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    Thermo-expansive microcapsules and their application
    11.
    发明授权
    Thermo-expansive microcapsules and their application 有权
    热膨胀微胶囊及其应用

    公开(公告)号：US06984347B2

    公开(公告)日：2006-01-10

    申请号：US10923811

    申请日：2004-08-24

    Applicant: Toshiaki Masuda ,  Ichiro Takahara ,  Takashi Hujie ,  Yoshiaki Shirakabe ,  Katsushi Miki

    Inventor： Toshiaki Masuda ,  Ichiro Takahara ,  Takashi Hujie ,  Yoshiaki Shirakabe ,  Katsushi Miki

    IPC: C08J9/16 ,  C08J9/18 ,  B01J13/02 ,  B32B15/02

    CPC classification number: B01J13/14 ,  Y10T428/2987

    Abstract: Thermo-expansive microcapsules comprising a shell of a polymer produced by polymerizing a mixture of monomers, which comprises (I) a nitrile monomer, (II) a monomer having an unsaturated double bond and carboxyl groups in a molecule, (III) a monomer having two or more of polymerizable double bonds in a molecule, and optionally, (IV) a monomer different from and copolymerizable with the monomers (I), (II) and (III) and a blowing agent encapsulated in the shell. The volume retention of the expanded microcapsules of the thermo-expansive microcapsules is 50% or more after loaded with 15 MPa.

    Abstract translation: 包含通过聚合单体混合物制备的聚合物的壳的热膨胀微胶囊，其包含（I）腈单体，（II）分子中具有不饱和双键的单体和羧基，（III）具有 分子中的两个或更多个可聚合双键，和任选地（Ⅳ）与单体（I），（II）和（III）不同且可共聚的单体和包封在壳中的发泡剂。 热膨胀微胶囊的膨胀微胶囊的体积保留率在加载15MPa后为50％以上。

    Thermo-expansive microspheres, their production process and their application
    13.
    发明授权
    Thermo-expansive microspheres, their production process and their application 有权
    热膨胀微球，其生产工艺及其应用

    公开(公告)号：US07994229B2

    公开(公告)日：2011-08-09

    申请号：US12068430

    申请日：2008-02-06

    Applicant: Katsushi Miki ,  Toshiaki Masuda ,  Ichiro Takahara ,  Takashi Fujie ,  Ikuo Yosejima

    Inventor： Katsushi Miki ,  Toshiaki Masuda ,  Ichiro Takahara ,  Takashi Fujie ,  Ikuo Yosejima

    IPC: C08J9/32

    CPC classification number: C08J9/32 ,  B01J13/14 ,  C08J2203/14 ,  C08J2203/22

    Abstract: The present invention provides a process for producing thermo-expansive microspheres comprising a thermoplastic resinous shell and a blowing agent being encapsulated in the shell, the blowing agent which is a fluorine-containing C2-10 compound having ether linkage, being free of chlorine and bromine atoms and gasifying at a temperature not higher than the softening point of the thermoplastic resin. The thermo-expansive microspheres have preferably an average particle size ranging from 1 to 100 μm and a CV, or coefficient of variation, of particle size distribution being 30% or less, and a retaining ratio of blowing agent encapsulated being 90% or more.

    Abstract translation: 本发明提供一种包含热塑性树脂壳和包封在壳中的发泡剂的热膨胀性微球的方法，发泡剂是具有醚键的含氟C2-10化合物，不含氯和溴 原子并在不高于热塑性树脂的软化点的温度下气化。 热膨胀性微球的平均粒径优选为1〜100μm，粒径分布的CV或变异系数为30％以下，发泡剂的保持率为90％以上。

    Thermally expanded microsphere, process for producing the same, thermally expandable microsphere and use thereof
    16.
    发明申请
    Thermally expanded microsphere, process for producing the same, thermally expandable microsphere and use thereof 有权
    热膨胀微球，其制造方法，热膨胀性微球及其用途

    公开(公告)号：US20070154711A1

    公开(公告)日：2007-07-05

    申请号：US10595910

    申请日：2004-11-15

    Applicant: Toshiaki Masuda ,  Takashi Fujie ,  Ichiro Takahara ,  Ikuo Yosejima ,  Katsushi Miki

    Inventor： Toshiaki Masuda ,  Takashi Fujie ,  Ichiro Takahara ,  Ikuo Yosejima ,  Katsushi Miki

    IPC: B32B17/02 ,  C08K9/10

    CPC classification number: C08J9/22 ,  B01J13/04 ,  B01J13/14 ,  C08J9/32 ,  C08J2203/142 ,  Y10T428/2985 ,  Y10T428/2987 ,  Y10T428/2991

    Abstract: A production process for heat-expanded microspheres comprising the step of providing a gaseous fluid containing heat-expandable microspheres, which comprise shell of thermoplastic resin and a blowing agent encapsulated therein having a boiling point not higher than the softening point of the thermoplastic resin and have an average particle size from 1 to 100 μm, feeding the gaseous fluid through a gas-introducing tube having a dispersion nozzle on its outlet and being fixed inside a hot gas flow, and emitting a jet of the gaseous fluid through the dispersion nozzle; a step wherein the gaseous fluid is collided on a collision plate fixed under the dispersion nozzle so as to disperse the heat-expandable microspheres in the hot gas flow; and a step wherein the dispersed heat-expandable microspheres are heated in the hot gas flow at a temperature not lower than their expansion initiating temperature and thus expanded. The production process results in minimum difference in the variation coefficient of particle size distribution between the microspheres before and after heat-expansion, slight ratio of raw microspheres and slightly expanded microspheres contained in resultant heat-expanded microspheres, and suppressed formation of aggregated microspheres.

    Abstract translation: 一种热膨胀微球的制造方法，包括以下步骤：提供包含热膨胀性微球的气态流体，其包含热塑性树脂壳和封装在其中的发泡剂，沸点不高于热塑性树脂的软化点，并具有 平均粒度为1〜100μm，通过具有分散喷嘴的气体导入管在其出口处供给气体流体并固定在热气流内，并通过分散喷嘴喷射气态流体; 其中气态流体碰撞在固定在分散喷嘴下方的碰撞板上，以将热膨胀性微球分散在热气流中; 以及在热气流中以不低于其膨胀开始温度的温度加热分散的热膨胀性微球从而膨胀的步骤。 生产过程导致热膨胀前后的微球之间的粒度分布的变异系数的差异最小，所得热膨胀微球中所含的微生物微球和微球的微小比例，抑制聚集的微球的形成。

    HEAT-EXPANDABLE MICROSPHERES AND HOLLOW FINE PARTICLES AND METHOD FOR PRODUCING THE SAME AS WELL AS TIRE/RIM ASSEMBLY
    18.
    发明申请
    HEAT-EXPANDABLE MICROSPHERES AND HOLLOW FINE PARTICLES AND METHOD FOR PRODUCING THE SAME AS WELL AS TIRE/RIM ASSEMBLY 审中-公开
    可热膨胀的微孔和中空微粒及其制造方法，如轮胎/ RIM装配

    公开(公告)号：US20120080131A1

    公开(公告)日：2012-04-05

    申请号：US13301256

    申请日：2011-11-21

    Applicant: Hiroyuki TERATANI ,  Toshiaki MASUDA ,  Kenichi KITANO ,  Katsushi MIKI ,  Takayuki AOKI ,  Takeshi INOHARA

    Inventor： Hiroyuki TERATANI ,  Toshiaki MASUDA ,  Kenichi KITANO ,  Katsushi MIKI ,  Takayuki AOKI ,  Takeshi INOHARA

    IPC: B60C17/04

    CPC classification number: B01J13/14 ,  B01J13/04 ,  B60C17/01 ,  B60C17/066 ,  B60C29/062 ,  C08J9/146 ,  C08J9/20

    Abstract: In heat-expandable microspheres as a starting material for hollow fine particles, which have excellent performances required for giving not only a durability in steady running region but also a durability in high-speed running region to a tire-rim assembly, and each consisting of an outer shell made of a thermoplastic resin obtained by polymerizing a monomer component in the presence of a polymerization initiator, and a foaming agent encapsulated in the outer shell and having a boiling point not higher than a softening point of the thermoplastic resin, the polymerization initiator comprises a peroxydicarbonate as an essential component, and the foaming agent comprises a fluorine-containing compound having an ether structure and a carbon number of 2-10 and containing no chlorine atom and bromine atom.

    Abstract translation: 在作为中空微粒的原料的热膨胀性微球中，其具有优异的性能，其不仅在稳定运行区域中不仅具有耐久性，而且在高速运行区域中对轮胎 - 轮辋组件的耐久性，并且各自由 由在聚合引发剂存在下聚合单体成分而获得的热塑性树脂制成的外壳和封装在外壳中并且沸点不高于热塑性树脂的软化点的发泡剂，聚合引发剂 以过氧化二碳酸酯为必须成分，发泡剂含有具有醚结构，碳数为2-10且不含氯原子和溴原子的含氟化合物。

    Heat-expanded microspheres, production process thereof, heat-expandable microspheres and application thereof
    19.
    发明授权
    Heat-expanded microspheres, production process thereof, heat-expandable microspheres and application thereof 有权
    热膨胀微球，其制备方法，热膨胀性微球及其应用

    公开(公告)号：US07807729B2

    公开(公告)日：2010-10-05

    申请号：US10595910

    申请日：2004-11-15

    Applicant: Toshiaki Masuda ,  Takashi Fujie ,  Ichiro Takahara ,  Ikuo Yosejima ,  Katsushi Miki

    Inventor： Toshiaki Masuda ,  Takashi Fujie ,  Ichiro Takahara ,  Ikuo Yosejima ,  Katsushi Miki

    IPC: C08J9/22 ,  C08J9/16 ,  B32B27/00

    CPC classification number: C08J9/22 ,  B01J13/04 ,  B01J13/14 ,  C08J9/32 ,  C08J2203/142 ,  Y10T428/2985 ,  Y10T428/2987 ,  Y10T428/2991

    Abstract: A production process for heat-expanded microspheres includes the step of providing a gaseous fluid containing heat-expandable microspheres, which includes a shell of thermoplastic resin and a blowing agent encapsulated therein having a boiling point not higher than the softening point of the thermoplastic resin and have an average particle size from 1 to 100 μm. The gaseous fluid is fed through a gas-introducing tube having a dispersion nozzle on its outlet that is fixed inside a conduit having a hot gas flow flowing therethrough. A jet of the gaseous fluid is emitted through the dispersion nozzle. Further, the gaseous fluid is collided on a collision plate fixed under the dispersion nozzle so as to disperse the heat-expandable microspheres in the hot gas flow. The dispersed heat-expandable microspheres are heated in the hot gas flow at a temperature not lower than their expansion initiating temperature and thus expanded.

    Abstract translation: 热膨胀微球的制造方法包括提供含有热膨胀性微球的气态流体的步骤，其包括热塑性树脂的壳和封装在其中的沸点不高于热塑性树脂的软化点的发泡剂， 平均粒径为1〜100μm。 气体流体通过其出口上具有分散喷嘴的气体导入管被供给，该出口固定在具有流过其中的热气流的管道内。 气体流体的射流通过分散喷嘴发射。 此外，气体流体在固定在分散喷嘴下方的碰撞板上碰撞，以将热膨胀性微球分散在热气流中。 分散的热膨胀性微球体在热气流中以不低于其膨胀开始温度的温度加热，从而膨胀。

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