在具有荧光灯的房间中表现出令人满意的光催化活性。

    Gas treatment device comprising SMSI material and methods for making and using the same
    138.
    发明授权
    Gas treatment device comprising SMSI material and methods for making and using the same 有权
    包含SMSI材料的气体处理装置及其制造和使用方法

    公开(公告)号：US06774080B2

    公开(公告)日：2004-08-10

    申请号：US10303616

    申请日：2002-11-25

    Applicant: William J. LaBarge ,  Richard F. Beckmeyer ,  Joachim Kupe

    Inventor： William J. LaBarge ,  Richard F. Beckmeyer ,  Joachim Kupe

    IPC: B01J3100

    CPC classification number: B01J37/0242 ,  B01D53/864 ,  B01D53/944 ,  B01J23/63 ,  B01J23/648 ,  B01J23/6482 ,  B01J23/6527 ,  B01J37/0225 ,  Y10T29/49345

    Abstract: A gas treatment device, comprises a substrate disposed within a shell. The substrate comprises a catalyst composition comprising a support, a catalyst, and a sufficient amount of SMSI material such that, upon exposure to a gas stream (at a gas treatment device operating temperature), less than or equal to about 35 wt % of hydrocarbons in the gas stream are burned. A method for forming a gas treatment device, comprises applying a slurry to a substrate, wherein the slurry comprises a support and a sufficient amount of SMSI material such that, upon exposure to a gas stream at a gas treatment device operating temperature, greater than or equal to about 50 wt % of hydrocarbons in the gas stream are cracked to a light fraction; applying a catalyst to the substrate; calcining the catalyst; and disposing the calcined substrate into a shell, with a retention material disposed between the shell and the calcined substrate.

    Abstract translation: 一种气体处理装置，包括设置在壳体内的基板。 底物包括催化剂组合物，其包含载体，催化剂和足量的SMSI材料，使得当暴露于气流（在气体处理装置工作温度下）时，小于或等于约35重量％的烃 一种用于形成气体处理装置的方法，包括将浆料施加到基材上，其中所述浆料包含载体和足量的SMSI材料，使得在气体处理下暴露于气流时 装置工作温度大于或等于约50重量％的气流中的烃被破裂成轻馏分; 将催化剂施加到基材上; 煅烧催化剂; 并将煅烧的基底设置在壳体中，其中保留材料设置在壳体和煅烧的基底之间。

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