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11.发明授权Method for quantitation of acid sites in acidic catalysts using silane and borane compounds 有权使用硅烷和硼烷化合物定量酸性催化剂中酸性位点的方法公开(公告)号：US09435688B2
公开(公告)日：2016-09-06
申请号：US14703249
申请日：2015-05-04
申请人： UOP LLC
IPC分类号： G01N31/10 , G01N31/22 , G01J3/28 , G01N30/02 , G01N23/223 , G01R33/46 , B01J31/00 , G01N24/08 , G01N30/88
CPC分类号： G01J3/28 , B01J31/00 , B01J31/0298 , B01J31/40 , B01J2231/32 , G01N23/223 , G01N24/08 , G01N30/02 , G01N30/88 , G01N31/10 , G01N2030/025 , G01N2030/027 , G01R33/46
摘要： A method of quantifying an amount of Brønsted acid sites in an aluminum chloride-containing catalyst is described. The method involves adding a known amount of at least one silane or borane compound to the aluminum chloride-containing catalyst being analyzed. The Brønsted acid sites in the aluminum chloride-containing catalyst react with the silane or borane compound to form a silyl boryl compound, resulting in a catalyst phase and a hydrocarbon phase which contains the silyl or boryl compound. The amount of silyl or boryl compound in the hydrocarbon phase is measured. From the measured amount of silyl or boryl compound formed, the amount of Brønsted acid sites can be determined.
摘要翻译： 描述了在含氯化铝的催化剂中量化布朗斯台德酸位点的方法。 该方法包括向已分析的含氯化铝的催化剂中加入已知量的至少一种硅烷或硼烷化合物。 含氯化铝催化剂中的布朗斯台德酸位与硅烷或硼烷化合物反应形成甲硅烷基硼基化合物，产生催化剂相和含有甲硅烷基或硼基化合物的烃相。 测量烃相中甲硅烷基或硼基化合物的量。 从形成的甲硅烷基或硼基化合物的测定量可以确定布朗斯台德酸位点的量。
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12.发明申请CONTAMINANT REMOVAL FROM KEROSENE STREAMS WITH LACTAMIUM BASED IONIC LIQUIDS 审中-公开用基于LACTAMIUM的离子液体从KEROSENE STREAMS中去除污染物公开(公告)号：US20160168483A1
公开(公告)日：2016-06-16
申请号：US14566058
申请日：2014-12-10
申请人： UOP LLC
发明人： Erin M. Broderick , Alakananda Bhattacharyya , Beckay J. Mezza , Soumendra Mohan Banerjee , Rajeswar R. Gattupalli
摘要： A process for removing a contaminant from a kerosene stream using a lactamium based ionic liquid is described. The process includes contacting the kerosene stream comprising the contaminant with a lean kerosene-immiscible lactamium ionic liquid to produce a mixture comprising the kerosene and a rich kerosene-immiscible lactamium ionic liquid comprising at least a portion of the removed contaminant; and separating the mixture to produce a kerosene effluent and a rich kerosene-immiscible lactamium ionic liquid effluent comprising the rich kerosene-immiscible lactamium ionic liquid.
摘要翻译： 描述了使用基于内酰胺的离子液体从煤油流中除去污染物的方法。 该方法包括使包含污染物的煤油流与贫煤油不混溶的内酰胺离子液体接触，以产生包含煤油和富含不溶于煤油的内酰胺离子液体的混合物，其包含至少一部分去除的污染物; 并分离混合物以产生煤油流出物和富含煤油不混溶的内酰胺离子液体流出物，其包含富含煤油不混溶的内酰胺离子液体。
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13.发明申请CONTAMINANT REMOVAL FROM HYDROCARBON STREAMS WITH CARBENIUM PSEUDO IONIC LIQUIDS 有权碳氢化合物离子液体污染物去除污染物公开(公告)号：US20160145501A1
公开(公告)日：2016-05-26
申请号：US14552333
申请日：2014-11-24
申请人： UOP LLC
CPC分类号： C10G21/06 , C10G21/27 , C10G55/06 , C10G61/04 , C10G67/04 , C10G2300/202 , C10G2300/301
摘要： Processes for removing sulfur and nitrogen contaminants from hydrocarbon streams are described. The processes include contacting the hydrocarbon stream comprising the contaminant with lean carbenium pseudo ionic liquid or a combination of carbenium pseudo ionic liquid and ionic liquid to produce a mixture comprising the hydrocarbon and rich carbenium pseudo ionic liquid or carbenium pseudo ionic liquid and ionic liquid comprising the contaminant. The mixture is separated to produce a hydrocarbon effluent and a rich carbenium pseudo ionic liquid or carbenium pseudo ionic liquid and ionic liquid effluent comprising the rich carbenium pseudo ionic liquid or carbenium pseudo ionic liquid and ionic liquid comprising the contaminant.
摘要翻译： 描述了从烃流中除去硫和氮污染物的方法。 该方法包括使包含污染物的烃流与贫碳化假假离子液体或碳鎓假离子液体和离子液体的组合接触，以产生包含烃和富碳的假离子液体或碳鎓假离子液体和离子液体的混合物， 污染物。 将混合物分离以产生烃流出物和富含碳氢化合物假离子液体或碳氢化合物假离子液体和离子液体流出物，其包含富含碳的假离子液体或碳鎓假离子液体和包含污染物的离子液体。
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公开(公告)号：US09233928B2
公开(公告)日：2016-01-12
申请号：US14271308
申请日：2014-05-06
申请人： UOP LLC
IPC分类号： C07D223/10
CPC分类号： C07D223/10 , C07C309/73
摘要： Lactamium based ionic liquids are described. They comprise at least one of: the reaction product of a lactam compound having a general formula wherein n is 1 to 8, and a Brønsted acid HX; or a Brønsted acid HX, where X is a halide, and a metal halide; where the reaction product is p-toluenesulfonate, halide, or the halometallate; or the reaction product of a lactam compound having a general formula wherein the ring has at least C—C one double bond, and n is 1 to 8, and a Brønsted acid HX; or a Brønsted acid HX, where X is a halide, and a metal halide; or the reaction product of a lactam compound having a general formula wherein n is 1 to 8, m is 1 to 8, and the rings can be saturated or unsaturated; and a Brønsted acid HX; or a Brønsted acid HX, where X is a halide, and a metal halide.
摘要翻译： 描述了基于乳酸的离子液体。 它们包括以下中的至少一种：具有通式其中n为1至8的内酰胺化合物与布朗斯台德酸HX的反应产物; 或布朗斯台德酸HX，其中X为卤化物，和金属卤化物; 其中反应产物是对甲苯磺酸盐，卤化物或卤代金属盐; 或具有通式的内酰胺化合物的反应产物，其中环具有至少C-C一个双键，n为1至8，Brnnsted酸HX; 或布朗斯台德酸HX，其中X为卤化物，和金属卤化物; 或其中n为1〜8，m为1〜8的通式的内酰胺化合物的反应产物，并且所述环可以是饱和或不饱和的; 和布朗斯台德酸HX; 或布朗斯台德酸HX，其中X为卤化物，和金属卤化物。
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15.发明申请公开(公告)号：US20150321977A1
公开(公告)日：2015-11-12
申请号：US14556932
申请日：2014-12-01
申请人： UOP LLC
CPC分类号： C07C6/10 , C07C2/20 , C07C2/22 , C07C2/60 , C07C2/62 , C07C5/2727 , C07C5/2748 , C07C6/123 , C07C2531/02 , C07C2531/14 , C07C9/14 , C07C9/10 , C07C9/21 , C07C9/16 , C07C11/02
摘要： A hydrocarbon conversion process is described. The process involves contacting a hydrocarbon feed with a lactamium based ionic liquid catalyst in a reaction zone under reaction conditions to form a mixture comprising reaction products, and the lactamium based ionic liquid catalyst. Typical hydrocarbon conversion processes include alkylation, oligomerization, isomerization, disproportionation, and reverse disproportionation.
摘要翻译： 描述烃转化方法。 该方法包括在反应条件下在反应区中将烃进料与基于内酰胺的离子液体催化剂接触以形成包含反应产物和基于内酰胺的离子液体催化剂的混合物。 典型的烃转化方法包括烷基化，低聚反应，异构化，歧化反应和反向歧化反应。
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16.发明申请METHOD FOR QUANTITATION OF ACID SITES IN ACIDIC CATALYSTS USING SILANE AND BORANE COMPOUNDS 有权使用硅烷和硼烷化合物在酸性催化剂中定量酸性位点的方法公开(公告)号：US20150316518A1
公开(公告)日：2015-11-05
申请号：US14703249
申请日：2015-05-04
申请人： UOP LLC
IPC分类号： G01N31/10 , G01R33/46 , G01N23/223 , G01N30/02 , G01J3/28
CPC分类号： G01J3/28 , B01J31/00 , B01J31/0298 , B01J31/40 , B01J2231/32 , G01N23/223 , G01N24/08 , G01N30/02 , G01N30/88 , G01N31/10 , G01N2030/025 , G01N2030/027 , G01R33/46
摘要： A method of quantifying an amount of Brønsted acid sites in an aluminum chloride-containing catalyst is described. The method involves adding a known amount of at least one silane or borane compound to the aluminum chloride-containing catalyst being analyzed. The Brønsted acid sites in the aluminum chloride-containing catalyst react with the silane or borane compound to form a silyl boryl compound, resulting in a catalyst phase and a hydrocarbon phase which contains the silyl or boryl compound. The amount of silyl or boryl compound in the hydrocarbon phase is measured. From the measured amount of silyl or boryl compound formed, the amount of Brønsted acid sites can be determined.
摘要翻译： 描述了在含氯化铝的催化剂中量化布朗斯台德酸位点的方法。 该方法包括向已分析的含氯化铝的催化剂中加入已知量的至少一种硅烷或硼烷化合物。 含氯化铝催化剂中的布朗斯台德酸位与硅烷或硼烷化合物反应形成甲硅烷基硼基化合物，产生催化剂相和含有甲硅烷基或硼基化合物的烃相。 测量烃相中甲硅烷基或硼基化合物的量。 从形成的甲硅烷基或硼基化合物的测定量可以确定布朗斯台德酸位点的量。
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公开(公告)号：US20150314281A1
公开(公告)日：2015-11-05
申请号：US14269978
申请日：2014-05-05
申请人： UOP LLC
发明人： Erin M. Broderick , Alakananda Bhattacharyya , Susie C. Martins , Kaitlin M. DeSalvo , Douglas A. Nafis
CPC分类号： B01J31/4053 , B01J31/0277 , B01J31/0288 , B01J31/0298 , B01J31/4092 , B01J38/50 , B01J38/56 , B01J2231/645 , B01J2531/31
摘要： A method of regenerating an acidic catalyst is described. A borane compound is contacted with an acidic catalyst that contains conjunct polymer, which releases the conjunct polymer from the acidic catalyst. The acidic catalyst can then be re-activated with acid. The conjunct polymer can be separated from the borane compound, and the borane compound can be recycled.
摘要翻译： 描述了酸性催化剂的再生方法。 将硼烷化合物与含有结合聚合物的酸性催化剂接触，该酸性催化剂从酸性催化剂释放结合聚合物。 酸性催化剂然后可以用酸重新活化。 可以将结合的聚合物与硼烷化合物分离，并且可以再循环硼烷化合物。
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公开(公告)号：US20150093313A1
公开(公告)日：2015-04-02
申请号：US14042647
申请日：2013-09-30
申请人： UOP LLC
CPC分类号： B01D53/526 , B01D53/1468 , B01D53/1493 , B01D2252/30 , B01D2252/504 , C07C7/11 , C10L3/103 , Y02P20/542 , C07C9/04
摘要： The invention comprises a process for removal of hydrogen sulfide from gaseous mixtures. The process involves the use of a mixture of a physical absorption solvent and an ionic liquid. The mixtures provided improved absorption of hydrogen sulfide, when compared to physical absorption solvents without the ionic liquid at low partial pressures of hydrogen sulfide. A regeneration cycle involving the addition of a solvent, such as water, is used to regenerate the mixture.
摘要翻译： 本发明包括从气体混合物中除去硫化氢的方法。 该方法包括使用物理吸收溶剂和离子液体的混合物。 与在硫化氢低分压下没有离子液体的物理吸收溶剂相比，混合物提供了改善的硫化氢吸收。 使用包括加入溶剂如水的再生循环来再生混合物。
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公开(公告)号：US20240335808A1
公开(公告)日：2024-10-10
申请号：US18586777
申请日：2024-02-26
申请人： UOP LLC
发明人： Erick J. Bennett, III , William J. Whyman , Aric G. Fisher , Elizabeth Jensen , Erin M. Broderick
CPC分类号： B01J3/008 , B01J8/0221 , B01J8/0285 , B01J2208/00495 , B01J2208/0053
摘要： Processes and apparatuses converting poly- and perfluoroalkyl substances (PFAS). An oxidation reaction zone, preferably a thermal oxidizer, is used to oxidize the PFAS into fluoride species. A reaction zone having at least one reactor containing a solid reactant for neutralizing the fluoride species is provided. The solid reactant is also configured to degrade any PFAS remaining in the effluent from the oxidation zone. A cooling zone, for example, a quench zone may be between the reaction zone and the oxidation zone. The PFAS may be liquid PFAS that is injected into the thermal oxidizer.
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20.发明授权公开(公告)号：US10550049B2
公开(公告)日：2020-02-04
申请号：US15867403
申请日：2018-01-10
申请人： UOP LLC
摘要： A hydrocarbon conversion process is described. The process involves contacting a hydrocarbon feed with a non-cyclic amide or thioamide based ionic liquid catalyst in a reaction zone under reaction conditions to form a mixture comprising reaction products, and the non-cyclic amide or thioamide based ionic liquid catalyst. Typical hydrocarbon conversion processes include alkylation, oligomerization, isomerization, disproportionation, and reverse disproportionation.
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