摘要:
A plurality of structured packing bricks are positioned in a column having a longitudinal axis to form one or more structured packing beds. Each brick is formed from a plurality of corrugated plates disposed in parallel relation and having opposed ends that form end surfaces of the bricks. At least one end surface, and normally both end surfaces, of the bricks are inclined at an angle to the column axis so each brick has an end surface that engages and overlaps the inclined end surface of a horizontally adjacent brick. The inclined end surfaces include openings formed by the plate corrugations and, due to the overlapping positioning of adjacent end surfaces, liquid is able to flow vertically downwardly from openings in one brick end surface into openings in the adjacent brick end surface. These angle end surfaces also disrupt the vertical flow of vapor so that vertical channeling of vapor along the end surfaces is disrupted. The shape of the packing bricks can include trapezoidal and parallelogram.
摘要:
A vapor-liquid contact tray and downcomer assembly is provided with louvres which serve to impart a horizontal directional flow to the liquid exiting the downcomer and/or the vapor passing through the tray. The downcomer includes a bottom plate which closes the outlet region of the downcomer and includes a plurality of louvres presenting generally vertical openings in the direction of liquid flow across the underlying tray. The downcomer receiving area in the underlying tray can include similar louvres. The louvres redirect the vertical momentum of the liquid and vapor streams to a generally horizontal momentum as the liquid exits the downcomer and as the vapor rises through the tray. In other embodiments, the louvres in either the bottom plate or the downcomer receiving area of the tray are replaced with apertures which do not block the vertical momentum of the stream passing through the apertures. An enhanced vapor-liquid active area on the tray results from the use of the louvres.
摘要:
In the catalytic oxidation of isobutylene and/or tertiary butyl alcohol to methacrolein, the product methacrolein is recovered as an aqueous solution, which thereafter is stripped of methacrolein by contacting the solution with recycle gases from the subsequent oxidation of methacrolein to methacrylic acid. In a preferred embodiment, the oxidation reactor effluent gases are quenched to near ambient temperatures by direct contact with a recirculating stream of partially condensed effluent to provide an aqueous solution of methacrolein and thereafter the methacrolein remaining in the effluent gases is absorbed into a refrigerated water stream to provide a second aqueous solution. The aqueous solutions are combined and stripped by recycle gases, thereby supplying methacrolein as feed to the subsequent oxidation process.
摘要:
A column having a region for reaction with distillation of fluid streams is provided with structures including catalyst-filled containers having liquid permeable upper surfaces which allow for the accumulation and flow of liquid from a liquid stream. The containers include catalyst beds positioned beneath the upper surface of the containers. A portion of the liquid on the containers is driven through the catalyst bed by the liquid head created by the accumulated liquid and is catalytically reacted. Another portion of the liquid may be directed through a downcomer which allows the accumulated liquid to leave the container without passing through the catalyst bed so that higher volumetric flow rates can be achieved.
摘要:
A packing section includes a plurality of vertically oriented, diagonally cross-corrugated packing sheets defining a section height. The section height has a base region, a bulk region, and a top region. The base region has a first particular geometry different from the geometry of the bulk region. The top region has a second particular geometry different from the geometry of the bulk region, and different from the first particular geometry of the base region.
摘要:
An integral collector-distributor device including chimney hats and adapted for use in a gas-liquid exchange column to promote radial mixing of a liquid on a distributor tray surface. The collector-distributor device includes a tray having a tray surface adapted to extend generally horizontally across the cross-sectional area of the column to collect downwardly flowing liquid. A plurality of gas risers on the tray permit the upward movement of an upwardly flowing gas through the tray, and a plurality of liquid distributors permit the generally uniform distribution of the collected downwardly flowing liquid to a lower section of the column. A plurality of chimney hats, each having an upper surface and a one and other end, extend over and above at least a portion of the gas risers, are angularly inclined from the horizontal, or are horizontal, collect downwardly flowing liquid on the upper surface and permit the collected liquid on the upper surface to flow away from the point of liquid collection to another section of the tray to promote improved liquid mixing across the tray surface and to reduce liquid concentration gradients on the tray surface. The chimney hats are of a selected width, wider that the width of the gas risers, to provide for minimal space between each adjacent chimney hat. The wide chimney hats, particularly where horizontal, may also be of different selected vertical heights to permit the upward flow of gas.
摘要:
A plurality of corrugated plates are arranged in parallel relationship with corrugations in adjacent plates extending in a criss-crossing pattern to form a packing element for a heat exchange or mass transfer column. The plates are spaced closer together by providing reliefs in adjacent plates at the points of intersection between the criss-crossing corrugations. The reliefs allow the corrugations on the adjacent plates to extend into each other to reduce the spacing between the plates. The reliefs may be in the form of apertures or recesses.
摘要:
A gas-liquid column and method having improved mist elimination particularly for the treatment of corrosive fluids which comprises directly introducing a liquid from a liquid distributor resting on a top structured packing layer into the upright flow passage of the structured packing to provide the initial gas-liquid contact within the top structured packing layer, thereby reducing mist and spray and particularly useful where corrosive fluids are used.
摘要:
A packing section includes a plurality of vertically oriented, diagonally cross-corrugated packing sheets defining a section height. The section height has a base region, a bulk region, and a top region. The base region has a first particular geometry different from the geometry of the bulk region.
摘要:
A hollow, saddle-shaped packing structure 14 includes a pair of porous outer and inner semi-cylindrical side walls 22, 34 that are spaced from one another to define an interior space 40, and a particulate catalyst component 20 retained in the interior space between the side walls. The packing structure may be formed by a pair of saddle-shaped shell elements 16, 18, each of which presents one of the side walls and a pair of radially opposed laterally extending flanges 26, 38. The flanges are connected together by tabs 30, 32, welding, or the like, and the interior space between axially spaced marginal edges 24, 36 of the outer and inner shell elements is closed off to retain the particulate catalyst component between the side walls.