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11.发明授权Cure controlled catalyzed mixtures of epoxy resins and curing agents containing mesogenic moieties 失效固化受控催化的环氧树脂混合物和含有介晶部分的固化剂
公开(公告)号：US5510431A
公开(公告)日：1996-04-23
申请号：US457070
申请日：1995-06-01
IPC分类号： C08G59/00 , C08G59/18 , C08G59/22 , C08G59/32 , C08G59/40 , C08G59/68 , C09K19/38 , C08G59/06 , C08G59/10 , C08L63/00 , C08L63/02
CPC分类号： C09K19/3814 , C08G59/18 , C08G59/22 , C08G59/32 , C08G59/68 , Y10T428/1073 , Y10T442/3585 , Y10T442/67
摘要： Curable compositions containing (A) one or more epoxy resins, one (B) or more curing agents and (C) one or more cure controlling catalysts wherein at least one of components (A) or (B) or both components (A) and (B) contain a mesogenic moiety are prepared. These curable compositions permit processing at higher temperatures and improved properties. They are useful in the preparation of coatings, castings, electrical or laminates or composites and the like.
摘要翻译： 包含（A）一种或多种环氧树脂，一种（B）或更多种固化剂和（C）一种或多种固化控制催化剂的可固化组合物，其中组分（A）或（B）或组分（A）和 （B）含有介晶部分。 这些可固化组合物允许在较高温度下进行加工和改进的性能。 它们可用于制备涂料，铸件，电气或层压材料或复合材料等。
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12.发明授权Latent catalysts, epoxy compositions incorporating same, and coating, impregnating and bonding methods employing the compositions 失效潜在催化剂，包含其的环氧组合物，以及使用该组合物的涂布，浸渍和粘合方法
公开(公告)号：US5169473A
公开(公告)日：1992-12-08
申请号：US526488
申请日：1990-05-21
摘要： Products resulting from contacting (1) at least one compound selected from the group consisting of (a) at least one onium compound of the element nitrogen, phosphorus, sulfur or arsenic; (b) at least one amine compound; and (c) a mixture of any two or more of the (a) and (b) components; with (2) either (a) boric acid or (b) a mixture of boric acid and at least one acid having a weak nucleophilic anion are suitable catalysts for reacting vicinal epoxy-containing compounds with aromatic hydroxyl-containing compounds.
摘要翻译： 产生的产物（1）至少一种选自（a）至少一种元素氮，磷，硫或砷的鎓化合物的化合物的化合物; （b）至少一种胺化合物; 和（c）（a）和（b）组分中的任何两种或更多种的混合物; 与（2）（a）硼酸或（b）硼酸和至少一种具有弱亲核阴离子的酸的混合物是使含邻位环氧基的化合物与芳族含羟基化合物反应的合适的催化剂。
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公开(公告)号：US5134239A
公开(公告)日：1992-07-28
申请号：US555350
申请日：1990-07-18
CPC分类号： C08G59/00 , B29C67/246 , C08G59/02 , C08G59/066 , C08G59/40 , C08G59/621 , C08G59/68
摘要： Latent catalyst compounds for catalyzing the reaction between epoxide groups and aromatic hydroxyl groups are prepared by contacting a nitrogen-containing heterocyclic compound with an acid having a weak nucleophilic anion.
摘要翻译： 通过使含氮杂环化合物与具有弱亲核阴离子的酸接触来制备用于催化环氧基和芳族羟基之间的反应的潜在催化剂化合物。
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公开(公告)号：US4594291A
公开(公告)日：1986-06-10
申请号：US716279
申请日：1985-03-25
CPC分类号： C08G59/00 , C08G59/02 , C08G59/40 , C08G59/68 , Y10T428/31515
摘要： Relatively high molecular weight epoxy resins cured with conventional curing agents are disclosed wherein the relatively high molecular weight epoxy resin is prepared in the presence of the curing agents. The resultant cured epoxy resin has an improvement in Tg or toughness and the mixture prior to reaction and curing is much easier to apply as a coating or in the preparation of castings, laminates and the like as compared to applications of mixtures of relatively high molecular weight epoxy resins and the curing agents.
摘要翻译： 公开了用常规固化剂固化的相对高分子量的环氧树脂，其中在固化剂存在下制备相对高分子量的环氧树脂。 得到的固化环氧树脂具有Tg或韧性的改善，并且在反应和固化之前的混合物比用于相对高分子量的混合物时更容易作为涂层或用于制备铸件，层压材料等 环氧树脂和固化剂。
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公开(公告)号：US4482692A
公开(公告)日：1984-11-13
申请号：US544671
申请日：1983-10-24
申请人： James L. Bertram , William Davis , Louis L. Walker
发明人： James L. Bertram , William Davis , Louis L. Walker
CPC分类号： C08G59/26 , C08G59/04 , C08G59/066 , C08G59/3236
摘要： Epoxy resin compositions are disclosed which are the reaction products resulting from reacting (A) the reaction product of a cyanuric halide and at least one dihydric or polyhydric phenol with (B) at least one dihydric or polyhydric phenol and (C) at least one epoxy resin having an average of more than one epoxy group per molecule. These epoxy resin compositions are suitable for use as electrical laminates, structural laminates, coatings, castings, electrical encapsulation and the like.
摘要翻译： 公开了环氧树脂组合物，其是由（A）氰尿酰卤和至少一种二羟基或多元酚与（B）至少一种二元或多元酚的反应产物（A）和（C）至少一种环氧 每分子平均具有多于一个环氧基团的树脂。 这些环氧树脂组合物适用于电气层压板，结构层压板，涂层，铸件，电气封装等。
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公开(公告)号：US5503937A
公开(公告)日：1996-04-02
申请号：US192465
申请日：1994-02-07
IPC分类号： B29C67/24 , C08G59/00 , C08G59/02 , C08G59/06 , C08G59/40 , C08G59/62 , C08G59/68 , C08G59/72 , C08L63/00 , C08G59/14
CPC分类号： C08G59/72 , B29C67/246 , C08G59/00 , C08G59/02 , C08G59/066 , C08G59/40 , C08G59/62 , C08G59/621 , C08G59/68 , C08L63/00 , Y10T428/31515 , Y10T428/31522 , Y10T428/31529
摘要： A curable composition which comprises:(1) a compound which contains on average more than 1 epoxy group per molecule;(2) a compound which contains on average more than 1 phenolic hydroxyl group per molecule; and(3) a catalytic amount of a catalyst compound which contains:(a) a cation containing at least one heterocyclic nitrogen-containing ring, and(b) an anion which is a conjugate base of fluoroarsenic acid, fluoroantimonic acid, fluorophosphoric acid, chloroarsenic acid, chloroantimonic acid, chlorophosphoric acid, nitric acid, hydrofluoric acid, trifluoroacetic acid, trifluoromethane sulfonic acid, picric acid, fluoboric acid, or an acid represented by the Formula:HBR.sub.3 R' wherein each R is independently a hydrocarbyl or substituted hydrocarbyl group and R' is a halogen, a hydrocarbonoxy group, a hydrocarbonamino group, or a hydrocarbonphosphino group.
摘要翻译： 一种可固化组合物，其包含：（1）每分子平均含有多于1个环氧基的化合物; （2）每分子含有平均多于1个酚羟基的化合物; 和（3）催化量的催化剂化合物，其含有：（a）含有至少一个杂环含氮环的阳离子，和（b）作为氟代酸的共轭碱的阴离子，氟代丙二酸，氟代磷酸， 氯磺酸，氯代丙二酸，氯代磷酸，硝酸，氢氟酸，三氟乙酸，三氟甲磺酸，苦味酸，氟硼酸或由式HBR 3 R'表示的酸，其中每个R独立地为烃基或取代的烃基， R'是卤素，烃氧基，烃氨基或烃基膦基。
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17.发明授权Cure controlled catalyzed mixtures of epoxy resins and curing agents containing mesogenic moieties, B-staged and cured products therefrom 失效固化控制催化的环氧树脂和含有介晶部分的固化剂的混合物，其B级和固化产物
公开(公告)号：US5458929A
公开(公告)日：1995-10-17
申请号：US196355
申请日：1994-02-15
IPC分类号： C08G59/00 , C08G59/18 , C08G59/22 , C08G59/32 , C08G59/40 , C08G59/68 , C09K19/38 , C08L63/02 , B32B17/10 , B32B27/04
CPC分类号： C09K19/3814 , C08G59/18 , C08G59/22 , C08G59/32 , C08G59/68 , Y10T428/1073 , Y10T442/3585 , Y10T442/67
摘要： Laminates containing one or more plies of substrate material impregnated with a composition containing (A) one or more epoxy resins, (B) one or more curing agent and (C) about 0.00005 to about 0.1 mole per epoxide equivalent of cure controlling catalyst, wherein at least one of components (A) or (B) contain at least one mesogenic moiety, which, optionally, has been subjected to either (a) the application of an electric field, (b) the application of a magnetic field, (c) drawing or shear forces, or (d) any combination thereof, are prepared.
摘要翻译： 含有一种或多种浸渍有含有（A）一种或多种环氧树脂，（B）一种或多种固化剂和（C）约0.00005至约0.1摩尔/环氧当量的固化控制催化剂）的组合物的基底材料层的层压板，其中 组分（A）或（B）中的至少一种包含至少一个介晶部分，其任选地已经经受（a）施加电场，（b）施加磁场，（c ）拉伸或剪切力，或（d）其任何组合。
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公开(公告)号：US4725652A
公开(公告)日：1988-02-16
申请号：US21837
申请日：1987-03-04
CPC分类号： C08G59/00 , C08G59/02 , C08G59/40 , C08G59/68 , Y10T428/31515
摘要： Latent catalysts for epoxy reactions are prepared by reacting a tetrasubstituted onium compound such as tetrabutylphosphonium acetate.acetic acid complex or an amine compound with an acid having a weak-nucleophilic anion such as fluoboric acid. These catalysts provide stable latent catalysts for epoxy resins for advancement or curing reactions.
摘要翻译： 用于环氧反应的潜在催化剂是通过使四取代的鎓化合物如乙酸四丁基乙酸盐，乙酸络合物或胺化合物与具有弱亲核阴离子的酸如氟硼酸反应来制备的。 这些催化剂为环氧树脂提供稳定的潜在催化剂用于进行或固化反应。
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公开(公告)号：US4665149A
公开(公告)日：1987-05-12
申请号：US796368
申请日：1985-11-08
申请人： James L. Bertram , Louis L. Walker
发明人： James L. Bertram , Louis L. Walker
CPC分类号： C08G59/3245 , C08G59/063
摘要： The thermal stability of epoxy resins prepared by dehydrohalogenating the reaction product of an epihalohydrin with an adduct prepared from a cyanuric halide and a polyhydric aromatic compound is improved by employing as the polyhydric aromatic compound one which is substituted with a hydrocarbyl group, a halogen atom or a nitro group at each ortho position relative to each aromatic hydroxyl group. These epoxy resins are useful in coating and molding compositions and in the preparation of laminates and composites.
摘要翻译： 通过使用由烃基，卤素原子或卤素原子取代的多元芳香族化合物，改善了由表卤代醇与由氰尿酰卤和多元芳香族化合物制备的加成物的反应产物脱卤化氢制备的环氧树脂的热稳定性， 在每个邻位相对于每个芳族羟基的硝基。 这些环氧树脂可用于涂料和模塑组合物以及制备层压材料和复合材料。
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20.发明授权Method for fractioning poly (ethylene oxide) formed using a metallic cyanide catalyst 有权使用金属氰化物催化剂分离聚（环氧乙烷）的方法公开(公告)号：US06552163B1
公开(公告)日：2003-04-22
申请号：US09611497
申请日：2000-07-07
IPC分类号： C08G5968
CPC分类号： C08G65/30 , C08G65/2663 , Y02P20/584
摘要： A poly(ethylene oxide) polymer having low and high molecular weight fractions is fractionated by dissolving the polymer in a solvent for the low molecular weight fraction. A good separation of the low and high molecular weight fractions can be obtained. When the poly(ethylene oxide) polymer contains a metal cyanide catalyst, this process also provides a good separation of the catalyst from the low molecular weight fraction. In this instance, the catalyst remains active and the high molecular weight fraction containing the catalyst can be recycled into subsequent polymerization processes.
摘要翻译： 通过将聚合物溶解在低分子量级分的溶剂中来分级具有低和高分子量级分的聚（环氧乙烷）聚合物。 可以获得低分子量和高分子量级分的良好分离。 当聚（环氧乙烷）聚合物含有金属氰化物催化剂时，该方法还提供了催化剂与低分子量级分的良好分离。 在这种情况下，催化剂保持活性，并且含有催化剂的高分子量级分可以再循环到随后的聚合方法中。
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