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    METHOD FOR PRODUCING ESTER COMPOUND AND PALLADIUM CATALYST USED IN THE METHOD
    1.
    发明申请
    METHOD FOR PRODUCING ESTER COMPOUND AND PALLADIUM CATALYST USED IN THE METHOD 有权
    生产方法中使用的酯化合物和钯催化剂的方法

    公开(公告)号：US20150343432A1

    公开(公告)日：2015-12-03

    申请号：US14431849

    申请日：2013-09-24

    Applicant: JX Nippon Oil & Energy Corporation

    Inventor： Shinichi KOMATSU ,  Akira SHIBASHI ,  Takaya MATSUMOTO

    IPC: B01J31/22 ,  C07C67/38

    CPC classification number: B01J31/2239 ,  B01J2231/32 ,  B01J2231/321 ,  B01J2531/0219 ,  B01J2531/824 ,  C07C67/38 ,  C07C2602/42 ,  C07C2603/94 ,  C07C69/753 ,  C07C69/757

    Abstract: A method for producing an ester compound includes reacting a compound having at least one cyclic structure of a norbornene ring and a norbornadiene ring with an alcohol and carbon monoxide by using a palladium catalyst and an oxidizing agent, to thereby introduce ester groups to carbon atoms forming a double bond in the cyclic structure and obtaining the ester compound, wherein the palladium catalyst includes a palladium acetate having a nitrite ligand in an amount of 10% by mole or more in terms of metal, and the palladium acetate having a nitrite ligand is represented by the general formula (1): Pd3(CH3COO)5(NO2).

    Abstract translation: 酯化合物的制造方法包括使用钯催化剂和氧化剂使具有降冰片烯环的至少一个环状结构的降冰片二烯环的化合物与醇和一氧化碳反应，从而将酯基引入形成的碳原子 环状结构中的双键并获得酯化合物，其中钯催化剂包括具有亚硝酸盐配体的乙酸钯，其量为金属换算为10摩尔％以上，并且具有亚硝酸盐配体的乙酸钯被表示 由通式（1）表示：Pd 3（CH 3 COO）5（NO 2）。

    Catalyst for the carbonylation of oxiraines
    3.
    发明申请
    Catalyst for the carbonylation of oxiraines 审中-公开
    羰基化环氧乙烷的催化剂

    公开(公告)号：US20070161806A1

    公开(公告)日：2007-07-12

    申请号：US10586826

    申请日：2005-01-20

    Applicant: Peter Preishuber-Pflugl ,  Ferenc Molnar

    Inventor： Peter Preishuber-Pflugl ,  Ferenc Molnar

    IPC: C07D305/12

    CPC classification number: B01J31/2208 ,  B01J31/182 ,  B01J31/20 ,  B01J2231/34 ,  B01J2531/0208 ,  B01J2531/0219 ,  B01J2531/0266 ,  B01J2531/0269 ,  B01J2531/22 ,  B01J2531/26 ,  B01J2531/31 ,  B01J2531/42 ,  B01J2531/46 ,  B01J2531/48 ,  B01J2531/845 ,  C07D305/12

    Abstract: Lactones are prepared by the catalytic carbonylation of oxiranes using a catalyst system comprising a) at least one carbonylation catalyst A comprising uncharged or anionic transition metal complexes of metals of groups 5 to 11 of the Periodic Table, b) at least one metal compound B of the formula (I) MXxRn-x  (I)  where M is an element of group 2, 3, 4, 12, 13, R is hydrogen or a hydrocarbon radical which may be substituted on the carbon atoms other than on the carbon atom bound to M, X is an anion, n is a number corresponding to the valence of M, x is in the range from 0 to n, and c) at least one organic, chiral compound C which has fewer than four coordination sites.

    Abstract translation: 内酯通过环氧乙烷的催化羰基化制备，所述催化剂体系包含a）至少一种羰基化催化剂A，其包含元素周期表第5至11族金属的不带电荷或阴离子过渡金属络合物，b）至少一种金属化合物B 公式（I）<？in-line-formula description =“In-line Formulas”end =“lead”？> MX in-line-formula description =“In-line Formulas”end =“tail”？>其中M是组2,3,4,12,13的元素，R是氢或可以被取代的烃基 除了与M结合的碳原子之外的碳原子，X是阴离子，n是对应于M的化合价的数，x在0至n的范围内，和c）至少一种有机手性化合物C，其中 有不到四个协调点。

    Complex compounds of iridium and process for preparing same
    6.
    发明授权
    Complex compounds of iridium and process for preparing same 失效
    复合化合物及其制备方法

    公开(公告)号：US3773814A

    公开(公告)日：1973-11-20

    申请号：US3773814D

    申请日：1971-10-13

    Applicant: SNAM PROGETTI

    Inventor： MASPERO F ,  PERROTTI E

    IPC: B01J31/24 ,  C07F15/00

    CPC classification number: B01J31/2404 ,  B01J31/1895 ,  B01J31/24 ,  B01J2231/641 ,  B01J2231/645 ,  B01J2531/0219 ,  B01J2531/80 ,  B01J2531/827 ,  C07F9/00 ,  C07F15/004

    Abstract: THERE ARE PROVIDED NOVEL COMPLEX COMPOUNDS OF THE GENERAL FORMULA

    (L)N-ME-ME-(L)N

    WHEREIN ME IS IR, AND L IS A COMPLEXING COMPOUND SELECTED FROM PHOSPHINES. THE NEW COMPLEXES ARE PREPARED BY TRANSFORMING A COMPOUND OF IRIDIUM INTO AT LEAST A PARTIAL HYDRIDE, THEN DEHYDROGENATING THIS IN THE PRESENCE OF A HYDROGEN ACCEPTOR AND OF A COMPLEXING AGENT. THE NEW COMPLEX COMPOUNDS HAVE CATALYTIC ACTIVITY, E.G., IN THE TRANSFER OF HYDROGEN IN UNSATURATED COMPOUNDS.

    Abstract translation: 1343470含有金属的磷砷和锑络合物SNAM PROGETTI SpA 8月1971年10月[1970年10月13日] 47065/71标题C1A [也在C2中]式I的络合物，其中M是Ⅷ族金属，L是膦，锑或胂， 或其任选卤化的烷基，芳基，烷芳基或芳烷基衍生物，n为2,3或4可以通过（a）通过与氢反应使第Ⅷ族金属和络合剂L的络合物的氢化物脱氢而制备 受体，（b）使任选与L以外的络合剂络合的第Ⅷ族金属的氢化物与络合剂L和氢受体反应。 在方法（a）中，起始配合物可以通过使L与（i）第Ⅷ族金属的氢化物，（ⅱ）第Ⅷ族金属的氢化物与不是L的络合剂的络合物或（ⅲ） 任选是部分氢化物的M的无机盐和氢化物的络合物。 在方法（b）中，第VIII族金属原料可以通过使氢化物与金属的无机盐或这种盐的络合物与除了L以外的络合剂的络合物反应来制备。氢受体可以是式 III其中R 1，R 2，R 3，R 3和R 4都是氢，烷基或芳基。

    Preparation of aromatic isocyanates
    8.
    发明授权
    Preparation of aromatic isocyanates 失效

    公开(公告)号：US3632827A

    公开(公告)日：1972-01-04

    申请号：US3632827D

    申请日：1968-11-21

    Applicant: OLIN MATHIESON

    Inventor： SMITH ERIC

    IPC: C07D279/20 ,  B01J31/00 ,  B01J31/26 ,  C07B61/00 ,  C07C67/00 ,  C07C241/00 ,  C07C263/14 ,  C07C265/00 ,  C07F15/00 ,  C07C119/04

    CPC classification number: B01J31/181 ,  B01J31/1815 ,  B01J31/1825 ,  B01J31/26 ,  B01J2531/0219 ,  B01J2531/82 ,  B01J2531/822 ,  B01J2531/824 ,  C07C263/14 ,  C07F15/0013 ,  C07C265/12 ,  C07C265/14

    Abstract: THE PROCESS FOR PREPARING AN ORGANIC ISOCYANATE BY REACTING AN ORGANIC NITRO COMPOUND WITH CARBON MONOXIDE IN THE PRESENCE OF A CATALYST SYSTEM COMPRISED OF (1) A NITROGEN-CONTAINING HETEROAROMATIC COMPOUND AND (2) A HALIDE OF A NOBLE METAL, AND (3) A HALIDE OF A NON-NOBLE METAL SELECTED FROM THE GROUP CONSISTING OF IRON AND THE METALS OF GROUPS IVA, VA, VIA, VIIA, IIB, IVB, AND VB OF THE PERIODIC TABLE. THE HETEROAROMATIC NITROGEN-CONTAINING COMPOUND IS ONE CONTAINING BETWEEN FIVE AND SIX MEMBERS IN THE RING, CONTAINING NO ELEMENT OTHER THAN NITROGEN AND CARBON IN THE RING, AND HAVING AT LEAST TWO DOUBLE BONDS IN THE RING. PYRIDINE AND ISOQUINOLINE ARE THE PREFERRED HETEROAROMATIC COMPOUNDS. THE NOBLE METAL HALIDE IS PREFERABLY A HALIDE OF PALLADIUM, RHODIUM, IRIDIUM, RHENIUM, PLATINUM OR MIXTURES THEREOF. THE PREFERRED NON-NOBLE METAL HALIDES ARE HALIDES OF TITANIUM, ZIRCONIUM, VANADIUM, TANTALUM, CHROMIUM, MANGANESE, IRON, ZINC, MERCURY, GERMANIUM, TIN, LEAD, ARSENIC, ANTIMONY AND BISMUTH. A FOURTH COMPONENT, SUCH AS MOLYBDENUM TRIOXIDE OR ANOTHER METAL OXIDE, MAY ALSO BE INCLUDED IN THE CATALYST SYSTEM.

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