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23 条记录 (耗时 0.031 秒)

    Method for Producing Tertiary Phosphines
    12.
    发明申请
    Method for Producing Tertiary Phosphines 审中-公开
    生产三膦的方法

    公开(公告)号：US20080146850A1

    公开(公告)日：2008-06-19

    申请号：US11815460

    申请日：2006-02-09

    申请人： Kathrin Wissel ,  Matthias Maase ,  Oliver Huttenloch ,  Toni Flajs ,  Melanie Kuhl

    发明人： Kathrin Wissel ,  Matthias Maase ,  Oliver Huttenloch ,  Toni Flajs ,  Melanie Kuhl

    IPC分类号： C07F9/50

    CPC分类号： C07F9/5081 ,  C07F9/5068

    摘要： Method for producing tertiary phosphines by reacting a compound of the general formula (I) in which A is R1 or L2, B is R2 or L3, the R1 and R2 radicals are each independently an organic radical having in each case from 1 to 30 carbon atoms, where the R1 and R2 radicals may also be joined together; and the leaving groups L1 to L3 are each independently halogen, alkyloxy having from 1 to 10 carbon atoms or aryloxy having from 6 to 10 carbon atoms (a) with an alkali metal in an organic aprotic solvent and (b) a compound of the general formula (II) L4-R3   (II) in which the R3 radical is an organic radical having in each case from 1 to 30 carbon atoms; and the leaving group L4 is halogen, alkyloxy having from 1 to 10 carbon atoms or aryloxy having from 6 to 10 carbon atoms, in which the resulting reaction mixture is hydrolyzed with an aqueous base which has a pH of ≧10 and the organic phase is removed from the aqueous phase.

    摘要翻译： 通过使其中A为R 1或L 2的通式（I）的化合物与B 2反应生成叔膦的方法，B为R 2 O / >或L 3，R 1和R 2基团各自独立地为在每种情况下具有1至30个碳原子的有机基团， 其中R 1和R 2基团也可以连接在一起; 和离去基团L 1至L 3各自独立地为卤素，具有1至10个碳原子的烷氧基或具有6至10个碳原子的芳氧基（a）与 有机质子惰性溶剂中的碱金属和（b）通式（II）的化合物<？in-line-formula description =“In-line Formulas”end =“lead”→> L 4 （II）<？in-line-formula description =“In-line formula”end =“tail”？>其中R 3是基团 在每种情况下具有1至30个碳原子的有机基团; 并且离去基团L 4是卤素，具有1至10个碳原子的烷氧基或具有6至10个碳原子的芳氧基，其中所得反应混合物用具有pH值的碱水溶液水解 > 10，并且从水相中除去有机相。

    METHOD FOR ISOLATING ACIDS FROM CHEMICAL REACTION MIXTURES BY USING 1-ALKYLIMIDAZOLES
    17.
    发明申请
    METHOD FOR ISOLATING ACIDS FROM CHEMICAL REACTION MIXTURES BY USING 1-ALKYLIMIDAZOLES 审中-公开
    通过使用1-烷基咪唑来分离化学反应混合物中的酸的方法

    公开(公告)号：US20090023933A1

    公开(公告)日：2009-01-22

    申请号：US10596548

    申请日：2004-12-17

    申请人： Matthias Maase ,  Oliver Huttenloch

    发明人： Matthias Maase ,  Oliver Huttenloch

    IPC分类号： C07D233/54

    CPC分类号： C07B63/04 ,  C07F9/025 ,  C07F9/4841

    摘要： Method of separating acids from reaction mixtures by means of an auxiliary base, where the auxiliary base b) reacts with the acid to form a salt which is liquid at temperatures at which the desired product is not significantly decomposed while the liquid salt is being separated off and c) the salt of the auxiliary base forms two immiscible liquid phases with the desired product or the solution of the desired product in a suitable solvent, in which the auxiliary base used is an alkylmidazole, which has a solubility in 30% strength by weight sodium chloride solution at 25° C. of 10% by weight or less and whose hydrochloride has a melting point below 55° C.

    摘要翻译： 通过辅助碱将酸与反应混合物分离的方法，其中辅助碱b）与酸反应以形成盐，其在所需产物在不明显分解的温度下为液体，同时液体盐被分离出 和c）辅助碱的盐与所需产物或所需产物的溶液在合适的溶剂中形成两个不混溶的液相，其中所用的辅助碱是烷基咪唑，其溶解度在30重量％ 25℃的氯化钠溶液为10重量％以下，其盐酸盐的熔点低于55℃。

    Method for Chlorinating Alcohols
    18.
    发明申请
    Method for Chlorinating Alcohols 审中-公开
    氯化醇的方法

    公开(公告)号：US20080228016A1

    公开(公告)日：2008-09-18

    申请号：US12066321

    申请日：2006-08-31

    申请人： Thorsten Rohde ,  Oliver Huttenloch ,  Friederike Osswald ,  Kathrin Wissel

    发明人： Thorsten Rohde ,  Oliver Huttenloch ,  Friederike Osswald ,  Kathrin Wissel

    IPC分类号： C07C17/16

    CPC分类号： C07C17/16 ,  C07C19/01

    摘要： A process for preparing organic chlorides in which the chlorine atom is bonded to a CH2 group by reacting the corresponding alcohols with thionyl chloride in the presence of a triaylphosphine oxide at a temperature of from 20 to 200° C. and a pressure of from 0.01 to 10 MPa abs, which comprises using the triarylphosphine oxide in a molar ratio to the amount of OH groups to be chlorinated of from 0.0001 to 0.5.

    摘要翻译： 一种制备有机氯化物的方法，其中氯原子通过在三乙烯基氧化膦存在下，在20〜200℃的温度下使相应的醇与亚硫酰氯反应而与CH 2 - 和0.01至10MPa abs的压力，其包括使用与被氯化的OH基团的摩尔比为0.0001-0.5的三芳基氧化膦。

    Method for operating a liquid ring compressor
    20.
    发明授权
    Method for operating a liquid ring compressor 失效
    操作液环式压缩机的方法

    公开(公告)号：US07927080B2

    公开(公告)日：2011-04-19

    申请号：US11662851

    申请日：2005-09-16

    申请人： Christian Müller ,  Martin Sesing ,  Martin Fiene ,  Oliver Huttenloch ,  Eckhard Stroefer

    发明人： Christian Müller ,  Martin Sesing ,  Martin Fiene ,  Oliver Huttenloch ,  Eckhard Stroefer

    IPC分类号： F04C19/00

    CPC分类号： F04C19/004 ,  C10N2220/04 ,  C10N2240/30 ,  F04C2210/12

    摘要： The invention relates to a method of operating a liquid ring compressor having an impeller installed eccentrically in a compressor body, with gas being supplied to the liquid ring compressor on a suction side and gas being discharged from the liquid ring compressor on a pressure side. A liquid ring is generated in the liquid ring compressor on the inside of the compressor body by rotation of the impeller. Chambers are formed between blades of the impeller and the liquid ring and gas is drawn into these. The gas is compressed in the chambers which become smaller from the suction side to the pressure side as a result of the rotation of the eccentrically mounted impeller. The compressed gas is ejected on the pressure side. An ionic liquid is used as service liquid for generation of the liquid ring.

    摘要翻译： 本发明涉及一种操作液压压缩机的方法，该液环压缩机具有偏心地安装在压缩机体中的叶轮，其中气体在吸入侧被供应到液环压缩机，气体在压力侧从液环压缩机排出。 通过叶轮的旋转，在压缩机主体内部的液环压缩机中产生液环。 在叶轮的叶片和液体环之间形成腔室，并且气体被吸入这些腔室中。 由于偏心安装的叶轮的旋转，气体在从吸入侧到压力侧变小的室中被压缩。 压缩气体在压力侧喷射。 离子液体用作产生液体环的服务液体。