摘要:
A shell-and-tube reactor is disclosed. Contact tubes are disposed within a cylindrical housing and are secured to tube plates. Gas and liquid phases are received via a feed opening in a lower end cap and discharged via an upper end cap in the housing. A distributor device for a gas phase/liquid phase mixture is disposed below the lowermost tube plate. The distributor device includes a distributor plate and a predistributor. The distributor plate is arranged horizontally within the housing and includes an active area having through-openings and a downward-extending margin, but does not extend over the entire cross section of the housing. The predistributor includes a second distributor plate disposed between the feed opening and the first distributor plate, wherein the second distributor plate includes a second active area with second through-openings and a second downward-extending margin.
摘要:
A process for a continuous production of a polyetherol first involves reacting a catalyst (5) with an alcohol starter (3) or an alkoxylated precursor, to give a mixture comprising an alcoholate and water. Water is then removed from the mixture. The process further involves feeding the alcoholate into a bubble column and feeding an alkylene oxide into the bottom of a compartment of the bubble column, such that the alkylene oxide rises in the alcoholate. The alkylene oxide then reacts with the alcoholate or a secondary product from the reaction between the alcoholate and alkylene oxide, to give the polyetherol.
摘要:
A process for a continuous production of a polyetherol first involves reacting an alcohol with a starter or an alkoxylated precursor, to give a mixture comprising an alcoholate and water. Water is then removed from the mixture. The process further involves feeding the alcoholate into a bubble column and feeding an alkylene oxide into the bottom of a compartment of the bubble column, such that the alkylene oxide rises in the alcoholate. The alkylene oxide then reacts with the alcoholate or a secondary product from the reaction between the alcoholate and alkylene oxide, to give the polyetherol.
摘要:
The invention relates to a device for fine machining workpieces, preferably for honing and/or fineboring cylinder bores in crankcases of internal combustion engines, wherein inside a module (1) one or two horizontally displaceable machining units (10, 11, 12, 13) each are provided on two longitudinal sides (2, 3) that are opposite each other for honing and/or fineboring. Each machining unit (10, 11, 12, 13) comprises a spindle (100), a drive for creating the oscillating stroke movement of the spindle (100) and for displacing the machining unit into the working position, a tool holder (8) with a rigid axis, and a feed device (60, 61, 62, 63, 64) for the radial feeding of the machining tools, and between the longitudinal sides equipped with the machining units (10, 11, 12, 13) a service chamber (7) that can be accessed from an end side, wherein at least one tool magazine (30, 31) is associated with the machining units (10, 11, 12, 13) at the rear end side (4) of the module (1).
摘要:
A reactor (1) for gas/liquid or gas/liquid/solid reactions having a vertical longitudinal axis and an inlet (2) for a liquid or liquid/solid feed stream in the upper region of the reactor and an inlet (3) for a gaseous stream in the lower region of the reactor (1), wherein the gaseous stream (3) is conveyed through a gas distributor module (9) which is made up exclusively of straight tube sections (14, 15).
摘要:
A shell-and-tube reactor is disclosed. Contact tubes are disposed within a cylindrical housing and are secured to tube plates. Gas and liquid phases are received via a feed opening in a lower end cap and discharged via an upper end cap in the housing. A distributor device for a gas phase/liquid phase mixture is disposed below the lowermost tube plate. The distributor device includes a distributor plate and a predistributor. The distributor plate is arranged horizontally within the housing and includes an active area having through-openings and a downward-extending margin, but does not extend over the entire cross section of the housing. The predistributor includes a second distributor plate disposed between the feed opening and the first distributor plate, wherein the second distributor plate includes a second active area with second through-openings and a second downward-extending margin.
摘要:
The continuous or quasi-continuous process for lightening organic polyisocyanates with ozone-containing gas, the treatment of the organic polyisocyanate being effected with an ozone-containing gas which furthermore comprises at least one further inert and/or reactive gas can be carried out, according to the invention, in a stirred tank with connected storage tank, in a sieve tray column or in a packed column.
摘要:
Distributor device (1) for a gas phase/liquid phase mixture for an apparatus (2) into whose interior a gas phase and a liquid phase are introduced via at least one feed opening (4), wherein the distributor device (1) comprises a horizontal plate (5) and vertical elements (6) which conduct the liquid phase and are arranged thereon and are open in the upstream direction and project outward in the direction of the feed opening (4) through the gas cushion formed, with at least one opening (10) for the gas phase being provided on the circumference of the elements (6) which conduct the liquid phase in the region of the gas cushion formed and at least one opening (11) for the liquid phase.