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    Method and device for analyzing the hardening of hardenable formulations
    2.
    发明申请
    Method and device for analyzing the hardening of hardenable formulations 审中-公开
    用于分析可硬化制剂硬化的方法和装置

    公开(公告)号：US20050000274A1

    公开(公告)日：2005-01-06

    申请号：US10491423

    申请日：2002-09-27

    Applicant: Wolfgang Schrof ,  Thorsten Muller ,  Sebastian Koltzenburg ,  Matthias Kroner ,  Stephan Lehmann ,  Joachim Hadeler

    Inventor： Wolfgang Schrof ,  Thorsten Muller ,  Sebastian Koltzenburg ,  Matthias Kroner ,  Stephan Lehmann ,  Joachim Hadeler

    IPC: G01N11/00 ,  G01N3/00 ,  G01N3/06 ,  G01N3/42 ,  G01N3/48

    CPC classification number: G01N3/42 ,  G01N2203/0092 ,  G01N2203/0682

    Abstract: The invention relates to a process for the combinatorial investigation of the hardening of hardenable liquid or viscous formulations (a) in which n hardenable formulations are prepared in parallel in n containers, and (b) the degree of hardening is determined at least once on each of the n formulations by inserting a measurement tip into the formulation with a certain force and measuring the maximum penetration depth achieved as a measure of the degree of hardening of this formulation, and (c) for in each case one composition of the formulations, one or more parameters that are characteristic of the kinetics of hardening are determined from the measurement values for the penetration depth at various times after preparation of the formulations. Steps (a) to (c) are preferably carried out a number of times, and a dependence of the characteristic parameter(s) on the composition of the formulations is determined by analysis of the large number of individual values obtained in this way for the parameter(s) that is (are) characteristic of the kinetics of hardening, enabling the composition of the formulations to be optimized with respect to its hardening behavior.

    Abstract translation: 本发明涉及用于组合研究可硬化液体或粘性制剂（a）的硬化的方法，其中在n个容器中并行制备n个可硬化制剂，和（b）硬化程度每个至少确定一次 通过以一定的力将测量尖端插入制剂中并测量作为该制剂的硬化程度的度量而获得的最大穿透深度，以及（c）在每种情况下，制剂的一种组合物，一种 或者从制剂配制后的不同时刻的穿透深度的测定值求出硬化动力学特征的更多的参数。 步骤（a）至（c）优选进行多次，并且通过分析以这种方式获得的大量个体值来确定特征参数对制剂组成的依赖性 硬化动力学特征的参数，使组合物能够根据其硬化行为进行优化。

    Use of modified polyaspartic acids in washing agents
    5.
    发明授权
    Use of modified polyaspartic acids in washing agents 失效
    在洗涤剂中使用改性聚天冬氨酸

    公开(公告)号：US6001798A

    公开(公告)日：1999-12-14

    申请号：US29247

    申请日：1998-03-04

    Applicant: Richard Baur ,  Werner Bertleff ,  Hans-Ulrich Jager ,  Angelika Funhoff ,  Matthias Kroner ,  Gunnar Schornick

    Inventor： Richard Baur ,  Werner Bertleff ,  Hans-Ulrich Jager ,  Angelika Funhoff ,  Matthias Kroner ,  Gunnar Schornick

    IPC: C08G69/36 ,  C08G73/06 ,  C08G73/10 ,  C11D3/37 ,  C11D17/00

    CPC classification number: C08G73/1092 ,  C11D3/3719

    Abstract: The use of modified polyaspartic acids which are obtainable by polycondensation of aspartic acid in the presence of, in each case based on the aspartic acid employed,(a) 2.5 to 25 mol % of amines with at least 6 carbon atoms(b) at least 2% by weight of phosphoric acid, phosphorous acid, hypophosphorous acid, polyphosphoric acids, phosphorus pentoxide, phosphonic acids or mixtures of said acids,at temperatures of at least 120.degree. C. and subsequent hydrolysis with bases to give modified polyaspartic acids with a phosphorus content of from 0.5 to 10% by weight, as additive to detergents, and detergents which contain the modified polyaspartic acids in amounts of from 0.1 to 20% by weight.

    Abstract translation: PCT No.PCT / EP96 / 03797 371日期：1998年3月4日 102（e）1998年3月4日PCT PCT 1996年8月29日PCT公布。 出版物WO97 / 09409 日期1997年3月13日使用通过天冬氨酸缩聚获得的改性聚天冬氨酸，在每种情况下，基于所使用的天冬氨酸，（a）2.5至25mol％具有至少6个碳原子的胺 （b）在至少120℃的温度下至少2重量％的磷酸，亚磷酸，次磷酸，多磷酸，五氧化二磷，膦酸或所述酸的混合物，随后用碱水解，得到改性的 磷含量为0.5〜10重量％的聚天冬氨酸，作为洗涤剂的添加剂，以及含有0.1〜20重量％的改性聚天冬氨酸的洗涤剂。

    Preparation of salts of polyaspartic acid and their use in detergents and cleaners
    6.
    发明授权
    Preparation of salts of polyaspartic acid and their use in detergents and cleaners 失效
    聚天冬氨酸盐的制备及其在洗涤剂和清洁剂中的应用

    公开(公告)号：US5886137A

    公开(公告)日：1999-03-23

    申请号：US776524

    申请日：1997-02-27

    Applicant: Matthias Kroner ,  Gunnar Schornick ,  Uwe Strotmann ,  Volker Schwendemann ,  Thomas Meyer ,  Alfons Ludwig

    Inventor： Matthias Kroner ,  Gunnar Schornick ,  Uwe Strotmann ,  Volker Schwendemann ,  Thomas Meyer ,  Alfons Ludwig

    IPC: C08G69/10 ,  C02F5/12 ,  C08G73/10 ,  C11D3/37 ,  C08G63/44 ,  C08G73/00

    CPC classification number: C02F5/12 ,  C08G73/1092 ,  C11D3/3719

    Abstract: A process for preparing salts of polyaspartic acid by treating polycondensates in aqueous medium with bases, employing at least 0.7 equivalent of an alkali metal and/or alkaline earth metal base per mole of the aspartimide, aspartic acid and/or aspartamide units present in the polycondensates, and the bases being added within from 30 min to 20 hours to an aqueous suspension of polycondensates of aspartic acid which has been heated to 40.degree.-140.degree. C., and the reaction mixture being allowed to react further where appropriate, and the use of alkali metal and/or alkaline earth metal salts of polyaspartic acids obtainable by treating polycondensates of aspartic acid in aqueous medium with more than 1 equivalent of an alkali metal and/or alkaline earth metal base, with the molecular weight of the polycondensates being reduced, as additive to detergents and cleaners.

    Abstract translation: PCT No.PCT / EP95 / 03224 Sec。 371日期1997年2月27日 102（e）日期1997年2月27日PCT提交1995年8月16日PCT公布。 出版物WO96 / 06879 日期1996年3月7日一种通过在水性介质中用碱处理缩聚物来制备聚天冬氨酸盐的方法，每摩尔天冬氨酰亚胺，天冬氨酸和/或天冬氨酰胺使用至少0.7当量碱金属和/或碱土金属碱 存在于缩聚物中的单元，并将碱在30分钟至20小时内加入已加热至40-140℃的天冬氨酸缩聚物的水性悬浮液，并使反应混合物进一步反应其中 适当地使用聚天冬氨酸的碱金属和/或碱土金属盐，其可以通过在水性介质中用多于1当量的碱金属和/或碱土金属碱处理天冬氨酸的缩聚物而获得，分子量为 减缩的缩聚物作为洗涤剂和清洁剂的添加剂。

    Process for preparing cocondensates of aspartic acid amines
    10.
    发明授权
    Process for preparing cocondensates of aspartic acid amines 失效
    制备天冬氨酸胺缩合物的方法

    公开(公告)号：US06063961A

    公开(公告)日：2000-05-16

    申请号：US147370

    申请日：1998-12-10

    Applicant: Matthias Kroner

    Inventor： Matthias Kroner

    IPC: C08G69/10 ,  C08G73/10 ,  C07C231/02 ,  C08F20/54

    CPC classification number: C08G73/1092

    Abstract: A process for preparing cocondensates of aspartic acid and amines by heating aspartic acid and amines in the presence of acidic catalysts comprises supplying the feed region of the extruder with particulate aspartic acid and a downstream metering zone with at least one amine and at least one acidic catalyst, condensing the resulting mixture to such an extent by heating that the downstream end of the extruder discharges a precondensate which contains at least 20-95% by weight of the starting aspartic acid in condensed form, and then completing the condensation of the precondensate. The cocondensates are useful as incrustation inhibitors in detergents.

    Abstract translation: PCT No.PCT / EP97 / 03751 Sec。 371 1998年12月10日第 102（e）日期1998年12月10日PCT 1997年7月14日PCT公布。 第WO98 / 04613号公报 日本1998年2月5日在酸性催化剂存在下，通过加热天冬氨酸和胺来制备天冬氨酸和胺的缩合物的方法包括将挤出机的进料区域供给至少一种胺的颗粒天冬氨酸和下游计量区， 至少一种酸性催化剂，通过加热将所得混合物冷凝至这样的程度，使得挤出机的下游端排出包含至少20-95重量％浓缩形式的起始天冬氨酸的预缩合物，然后完成冷凝 的预缩合物。 共缩合物可用作洗涤剂中的结垢抑制剂。

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