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    Manufacture of carboxamides
    11.
    发明授权
    Manufacture of carboxamides 失效
    甲酰胺的制造

    公开(公告)号：US3928439A

    公开(公告)日：1975-12-23

    申请号：US45945874

    申请日：1974-04-10

    Applicant: BASF AG

    Inventor： DOCKNER TONI ,  PLATZ ROLF

    IPC: C07C231/06 ,  B01J21/00 ,  B01J23/12 ,  B01J23/84 ,  C07C67/00 ,  C07C231/00 ,  C07C233/09 ,  C07C233/65 ,  C07C103/00

    CPC classification number: B01J23/12 ,  B01J23/84

    Abstract: Manufacture of carboxamides by the addition of water to nitriles in the presence of a copper-containing and magnesium silicatecontaining catalyst which has been treated with a reducing gas. The carboxamides obtained by the process of the invention are valuable starting materials for the manufacture of solvents, flocculating agents, crosslinking agents, pesticides, plant protectants, textile auxiliaries such as levelling agents, waterproofing agents, foam stabilizers and detergents.

    Abstract translation: 在含还原气体处理过的含铜硅酸镁催化剂存在下，通过向腈中加入水来制造甲酰胺。 通过本发明方法获得的羧酰胺是用于制造溶剂，絮凝剂，交联剂，农药，植物保护剂，纺织助剂如流平剂，防水剂，泡沫稳定剂和洗涤剂的有价值的原料。

    Production of alkynols and alkynediols
    12.
    发明授权
    Production of alkynols and alkynediols 失效
    生产烷基醇和烷基二醇

    公开(公告)号：US3723545A

    公开(公告)日：1973-03-27

    申请号：US921170

    申请日：1970-02-06

    Applicant: BASF AG

    Inventor： NAGEL OTTO ,  PLATZ ROLF ,  FUCHS WERNER

    IPC: B01J10/00 ,  B01J31/00 ,  C07B61/00 ,  C07C27/00 ,  C07C29/42 ,  C07C33/04 ,  C07C33/046 ,  C07C33/28 ,  C07C67/00 ,  C07C33/06

    CPC classification number: C07C29/42 ,  C07C33/046 ,  Y10S261/75

    Abstract: Production of alkynols and/or alkynediols by reaction of acetylene with aldehydes in a liquid reaction medium in the presence of a heavy metal acetylide as catalyst and in the presence or absence of basic reagents, at least one of the starting materials being introduced in gaseous form. The catalyst is suspended in the liquid medium and during the reaction a portion of the reaction medium is withdrawn and returned at the entry point below the level of the liquid of the gaseous starting material(s) at a speed of 5 to 100 meters per second into the reaction medium and is introduced into a chamber (located in the reaction medium and extending in the direction of the liquid returned) whose inlet opening has a mean diameter from twice to twenty times the mean diameter of the liquid nozzle and whose length is three to thirty times ints hydraulic diameter. The products are important intermediates for example for the production of solvents or may be used in electrolytic baths.

    Abstract translation: 在重金属乙炔化物作为催化剂的存在下，在液态反应介质中，乙炔与醛反应生成炔烃和/或炔二醇，在碱性试剂存在或不存在下，至少一种原料以气态形式引入 。 催化剂悬浮在液体介质中，并且在反应期间，反应介质的一部分以5至100米/秒的速度在气态起始材料液体的入口点下方返回 进入反应介质并引入到入口开口的平均直径为液体喷嘴的平均直径的二倍至二十倍的室（位于反应介质中并沿着返回的液体的方向延伸），其长度为三 至30倍液压直径。 该产品是重要的中间体，例如用于生产溶剂或可用于电解池。

    Production of lactic acid
    14.
    发明授权
    Production of lactic acid 失效
    生产酸性酸

    公开(公告)号：US3642889A

    公开(公告)日：1972-02-15

    申请号：US3642889D

    申请日：1966-11-01

    Applicant: BASF AG

    Inventor： PLATZ ROLF ,  NOHE HEINZ ,  DOCKNER TONI

    IPC: C07C51/097 ,  C07C59/08

    CPC classification number: C07C51/097 ,  C07C59/08

    Abstract: PROCESS FOR PRODUCING LACTIC ACID BY THE HYDROLYSIS OF LACTIC ACID NITRATE IN WHICH THE LACTICE ACID NITRATE IS REACTED WITH MORE THAN TWICE ITS WEIGHT OF WATER. IT HAS BEEN FOUND THAT HIGH YEILDS OF LACTICE ACID CAN BE OBTAINED EITHER FROM PURE LATICE ACID NITRATE OR FROM THE REACTION PRODUCT CONTAINING IMPURITIES AS WELL AS LACTIC ACID NITRATE.

    Recovering bromine and iodine from reaction products of oxydehydrogenations
    16.
    发明授权
    Recovering bromine and iodine from reaction products of oxydehydrogenations 失效
    从氧自由基的反应产物中回收溴和碘

    公开(公告)号：US3592600A

    公开(公告)日：1971-07-13

    申请号：US3592600D

    申请日：1968-09-06

    Applicant: BASF AG

    Inventor： PLATZ ROLF ,  BAUR KARL GERHARD

    IPC: B01J38/00 ,  C01B7/09 ,  C01B7/13 ,  C07C5/48 ,  C01C1/16

    CPC classification number: C07C5/48 ,  B01J38/00 ,  C01B7/09 ,  C01B7/13 ,  Y02P20/584

    Abstract: THE RECOVERY OF BROMINE AND/OR IODINE FROM THE REACTION PRODUCTS OF OXYDEHYDROGENATIONS OF HYDROCARBONS IN WHICH BROMINE AND/OR IODINE SERVES AS A CATALYST, WHEREIN THE REACTION PRODUCT LEAVING THE REACTOR IS TREATED WITH AN AGUEOUS AMMONIA SOLUTION TO WHICH HAS BEE ADDED AN AMOUNT OF HYDRAZINE SUFFICIENT FOR THE REDUCTION OF THE ELEMENTARY CONSTITUENTS. THE AQUEOUS PHASE IS SEPARATED AND THE BYPRODUCTS CONTAINING BROMINE AND/ OR IODINE SEPARATED IN THE WORKING UP OF THE ORGANIC PHASE ARE BURNT AND OXYGEN-CONTAINING GASES AND THE GAS FROM THE COMBUSTION IS SCRUBBED WITH AN AMMONIA SOLUTION CONTAINING HYDRAZINE.

    Production of acetylene
    17.
    发明授权
    Production of acetylene 失效
    乙烯的生产

    公开(公告)号：US3686344A

    公开(公告)日：1972-08-22

    申请号：US3686344D

    申请日：1970-06-22

    Applicant: BASF AG

    Inventor： BRUNNER ERWIN ,  PLATZ ROLF ,  TAGLIEBER KURT ,  WEINFURTER KURT

    IPC: C07C7/00 ,  C07C7/11 ,  C07C11/24

    CPC classification number: C07C11/24 ,  C07C7/005 ,  C07C7/11

    Abstract: Production of pure acetylene from a cracked gas obtained by cracking gaseous hydrocarbons, the process comprising a number of steps wherein the higher C3 to C5 hydrocarbons remaining in the crude acetylene are washed out with an organic solvent such as toluene.

    Abstract translation: 从通过裂解气态烃获得的裂化气体中生产纯乙炔，该方法包括若干步骤，其中残留在粗乙炔中的较高C3至C5烃用有机溶剂如甲苯洗涤。

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