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    METHOD FOR PRODUCING RUTHENIUM COMPLEX
    12.
    发明申请
    METHOD FOR PRODUCING RUTHENIUM COMPLEX 有权
    生产金属复合材料的方法

    公开(公告)号：US20120016148A1

    公开(公告)日：2012-01-19

    申请号：US13138709

    申请日：2010-03-18

    申请人： Takahiro Fujiwara ,  Hideki Nara

    发明人： Takahiro Fujiwara ,  Hideki Nara

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0046 ,  C07F17/02

    摘要： The present invention provides a method for inexpensively producing di-μ-chloro-bis[chloro(η6-1-isopropyl-4-methylbenzene)ruthenium (II)] complex used as a catalyst raw material for a hydrogenation or metathesis polymerization reaction at a high yield. In the present invention, the above-described problem can be solved by reacting ruthenium chloride or a hydrate thereof with γ-terpinene in a solvent. In particular, by using an alcohol having a boiling point of 100° C. or higher as a solvent, the yield of the above-described complex can be increased.

    摘要翻译： 本发明提供了一种廉价生产用作氢化或易位聚合反应的催化剂原料的二 - 氯 - 双[氯（＆eegr; 6-1-异丙基-4-甲苯）钌（II）]络合物的方法 以高产量。 在本发明中，上述问题可以通过使氯化钌或其水合物与γ-萜品烯在溶剂中反应来解决。 特别是通过使用沸点为100℃以上的醇作为溶剂，可以提高上述络合物的收率。

    Process for the production of optically active amino alcohols
    13.
    发明授权
    Process for the production of optically active amino alcohols 失效
    用于制备光学活性氨基醇的方法

    公开(公告)号：US07038087B2

    公开(公告)日：2006-05-02

    申请号：US10656617

    申请日：2003-09-04

    申请人： Takahiro Fujiwara ,  Hideki Nara ,  Tsukasa Sotoguchi

    发明人： Takahiro Fujiwara ,  Hideki Nara ,  Tsukasa Sotoguchi

    IPC分类号： C07C209/16 ,  C07C209/46 ,  C07C209/56

    CPC分类号： C07C269/00 ,  C07B2200/07 ,  C07C213/02 ,  C07C2601/08 ,  C07C2601/14 ,  Y02P20/55 ,  C07C215/44 ,  C07C271/24

    摘要： An object of the present invention is to provide a process for the production of an optically active amino alcohol, particularly an optically active amino alcohol of a trans-form, being excellent in economy and efficiency, and suitable for industry using easily available and less expensive materials.The present invention relates to a process for the production of an optically active amino alcohol comprising the steps that an optically active hydroxy ester in a trans-form obtained by an asymmetric hydrogenation of an easily available β-keto ester is reacted with hydrazine, the resulting optically active hydrazinocarbonyl alcohol is subjected to a Curtius rearrangement in the presence of alcohol and protective group of amino group of the resulting optically active alkoxycarbonylamino alcohol is deprotected. As a result of the process for the production in accordance with the present invention, the objected substance is able to be prepared in a high optical purity and in a high yield.

    摘要翻译： 本发明的目的是提供一种制备光学活性氨基醇，特别是反式形式的光学活性氨基醇的方法，其经济性和效率优异，并且适用于易于获得和较便宜的工业应用 材料 本发明涉及一种制备光学活性氨基醇的方法，该方法包括以下步骤：通过易于获得的β-酮酯的不对称氢化获得的反式的光学活性羟基酯与肼反应，得到 光学活性肼基羰基醇在醇的存在下进行Curtius重排，并将得到的光学活性烷氧基羰基氨基醇的保护基的氨基脱保护。 作为根据本发明的生产方法的结果，可以以高光学纯度和高产率制备被
    反应物质。

    Water-soluble polymer and additive for paper manufacture
    14.
    发明授权
    Water-soluble polymer and additive for paper manufacture 有权
    用于造纸的水溶性聚合物和添加剂

    公开(公告)号：US08816031B2

    公开(公告)日：2014-08-26

    申请号：US11367487

    申请日：2006-03-06

    申请人： Yoshiharu Kimura ,  Takahiro Fujiwara

    发明人： Yoshiharu Kimura ,  Takahiro Fujiwara

    IPC分类号： C08F20/54 ,  C08F20/70 ,  C08F120/54 ,  C08F2/00 ,  C08F2/10 ,  C08F220/56 ,  C08F220/34 ,  C08F222/02 ,  C08F220/06 ,  C08F230/08

    CPC分类号： C08F20/56 ,  C08F2/001 ,  C08F2/10 ,  C08F220/06 ,  C08F220/34 ,  C08F220/56 ,  C08F222/02 ,  C08F230/08

    摘要： The present invention provides a method for preparing a water soluble polymer, which comprises: a first step of polymerizing: (a) 60 to 99.5 mol % of at least one selected from acrylamide and methacrylamide, (b) 0.5 to 20 mol % of at least one selected from α,β-unsaturated monocarboxylic acid, α,β-unsaturated dicarboxylic acid and salts thereof, and (c) 1 to 20 mol % of at least one selected from a water soluble cationic monomer and a salt thereof, (d) 0.01 to 1 mol % of a chain transfer agent, and (e) 0.005 to 5 mol % of a crosslinkable monomer, in the presence of a persulfate-based catalyst to obtain a prepolymer; and a second step of further adding the persulfate-based catalyst to the prepolymer obtained in the first step and the residual monomer, followed by the polymerization and termination of the polymerization. Consequently, it is made possible to suppress a rapid increase in viscosity during the polymerization thereby to obtain a water soluble branched polymer having high molecular weight and low viscosity.

    摘要翻译： 本发明提供一种制备水溶性聚合物的方法，其包括：聚合的第一步骤：（a）60至99.5mol％的选自丙烯酰胺和甲基丙烯酰胺的至少一种，（b）0.5至20mol％的 至少一种选自α，β-不饱和一元羧酸，α，bgr-不饱和二羧酸及其盐，和（c）1〜20mol％的选自水溶性阳离子单体及其盐中的至少一种， （d）0.01〜1mol％的链转移剂，（e）0.005〜5mol％的交联性单体，在过硫酸系催化剂的存在下，得到预聚物; 以及将第一步骤中得到的预聚物和残留单体进一步添加过硫酸盐系催化剂，然后聚合并终止聚合的第二工序。 因此，可以抑制聚合期间的粘度的快速增加，从而得到具有高分子量和低粘度的水溶性支链聚合物。

    Ruthenium silyl-arene complex , and method for production thereof
    16.
    发明授权
    Ruthenium silyl-arene complex , and method for production thereof 有权
    钌甲硅烷基芳烃络合物及其制备方法

    公开(公告)号：US07880025B2

    公开(公告)日：2011-02-01

    申请号：US12782153

    申请日：2010-05-18

    申请人： Taichiro Touge ,  Hideki Nara ,  Takahiro Fujiwara

    发明人： Taichiro Touge ,  Hideki Nara ,  Takahiro Fujiwara

    IPC分类号： C07F15/00 ,  B01J31/00

    CPC分类号： C07F15/0046 ,  C07F17/02

    摘要： The present invention is to provide a ruthenium complex having a novel arene moiety, which has improved solubility in various solvents, and a method for production thereof.The present invention relates to a novel ruthenium complex having an arene moiety, which has a trisubstituted silyl group introduced to the arene moiety, and a method for production thereof.

    摘要翻译： 本发明提供一种具有新的芳族部分的钌配合物及其制备方法，其在各种溶剂中的溶解度提高。 本发明涉及一种具有引入到芳族部分的三取代甲硅烷基的具有芳烃部分的新型钌络合物及其制备方法。

    RUTHENIUM SILYL-ARENE COMPLEX , AND METHOD FOR PRODUCTION THEREOF
    17.
    发明申请
    RUTHENIUM SILYL-ARENE COMPLEX , AND METHOD FOR PRODUCTION THEREOF 有权
    镧系复合物及其生产方法

    公开(公告)号：US20100298588A1

    公开(公告)日：2010-11-25

    申请号：US12782153

    申请日：2010-05-18

    申请人： Taichiro Touge ,  Hideki Nara ,  Takahiro Fujiwara

    发明人： Taichiro Touge ,  Hideki Nara ,  Takahiro Fujiwara

    IPC分类号： C07F7/08

    CPC分类号： C07F15/0046 ,  C07F17/02

    摘要： The present invention is to provide a ruthenium complex having a novel arene moiety, which has improved solubility in various solvents, and a method for production thereof.The present invention relates to a novel ruthenium complex having an arene moiety, which has a trisubstituted silyl group introduced to the arene moiety, and a method for production thereof.

    摘要翻译： 本发明提供一种具有新的芳族部分的钌配合物及其制备方法，其在各种溶剂中的溶解度提高。 本发明涉及一种具有引入到芳族部分的三取代甲硅烷基的具有芳烃部分的新型钌络合物及其制备方法。

    Method of estimating location of abnormality in fluid feed pipeline network
    18.
    发明授权
    Method of estimating location of abnormality in fluid feed pipeline network 失效
    估计流体输送管网异常位置的方法

    公开(公告)号：US06912472B2

    公开(公告)日：2005-06-28

    申请号：US10430434

    申请日：2003-05-07

    申请人： Shizuo Mizushina ,  Atsushi Adachi ,  Takahiro Fujiwara

    发明人： Shizuo Mizushina ,  Atsushi Adachi ,  Takahiro Fujiwara

    IPC分类号： G01D21/00 ,  G01M3/28 ,  G06F19/00

    CPC分类号： G01M3/2807

    摘要： A method of detecting the location of a failure (e.g., a sudden leak) in a fluid pipeline network, which can be suitably used for estimation of the location of a failure in a water pipeline network, includes the steps of periodically measuring a flow rate or fluid pressure with sensors arranged at a plurality of measuring points along a pipeline in a water pipeline network; comparing a latest measured amount and a previous measured amount at each measuring point to determine if an amount of change at an arbitrary point has exceeded a predetermined value; and calculating a position at which an amount of change becomes maximum, the position being calculated from the magnitudes of the amounts of changes in respective measured values at the time of the detection. The pipeline network may be a water supply and distribution pipeline network which includes a trunk pipeline and branch pipelines.

    摘要翻译： 检测流体管线网络中可能适合用于估计水管网故障位置的故障位置（例如突然泄漏）的方法包括以下步骤：周期性地测量流量 或流体压力，其中传感器布置在沿着管道网络中的管道的多个测量点处; 比较每个测量点处的最近测量量和先前测量量，以确定任意点的变化量是否超过预定值; 以及计算变化量变得最大的位置，所述位置是根据检测时的各个测量值的变化量的大小来计算的。 管网可以是供水和配水管网，其中包括一个干线管道和分支管道。

    Method for producing ruthenium complex
    19.
    发明授权
    Method for producing ruthenium complex 有权
    钌络合物的制备方法

    公开(公告)号：US08658815B2

    公开(公告)日：2014-02-25

    申请号：US13138709

    申请日：2010-03-18

    申请人： Takahiro Fujiwara ,  Hideki Nara

    发明人： Takahiro Fujiwara ,  Hideki Nara

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0046 ,  C07F17/02

    摘要： The present invention provides a method for inexpensively producing di-μ-chloro-bis[chloro(η6-1-isopropyl-4-methylbenzene)ruthenium (II)] complex used as a catalyst raw material for a hydrogenation or metathesis polymerization reaction at a high yield. In the present invention, the above-described problem can be solved by reacting ruthenium chloride or a hydrate thereof with γ-terpinene in a solvent. In particular, by using an alcohol having a boiling point of 100° C. or higher as a solvent, the yield of the above-described complex can be increased.

    摘要翻译： 本发明提供了一种低成本生产用作氢化或易位聚合反应的催化剂原料的二氯氯 - 双[氯（eta6-1-异丙基-4-甲苯）钌（II）]络合物的方法， 高产。 在本发明中，上述问题可以通过使氯化钌或其水合物与γ-萜品烯在溶剂中反应来解决。 特别是通过使用沸点为100℃以上的醇作为溶剂，可以提高上述络合物的收率。