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    Method for polymerizing cycloolefin polymer containing polar functional groups and electronic devices employing the polymerized cycloolefins
    11.
    发明授权
    Method for polymerizing cycloolefin polymer containing polar functional groups and electronic devices employing the polymerized cycloolefins 有权
    聚合包含极性官能团的环烯烃聚合物的方法和使用聚合环烯烃的电子器件

    公开(公告)号：US07718744B2

    公开(公告)日：2010-05-18

    申请号：US10502185

    申请日：2003-12-03

    申请人： Sung-Cheol Yoon ,  Sung-Ho Chun ,  Won-Kook Kim ,  Tae-Sun Lim ,  Heon Kim ,  Jung-Min Lee

    发明人： Sung-Cheol Yoon ,  Sung-Ho Chun ,  Won-Kook Kim ,  Tae-Sun Lim ,  Heon Kim ,  Jung-Min Lee

    IPC分类号： C08F4/80 ,  C08F10/00 ,  C08F36/00 ,  C08F38/00 ,  C08F32/00 ,  C08F210/00

    CPC分类号： C08F4/70 ,  C08F32/00 ,  C08F232/08 ,  C08G61/06 ,  C08G61/08 ,  C09K19/38 ,  Y10T428/1036

    摘要： Disclosed is a method for preparing a cycloolefin polymer containing polar functional groups, comprising: preparing a catalyst mixture including i) a precatalyst, containing a Group 10 transition metal having a ligand containing oxygen ions bonded to the metal; ii) a first cocatalyst which is an organic compound containing a Group 15 element; and iii) a second cocatalyst which is capable of providing an anion and weakly coordinating to the metal of the precatalyst; and subjecting a monomer solution comprising a norbornene-based compound containing a polar functional group to an addition polymerization reaction in the presence of an organic solvent and the catalyst mixture, at a temperature of 80-200° C., the total amount of the organic solvent being 50-800% by weight based on the total weight of the monomer contained in the monomer solution, and the product yield of the polymer being 50% by weight or more based on the total weight of the monomer.

    摘要翻译： 公开了一种制备含有极性官能团的环烯烃聚合物的方法，包括：制备催化剂混合物，其包括i）含有具有与金属键合的含氧离子的配体的第10族过渡金属的预催化剂; ii）第一助催化剂，其是含有第15族元素的有机化合物; 和iii）能够提供阴离子并与预催化剂的金属弱配位的第二助催化剂; 将含有极性官能团的降冰片烯系化合物的单体溶液在有机溶剂和催化剂混合物的存在下，在80〜200℃的温度下进行加成聚合反应， 溶剂为50-800重量％，基于单体溶液中所含单体的总重量，聚合物的产物收率基于单体的总重量为50重量％以上。

    Method for preparing norbornene based addition polymer containing ester or acetyl functional group
    17.
    发明授权
    Method for preparing norbornene based addition polymer containing ester or acetyl functional group 有权
    制备含有酯或乙酰基官能团的降冰片烯基加成聚合物的方法

    公开(公告)号：US07312285B2

    公开(公告)日：2007-12-25

    申请号：US10494882

    申请日：2003-07-07

    申请人： Sung-Ho Chun ,  Won-Kook Kim ,  Sung-Cheol Yoon ,  Tae-Sun Lim ,  Heon Kim ,  Kyoung-Hoon Kim

    发明人： Sung-Ho Chun ,  Won-Kook Kim ,  Sung-Cheol Yoon ,  Tae-Sun Lim ,  Heon Kim ,  Kyoung-Hoon Kim

    IPC分类号： C08F4/44

    CPC分类号： C08G61/08 ,  C08F4/7027 ,  C08F32/08 ,  C08F132/08 ,  C08F2410/01 ,  C08G61/06 ,  G02F1/136227

    摘要： The present invention relates to a method for preparing a cyclic olefin polymer by addition polymerization, and more particularly to a method for preparing a norbornene-based addition polymer, which comprises a step of contacting a norbornene-based monomer having an ester or acetyl group with a catalyst system comprising: a Group X transition metal compound; a compound comprising a neutral Group XV electron donor ligand having a cone angle of at least 160°; and a salt capable of offering an anion that can be weakly coordinated to the transition metal, in solvent. The norbornene-based addition polymer having an ester or acetyl group according to the present invention is transparent, has superior adhesivity and a low dielectric constant, and it generates no byproducts when attached to metal. Therefore, it can be used as an optical film, a retardation film, a protection film for a polarizer, POFs (plastic optical fiber), PCBs (printed circuit board), or insulators of electronic devices.

    摘要翻译： 本发明涉及通过加成聚合制备环烯烃聚合物的方法，更具体地说涉及一种制备降冰片烯系加成聚合物的方法，该方法包括使具有酯或乙酰基的降冰片烯系单体与 一种催化剂体系，包括：第X族过渡金属化合物; 包含具有至少160°的锥角的中性第XV族电子供体配体的化合物; 以及能够在溶剂中提供能够与过渡金属配位的阴离子的盐。 具有根据本发明的酯或乙酰基的降冰片烯系加成聚合物是透明的，具有优异的粘合性和低介电常数，并且当附着于金属时不产生副产物。 因此，它可以用作光学膜，延迟膜，偏振器用保护膜，POF（塑料光纤），PCB（印刷电路板）或电子器件的绝缘体。