Packing brick and method of constructing packing bed in exchange column
using same
    11.
    发明授权
    Packing brick and method of constructing packing bed in exchange column using same 失效
    包装砖和使用相同方式在交换柱中构建包装床

    公开(公告)号:US5997173A

    公开(公告)日:1999-12-07

    申请号:US257159

    申请日:1999-02-24

    摘要: A plurality of structured packing bricks are positioned in a column having a longitudinal axis to form one or more structured packing beds. Each brick is formed from a plurality of corrugated plates disposed in parallel relation and having opposed ends that form end surfaces of the bricks. At least one end surface, and normally both end surfaces, of the bricks are inclined at an angle to the column axis so each brick has an end surface that engages and overlaps the inclined end surface of a horizontally adjacent brick. The inclined end surfaces include openings formed by the plate corrugations and, due to the overlapping positioning of adjacent end surfaces, liquid is able to flow vertically downwardly from openings in one brick end surface into openings in the adjacent brick end surface. These angle end surfaces also disrupt the vertical flow of vapor so that vertical channeling of vapor along the end surfaces is disrupted. The shape of the packing bricks can include trapezoidal and parallelogram.

    摘要翻译: 多个规整填料砖定位在具有纵向轴线的柱中以形成一个或多个规整填料床。 每个砖由平行布置的多个波纹板形成,并且具有形成砖的端面的相对端。 砖的至少一个端面,通常两个端面都倾斜成与柱轴线成一定角度,因此每个砖具有与水平相邻的砖的倾斜端面接合和重叠的端面。 倾斜的端面包括由板波纹形成的开口,并且由于相邻端面的重叠定位,液体能够从一个砖端面中的开口垂直向下流动到相邻砖端面中的开口。 这些角度的端面也破坏了蒸气的垂直流动,使得沿着端面的蒸气的垂直通道被破坏。 包装砖的形状可以包括梯形和平行四边形。

    Vapor-liquid contact tray and downcomer assembly and method employing
same
    12.
    发明授权
    Vapor-liquid contact tray and downcomer assembly and method employing same 失效
    蒸汽 - 液体接触盘和降液管组件及其使用方法

    公开(公告)号:US5480595A

    公开(公告)日:1996-01-02

    申请号:US234188

    申请日:1994-04-28

    摘要: A vapor-liquid contact tray and downcomer assembly is provided with louvres which serve to impart a horizontal directional flow to the liquid exiting the downcomer and/or the vapor passing through the tray. The downcomer includes a bottom plate which closes the outlet region of the downcomer and includes a plurality of louvres presenting generally vertical openings in the direction of liquid flow across the underlying tray. The downcomer receiving area in the underlying tray can include similar louvres. The louvres redirect the vertical momentum of the liquid and vapor streams to a generally horizontal momentum as the liquid exits the downcomer and as the vapor rises through the tray. In other embodiments, the louvres in either the bottom plate or the downcomer receiving area of the tray are replaced with apertures which do not block the vertical momentum of the stream passing through the apertures. An enhanced vapor-liquid active area on the tray results from the use of the louvres.

    摘要翻译: 气液接触托盘和降液管组件设置有百叶窗,其用于向离开降液管的液体和/或通过托盘的蒸汽赋予水平定向流。 降液管包括封闭降液管的出口区域的底板,并且包括多个百叶窗,所述多个百叶窗在液体流动方向上大体垂直地穿过下面的托盘。 底层托盘中的降液管接收区域可以包括类似的百叶窗。 当液体离开降液管并且蒸汽通过托盘升高时,百叶窗将液体和蒸气流的垂直动量重定向到大体上水平的动量。 在其他实施例中,托盘的底板或降液管接收区域中的百叶窗被不被阻挡穿过孔的流的垂直动量的孔所代替。 托盘上增强的气液活性区域是由于使用百叶窗而产生的。

    Recovery of methacrolein
    13.
    发明授权
    Recovery of methacrolein 失效
    甲基丙烯醛的回收

    公开(公告)号:US4234519A

    公开(公告)日:1980-11-18

    申请号:US6824

    申请日:1979-01-26

    摘要: In the catalytic oxidation of isobutylene and/or tertiary butyl alcohol to methacrolein, the product methacrolein is recovered as an aqueous solution, which thereafter is stripped of methacrolein by contacting the solution with recycle gases from the subsequent oxidation of methacrolein to methacrylic acid. In a preferred embodiment, the oxidation reactor effluent gases are quenched to near ambient temperatures by direct contact with a recirculating stream of partially condensed effluent to provide an aqueous solution of methacrolein and thereafter the methacrolein remaining in the effluent gases is absorbed into a refrigerated water stream to provide a second aqueous solution. The aqueous solutions are combined and stripped by recycle gases, thereby supplying methacrolein as feed to the subsequent oxidation process.

    摘要翻译: 在异丁烯和/或叔丁醇向异丁烯醛的催化氧化中,产物甲基丙烯醛作为水溶液回收,然后通过使溶液与随后的甲基丙烯醛氧化成甲基丙烯酸的循环气体相接触而除去甲基丙烯醛。 在优选的实施方案中,氧化反应器流出气体通过与部分冷凝的流出物的再循环流直接接触而淬灭到接近环境温度,以提供甲基丙烯醛的水溶液,此后残存在流出气体中的甲基丙烯醛被吸收到冷冻水流 以提供第二水溶液。 将水溶液合并并通过再循环气体汽提,从而将甲基丙烯醛作为进料提供给随后的氧化过程。

    Apparatus for concurrent reaction with distillation
    14.
    发明授权
    Apparatus for concurrent reaction with distillation 失效
    与蒸馏同时反应的装置

    公开(公告)号:US5855741A

    公开(公告)日:1999-01-05

    申请号:US376046

    申请日:1995-01-19

    摘要: A column having a region for reaction with distillation of fluid streams is provided with structures including catalyst-filled containers having liquid permeable upper surfaces which allow for the accumulation and flow of liquid from a liquid stream. The containers include catalyst beds positioned beneath the upper surface of the containers. A portion of the liquid on the containers is driven through the catalyst bed by the liquid head created by the accumulated liquid and is catalytically reacted. Another portion of the liquid may be directed through a downcomer which allows the accumulated liquid to leave the container without passing through the catalyst bed so that higher volumetric flow rates can be achieved.

    摘要翻译: 具有用于与流体流的蒸馏反应的区域的塔被提供有包括具有液体可渗透上表面的催化剂填充容器的结构,其允许来自液体流的液体的积聚和流动。 容器包括位于容器上表面下方的催化剂床。 容器中的液体的一部分通过催化剂床被积聚的液体产生的液体头驱动并被催化反应。 液体的另一部分可以被引导通过降液管,其允许积聚的液体离开容器而不通过催化剂床,使得可以实现更高的体积流速。

    Liquid collector-distributor device, system and method
    16.
    发明授权
    Liquid collector-distributor device, system and method 失效
    液体收集器 - 分配器,系统和方法

    公开(公告)号:US5645770A

    公开(公告)日:1997-07-08

    申请号:US634656

    申请日:1996-04-18

    IPC分类号: B01D3/00 B01F3/04

    CPC分类号: B01F3/04078 B01D3/008

    摘要: An integral collector-distributor device including chimney hats and adapted for use in a gas-liquid exchange column to promote radial mixing of a liquid on a distributor tray surface. The collector-distributor device includes a tray having a tray surface adapted to extend generally horizontally across the cross-sectional area of the column to collect downwardly flowing liquid. A plurality of gas risers on the tray permit the upward movement of an upwardly flowing gas through the tray, and a plurality of liquid distributors permit the generally uniform distribution of the collected downwardly flowing liquid to a lower section of the column. A plurality of chimney hats, each having an upper surface and a one and other end, extend over and above at least a portion of the gas risers, are angularly inclined from the horizontal, or are horizontal, collect downwardly flowing liquid on the upper surface and permit the collected liquid on the upper surface to flow away from the point of liquid collection to another section of the tray to promote improved liquid mixing across the tray surface and to reduce liquid concentration gradients on the tray surface. The chimney hats are of a selected width, wider that the width of the gas risers, to provide for minimal space between each adjacent chimney hat. The wide chimney hats, particularly where horizontal, may also be of different selected vertical heights to permit the upward flow of gas.

    摘要翻译: 一种整体收集器 - 分配器装置,其包括烟囱帽并且适用于气液交换塔以促进液体在分配器托盘表面上的径向混合。 集电器 - 分配器装置包括具有托盘表面的托盘,该托盘表面适于大致水平延伸穿过塔的横截面积以收集向下流动的液体。 托盘上的多个气体提升器允许向上流动的气体通过托盘向上运动,并且多个液体分配器允许收集的向下流动的液体大致均匀地分布到塔的下部。 多个烟囱,每个具有上表面和一个和另一端,在气体立管的至少一部分上方延伸并且在其上方,从水平面倾斜倾斜或水平地收集向上流动的液体在上表面 并允许上表面上的收集液体从液体收集点流出到托盘的另一部分,以促进跨越托盘表面的改进的液体混合并减少托盘表面上的液体浓度梯度。 烟囱帽具有选定的宽度,使气体立管的宽度更宽,从而在每个相邻的烟囱帽之间提供最小的空间。 宽的烟囱,特别是水平的烟囱,也可能具有不同的垂直高度,以允许气体向上流动。

    Nested packing for distillation column
    17.
    发明授权
    Nested packing for distillation column 失效
    用于蒸馏塔的嵌套填料

    公开(公告)号:US5413741A

    公开(公告)日:1995-05-09

    申请号:US203876

    申请日:1994-03-01

    IPC分类号: B01J19/32 F28F25/08 B01F3/04

    摘要: A plurality of corrugated plates are arranged in parallel relationship with corrugations in adjacent plates extending in a criss-crossing pattern to form a packing element for a heat exchange or mass transfer column. The plates are spaced closer together by providing reliefs in adjacent plates at the points of intersection between the criss-crossing corrugations. The reliefs allow the corrugations on the adjacent plates to extend into each other to reduce the spacing between the plates. The reliefs may be in the form of apertures or recesses.

    摘要翻译: 多个波纹板与相邻板中的波纹平行地布置成以交叉图案延伸形成用于热交换或传质柱的填充元件。 通过在交叉波纹之间的相交点处在相邻的板中提供浮雕,使板彼此靠近在一起。 浮雕允许相邻板上的波纹彼此延伸以减小板之间的间隔。 凹凸可以是孔或凹槽的形式。

    Gas-liquid contact column with improved mist eliminator and method
    18.
    发明授权
    Gas-liquid contact column with improved mist eliminator and method 失效
    气体 - 液体接触柱与改进的雾化消解器和方法

    公开(公告)号:US5139544A

    公开(公告)日:1992-08-18

    申请号:US601909

    申请日:1990-10-22

    摘要: A gas-liquid column and method having improved mist elimination particularly for the treatment of corrosive fluids which comprises directly introducing a liquid from a liquid distributor resting on a top structured packing layer into the upright flow passage of the structured packing to provide the initial gas-liquid contact within the top structured packing layer, thereby reducing mist and spray and particularly useful where corrosive fluids are used.

    摘要翻译: 一种气液柱和方法,特别是用于处理腐蚀性流体的具有改进的除雾,包括将液体从搁置在顶部规整填料层上的液体分配器直接引入到规定填料的直立流动通道中,以提供初始气体 - 在顶部规整填料层内液体接触,从而减少雾气和喷雾,特别是在使用腐蚀性流体时尤其有用。

    Saddle structure for reactive distillation
    20.
    发明授权
    Saddle structure for reactive distillation 失效
    用于反应蒸馏的鞍形结构

    公开(公告)号:US06565816B1

    公开(公告)日:2003-05-20

    申请号:US08881969

    申请日:1997-06-25

    IPC分类号: B01F300

    摘要: A hollow, saddle-shaped packing structure 14 includes a pair of porous outer and inner semi-cylindrical side walls 22, 34 that are spaced from one another to define an interior space 40, and a particulate catalyst component 20 retained in the interior space between the side walls. The packing structure may be formed by a pair of saddle-shaped shell elements 16, 18, each of which presents one of the side walls and a pair of radially opposed laterally extending flanges 26, 38. The flanges are connected together by tabs 30, 32, welding, or the like, and the interior space between axially spaced marginal edges 24, 36 of the outer and inner shell elements is closed off to retain the particulate catalyst component between the side walls.

    摘要翻译: 中空的马鞍形填料结构14包括彼此间隔开以限定内部空间40的一对多孔外部和内部半圆柱形侧壁22,34,以及保持在内部空间中的颗粒状催化剂组分20 侧墙。 包装结构可以由一对鞍状壳体元件16,18形成,每个鞍形壳体元件16,18分别具有一个侧壁和一对径向相对的横向延伸的凸缘26,38。凸缘通过凸片30连接在一起, 32,焊接等,并且外壳和内壳元件的轴向间隔的边缘24,36之间的内部空间被封闭以将颗粒催化剂组分保持在侧壁之间。