公开(公告)号：US06310167B1

公开(公告)日：2001-10-30

申请号：US09373194

申请日：1999-08-12

申请人： Mitsugu Kanzawa ,  Fumio Okuda ,  Tatsuya Housaki ,  Tomio Tatsumi

发明人： Mitsugu Kanzawa ,  Fumio Okuda ,  Tatsuya Housaki ,  Tomio Tatsumi

IPC分类号： C08F1002

CPC分类号： C08F110/02 ,  C08F10/00 ,  C08F2500/10 ,  C08F2500/12 ,  C08F2500/08 ,  C08F4/7006

摘要： Provided are an ethylene homopolymer having well-balanced properties of good heat resistance, good heat-sealability and good moldability, and its molded articles. The ethylene homopolymer is characterized in that the number of butyl branches per 100 methyl branches therein falls between 1 and 20, as measured through 13C-NMR, that its density, d (kg/m3), falls between 880 and 980, and that the density, d, and its melting point, Tm (° C.) , satisfy the conditions defined by the following formulae (1) to (3): Tm≧1.2×d−982 (980≧d≧925)  (1), Tm≧0.6×d−430 (925>d≧915)  (2), Tm≧0.16×d−28.4 (915>d≧880)  (3). The ethylene homopolymer is molded into moldings.

摘要翻译： 提供具有良好的耐热性，良好的热封性和良好的成型性的良好平衡性的乙烯均聚物及其模塑制品。 乙烯均聚物的特征在于，通过13 C-NMR测量，其每100个甲基支链中的丁基支链数目在1和20之间，其密度d（kg / m 3）在880和980之间， 密度d及其熔点Tm（℃）满足由下式（1）至（3）定义的条件：将乙烯均聚物模塑成型。

公开(公告)号：US20120037890A1

公开(公告)日：2012-02-16

申请号：US13138501

申请日：2010-02-25

申请人： Fumio Okuda ,  Kiyoshi Ikeda ,  Takayasu Sado ,  Takahiko Ochi ,  Yoshimitsu Tanabe ,  Bunji Sawano

发明人： Fumio Okuda ,  Kiyoshi Ikeda ,  Takayasu Sado ,  Takahiko Ochi ,  Yoshimitsu Tanabe ,  Bunji Sawano

IPC分类号： H01L51/54 ,  C07F5/04

CPC分类号： C07D403/06 ,  C07D207/44 ,  C07D209/44 ,  C07F5/022 ,  C09K11/06 ,  C09K2211/1022 ,  C09K2211/1029 ,  H01L51/0054 ,  H01L51/008 ,  H01L51/5012 ,  H05B33/14

摘要： A pyrromethene-boron complex compound represented by the following formula (1); wherein Z1 and Z2 are independently a hydrogen atom, a substituted or unsubstituted aryl group, a substituted or unsubstituted alkoxy group or a substituted or unsubstituted aryloxy group, at least one of Z1 and Z2 is an alkoxy group substituted with a fluorine atom or an aryloxy group substituted with a fluorine atom or a fluoroalkyl group, and Z1 and Z2 may form a ring.

摘要翻译： 由下式（1）表示的亚甲基吡咯 - 硼络合物; 其中Z1和Z2独立地是氢原子，取代或未取代的芳基，取代或未取代的烷氧基或取代或未取代的芳氧基，Z1和Z2中的至少一个是被氟原子取代的烷氧基或芳氧基 被氟原子或氟烷基取代的基团，Z1和Z2可以形成环。

公开(公告)号：US20090039767A1

公开(公告)日：2009-02-12

申请号：US11833657

申请日：2007-08-03

申请人： Masa-aki Haga ,  Masumi Itabashi ,  Misa Ashizawa ,  Fumio Okuda ,  Toshinari Ogiwara ,  Hideaki Nagashima

发明人： Masa-aki Haga ,  Masumi Itabashi ,  Misa Ashizawa ,  Fumio Okuda ,  Toshinari Ogiwara ,  Hideaki Nagashima

IPC分类号： H01L51/54 ,  C07F17/02

CPC分类号： C07F15/0033 ,  H01L51/0059 ,  H01L51/006 ,  H01L51/0067 ,  H01L51/0071 ,  H01L51/0072 ,  H01L51/0077 ,  H01L51/0081 ,  H01L51/0085 ,  H01L51/5016 ,  H01L51/5036 ,  H01L51/5048 ,  H01L2251/308

摘要： Provided are an organic electroluminescence device which: can emit blue light having a short wavelength and a high color purity; and can be combined with any other light emitting compound to emit white light and a metal complex compound for realizing the device, and a material for an organic electroluminescence device. The metal complex is of a specific structure having a tridentate chelate ligand and an electron withdrawing group. The material for an organic electroluminescence device is formed of the metal complex compound. The organic electroluminescence device has an organic thin film layer formed of one or more layers including at least a light emitting layer, the organic thin film layer being interposed between a pair of electrodes. In the organic electroluminescence device, at least one layer of the organic thin film layer contains the metal complex compound, and emits light by applying a voltage between both the electrodes.

摘要翻译： 提供一种有机电致发光元件，其能够发出短波长，高纯度的蓝光; 并且可以与任何其它发光化合物组合以发射白光，并且用于实现该装置的金属络合物和用于有机电致发光器件的材料。 金属络合物是具有三齿螯合配体和吸电子基团的特定结构。 用于有机电致发光器件的材料由金属络合物形成。 有机电致发光器件具有由至少包含发光层的一层或多层形成的有机薄膜层，有机薄膜层介于一对电极之间。 在有机电致发光元件中，有机薄膜层的至少一层含有金属络合物，通过在两电极之间施加电压来发光。

公开(公告)号：US20070210699A1

公开(公告)日：2007-09-13

申请号：US11515777

申请日：2006-09-06

申请人： Masa-aki Haga ,  Li-fen Yang ,  Fumio Okuda

发明人： Masa-aki Haga ,  Li-fen Yang ,  Fumio Okuda

IPC分类号： H01J1/62 ,  C07F15/00 ,  H01J63/04

CPC分类号： H01L51/0085 ,  C07F15/0033 ,  C09K11/06 ,  C09K2211/1007 ,  C09K2211/1029 ,  C09K2211/1044 ,  C09K2211/185 ,  H01L51/5016 ,  H05B33/14

摘要： A metal-complex compound which comprises a tridentate chelate ligand having a specified partial structure. An organic electroluminescence device which comprises one or more organic thin film layers having at least one light emitting layer sandwiched between a pair of electrodes, wherein the organic thin film layer comprises the metal-complex compound, which emits light by applying an electric voltage between the pair of electrodes. The present invention provides an organic EL device which emits blue light of high purity and of short wavelength together with a metal-complex compound realizing the organic EL device.

摘要翻译： 一种金属络合物，其包含具有特定部分结构的三齿螯合配位体。 一种有机电致发光器件，包括一个或多个有机薄膜层，所述有机薄膜层具有夹在一对电极之间的至少一个发光层，其中所述有机薄膜层包含金属络合物，该化合物通过施加电压 一对电极。 本发明提供了一种发射具有高纯度和短波长的蓝光的有机EL器件与实现有机EL器件的金属络合物。

公开(公告)号：US5283351A

公开(公告)日：1994-02-01

申请号：US859930

申请日：1992-03-30

申请人： Hiroaki Kezuka ,  Fumio Okuda

发明人： Hiroaki Kezuka ,  Fumio Okuda

IPC分类号： B01J31/12 ,  B01J31/28 ,  C07B61/00 ,  C07C68/00 ,  C07C69/96 ,  C07C69/88

CPC分类号： C07C68/00

摘要： A process for efficiently producing an organic carbonate which comprises reacting an organic hydroxy compound and carbon monoxide in the absence of oxygen and in the presence of a catalyst comprising (a) palladium or a palladium compound, (b) a quinone or an aromatic diol formed by reduction of the quinone or a mixture thereof, and (c) a halogenated onium compound is disclosed.

摘要翻译： 一种有效制备有机碳酸酯的方法，其包括使有机羟基化合物与一氧化碳在不存在氧气的条件下和催化剂存在下反应，所述催化剂包含（a）钯或钯化合物，（b）形成的醌或芳族二醇 通过还原醌或其混合物，和（c）卤化鎓化合物。

公开(公告)号：US08778510B2

公开(公告)日：2014-07-15

申请号：US13138501

申请日：2010-02-25

申请人： Fumio Okuda ,  Kiyoshi Ikeda ,  Takayasu Sado ,  Takahiko Ochi ,  Yoshimitsu Tanabe ,  Bunji Sawano

发明人： Fumio Okuda ,  Kiyoshi Ikeda ,  Takayasu Sado ,  Takahiko Ochi ,  Yoshimitsu Tanabe ,  Bunji Sawano

IPC分类号： H01L51/54 ,  C07F5/04

CPC分类号： C07D403/06 ,  C07D207/44 ,  C07D209/44 ,  C07F5/022 ,  C09K11/06 ,  C09K2211/1022 ,  C09K2211/1029 ,  H01L51/0054 ,  H01L51/008 ,  H01L51/5012 ,  H05B33/14

摘要： A pyrromethene-boron complex compound represented by the following formula (1); wherein Z1 and Z2 are independently a hydrogen atom, a substituted or unsubstituted aryl group, a substituted or unsubstituted alkoxy group or a substituted or unsubstituted aryloxy group, at least one of Z1 and Z2 is an alkoxy group substituted with a fluorine atom or an aryloxy group substituted with a fluorine atom or a fluoroalkyl group, and Z1 and Z2 may form a ring.

摘要翻译： 由下式（1）表示的亚甲基吡咯 - 硼络合物; 其中Z1和Z2独立地是氢原子，取代或未取代的芳基，取代或未取代的烷氧基或取代或未取代的芳氧基，Z1和Z2中的至少一个是被氟原子取代的烷氧基或芳氧基 被氟原子或氟烷基取代的基团，Z1和Z2可以形成环。

公开(公告)号：US20070141397A1

公开(公告)日：2007-06-21

申请号：US11610093

申请日：2006-12-13

申请人： Masami Watanabe ,  Fumio Okuda

发明人： Masami Watanabe ,  Fumio Okuda

IPC分类号： B32B19/00

CPC分类号： H01L51/0085 ,  C07D213/81 ,  C07D233/58 ,  C07F15/0033 ,  H01L51/0067 ,  H01L51/0068 ,  H01L51/0071 ,  H01L51/0072 ,  H01L51/0081 ,  H01L51/5016

摘要： The present invention relates to a transition metal complex compound of a specific structure having a metal carbene bond and an organic electroluminescent device in which an organic thin film layer comprising a single layer or plural layers having at least a light emitting layer is interposed between an anode and a cathode, wherein at least one layer in the organic thin film layer contains the transition metal complex compound described above, and provided are an organic EL device having a high luminous efficiency and emitting blue light and a transition metal complex compound materializing the same.

摘要翻译： 本发明涉及具有金属卡宾键的特定结构的过渡金属络合物和有机电致发光器件，其中包含至少具有发光层的单层或多层的有机薄膜层插入在阳极 和阴极，其中有机薄膜层中的至少一层含有上述过渡金属络合物，并且提供了具有高发光效率和发出蓝光的有机EL器件和实现其的过渡金属络合物。

公开(公告)号：US07087315B2

公开(公告)日：2006-08-08

申请号：US10944863

申请日：2004-09-21

申请人： Yoshihiko Matsuo ,  Ryukichi Ikeda ,  Kimihiko Yoshida ,  Fumio Okuda

发明人： Yoshihiko Matsuo ,  Ryukichi Ikeda ,  Kimihiko Yoshida ,  Fumio Okuda

IPC分类号： B32B15/01 ,  C25D5/48

CPC分类号： H05K3/244 ,  B32B15/01 ,  C22C13/00 ,  C25D3/60 ,  C25D5/18 ,  C25D5/34 ,  H01L21/2885 ,  H01L23/49582 ,  H01L24/45 ,  H01L24/48 ,  H01L2224/29339 ,  H01L2224/32245 ,  H01L2224/45144 ,  H01L2224/48095 ,  H01L2224/48247 ,  H01L2224/73265 ,  H01L2224/92247 ,  H01L2924/01028 ,  H01L2924/01046 ,  H01L2924/01078 ,  H01L2924/01079 ,  H01L2924/14 ,  H01L2924/15747 ,  H01L2924/1576 ,  H01L2924/181 ,  H01L2924/3025 ,  H05K2203/1476 ,  Y10S428/926 ,  Y10T428/12014 ,  Y10T428/12493 ,  Y10T428/12646 ,  Y10T428/12708 ,  Y10T428/12715 ,  Y10T428/12722 ,  Y10T428/12785 ,  Y10T428/12792 ,  Y10T428/12875 ,  Y10T428/12882 ,  Y10T428/12889 ,  Y10T428/12896 ,  Y10T428/12903 ,  Y10T428/1291 ,  Y10T428/12917 ,  Y10T428/12951 ,  Y10T428/12993 ,  H01L2924/00014 ,  H01L2924/00 ,  H01L2924/00012

摘要： A method for forming a plating film, comprising the steps of: applying a plating film onto an object to be plated at a first current density for a predetermined period in a plating bath having a cathode capable of varying current and an anode and; and maintaining the object to be plated at a second current density lower than the first current density. According to the present invention, it is possible to improve solderability of a plating film for conventional lead-free solder by a simple method, which allows the productivity to further enhanced, resulting in a plating film with reduced production costs.

摘要翻译： 一种形成镀膜的方法，包括以下步骤：在具有能够改变电流的阴极和阳极的电镀浴中，将第一电流密度下的电镀膜施加到预定时间段上的镀膜; 并且以比第一电流密度低的第二电流密度来保持待镀物体。 根据本发明，可以通过简单的方法提高常规无铅焊料的镀膜的可焊性，从而可以进一步提高生产率，从而降低生产成本。

公开(公告)号：US20060115675A1

公开(公告)日：2006-06-01

申请号：US11270500

申请日：2005-11-10

申请人： Masa-aki Haga ,  Fumio Okuda

发明人： Masa-aki Haga ,  Fumio Okuda

IPC分类号： C09K11/06 ,  H01L51/54 ,  H05B33/14

CPC分类号： H01L51/0085 ,  C07F15/0033 ,  C09K11/06 ,  C09K2211/1029 ,  C09K2211/1044 ,  C09K2211/185 ,  H05B33/14 ,  Y10S428/917

摘要： A metal-complex compound which comprises a tridentate chelate ligand having a specified partial structure. An organic electroluminescence device which comprises at least one organic thin film layer sandwiched between a pair of electrode consisting of an anode and a cathode, wherein the organic thin film layer comprises the metal-complex compound, which emits light by applying an electric voltage between the pair of electrode. The present invention provides an organic EL device which emits blue light with high purity and of short wavelength with an enhanced efficiency of light emission.

摘要翻译： 一种金属络合物，其包含具有特定部分结构的三齿螯合配位体。 一种有机电致发光器件，其包括夹在由阳极和阴极组成的一对电极之间的至少一个有机薄膜层，其中所述有机薄膜层包含金属络合物，所述金属络合物通过在所述金属络合物之间施加电压而发光 一对电极。 本发明提供了发射高纯度和短波长的蓝光并提高发光效率的有机EL器件。

公开(公告)号：US07999103B2

公开(公告)日：2011-08-16

申请号：US11608494

申请日：2006-12-08

申请人： Masa-aki Haga ,  Li-fen Yang ,  Masumi Itabashi ,  Misa Ashizawa ,  Fumio Okuda

发明人： Masa-aki Haga ,  Li-fen Yang ,  Masumi Itabashi ,  Misa Ashizawa ,  Fumio Okuda

IPC分类号： C07F15/00 ,  H01L51/50

CPC分类号： H05B33/10 ,  C07F15/0033 ,  C09K11/06 ,  C09K2211/1007 ,  C09K2211/1029 ,  C09K2211/1044 ,  C09K2211/185 ,  H01L51/0085 ,  H01L51/5016

摘要： Provided are an organic electroluminescence device whose wavelength of light emission is short and which can emit blue light having a high color purity, and a metal complex compound for realizing the device. The metal complex compound is of a specific structure having a partial structure including two tridentate ligands. The organic electroluminescence device includes: a pair of electrodes; and an organic thin film layer which has one layer or a plurality of layers including at least a light emitting layer and is disposed between the pair of electrodes. In the organic electroluminescence device, at least one layer of the organic thin film layer contains the metal complex compound. The organic electroluminescence device emits light by applying a voltage between both the electrodes.

摘要翻译： 提供一种发光波长短且可以发出高纯度的蓝色光的有机电致发光元件，以及用于实现该器件的金属络合物。 金属络合物具有包含两个三齿配体的部分结构的特定结构。 有机电致发光器件包括：一对电极; 以及具有至少包含发光层并且设置在所述一对电极之间的一层或多层的有机薄膜层。 在有机电致发光器件中，有机薄膜层的至少一层含有金属络合物。 有机电致发光器件通过在两个电极之间施加电压而发光。