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    CORE-SHELL NANOPARTICLES AND METHOD FOR MANUFACTURING THE SAME
    12.
    发明申请
    CORE-SHELL NANOPARTICLES AND METHOD FOR MANUFACTURING THE SAME 审中-公开
    核壳纳米粒子及其制造方法

    公开(公告)号：US20160002438A1

    公开(公告)日：2016-01-07

    申请号：US14770911

    申请日：2014-01-21

    Applicant: DIC CORPORATION

    Inventor： Jianjun Yuan ,  Hiroshi Kinoshita

    IPC: C08K3/36

    CPC classification number: C08K3/36 ,  B01J13/14 ,  B01J21/08 ,  B01J23/50 ,  B01J23/52 ,  B01J35/0013 ,  B01J35/002 ,  B01J35/008 ,  B22F1/02 ,  B22F9/00 ,  B82Y30/00 ,  B82Y40/00 ,  C09B65/00 ,  C09B67/0097

    Abstract: Provided are core-shell nanoparticles including a metal nanoparticle core and a shell layer composed of an oxide hybridized with a polyamine containing primary amino groups and/or secondary amino groups, core-shell metal nanoparticles prepared by removing the organic component from the shell layer and including a metal nanoparticle core and a shell layer based on silica, and simple and efficient methods for manufacturing such nanoparticles. Provided are a method for manufacturing a core-shell nanoparticle including performing a sol-gel reaction of an oxide source (C′) in the presence of a metal nanoparticle (A) having thereon a layer of a compound (B) containing a polyamine segment (b1) containing primary amino groups and/or secondary amino groups, a method for manufacturing a core-shell metal nanoparticle further including performing a sol-gel reaction of an organosilane to form a shell layer containing a polysilsesquioxane (D), and nanoparticles prepared by such methods.

    Abstract translation: 提供的是包含金属纳米颗粒核心的核 - 壳纳米颗粒和由与含有伯氨基和/或仲氨基的多胺杂化的氧化物构成的壳层，通过从壳层除去有机组分制备的核 - 壳金属纳米颗粒， 包括金属纳米颗粒芯和基于二氧化硅的壳层，以及用于制造这种纳米颗粒的简单而有效的方法。 提供一种核 - 壳纳米粒子的制造方法，其包括在金属纳米粒子（A）的存在下进行氧化物源（C'）的溶胶 - 凝胶反应，所述金属纳米粒子（A）上具有含有多胺链段 （b1），还包括进行有机硅烷的溶胶 - 凝胶反应以形成含有聚倍半硅氧烷（D）的壳层的核 - 壳金属纳米粒子的制造方法，和制备的纳米颗粒 通过这种方法。

    ORGANIC-INORGANIC HYBRID SILICA NANOPARTICLE AND METHOD FOR PRODUCING SAME
    17.
    发明申请
    ORGANIC-INORGANIC HYBRID SILICA NANOPARTICLE AND METHOD FOR PRODUCING SAME 审中-公开
    有机无机混合二氧化硅纳米微粒及其生产方法

    公开(公告)号：US20150291764A1

    公开(公告)日：2015-10-15

    申请号：US14433953

    申请日：2013-10-10

    Applicant: DIC Corporation

    Inventor： Jianjun Yuan ,  Hiroshi Kinoshita

    IPC: C08K3/36 ,  C08K3/32

    CPC classification number: C08K3/36 ,  B82Y30/00 ,  B82Y40/00 ,  C01B33/145 ,  C01B33/18 ,  C08G77/045 ,  C08G83/001 ,  C08K3/32 ,  C08K9/08 ,  C08K2003/329 ,  C08L87/00 ,  C09K3/1436

    Abstract: Provided are organic-inorganic hybrid silica nanoparticles having excellent monodispersity, an organic component (polymer) being introduced into a silica matrix, the whole of each particle being composed of a hybrid between the organic component and an inorganic component [silica], and the particle diameter being in the range of 5 to 100 nm; and a simple and efficient method for producing the silica nanoparticles. Organic-inorganic hybrid silica nanoparticles contain a copolymer (A) composed of an amorphous polyamine chain and a nonionic polymer chain, an acidic group-containing compound (B), and silica (C). A method for producing organic-inorganic hybrid silica nanoparticles includes the steps of allowing a copolymer (A) composed of an amorphous polyamine chain and a nonionic polymer chain to associate with an acidic group-containing compound (B) in a medium and then performing a sol-gel reaction of a silica source using the association product as a reaction field in the presence of water.

    Abstract translation: 提供了具有优异的单分散性的有机 - 无机杂化二氧化硅纳米粒子，将有机成分（聚合物）引入到二氧化硅基质中，整个粒子由有机成分和无机成分[二氧化硅]的混合物构成，粒子 直径在5至100nm的范围内; 以及用于制备二氧化硅纳米颗粒的简单有效的方法。 有机 - 无机混合二氧化硅纳米粒子含有由无定形多胺链和非离子聚合物链组成的共聚物（A），含酸性基团的化合物（B）和二氧化硅（C）。 制备有机 - 无机混合二氧化硅纳米粒子的方法包括以下步骤：使由无定形多胺链和非离子聚合物链组成的共聚物（A）与介质中的含酸性基团的化合物（B）缔合，然后进行 在水存在下使用缔合产物作为反应场的二氧化硅源的溶胶 - 凝胶反应。

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