公开(公告)号：US20030146417A1

公开(公告)日：2003-08-07

申请号：US10333827

申请日：2003-01-23

Inventor： Lee Sergey Romonovich ,  Ayako Yamamoto ,  Setsuko Tajima

IPC: H01C001/00

CPC classification number: C01B35/04 ,  B01J3/062 ,  B01J2203/0605 ,  B01J2203/0645 ,  B01J2203/068 ,  Y10T29/49014 ,  Y10T29/49117

Abstract: The invention is intended to establish means for manufacturing MB2 single crystals and to provide a useful superconductive material (wire rod and so forth) taking advantage of anisotropic superconductive properties thereof. A mixed raw material of Mg and B or a precursor containing MgB2 crystallites, obtained by causing reaction of the mixed raw material of Mg and B, kept in contact with hexagonal boron nitride (hBN), is held at a high temperature in the range of 1300 to 1700null C. and under a high pressure in the range of 3 to 6 GPa to cause reaction for forming an intermediate product, thereby growing the MB2 single crystals having anisotropic superconductive properties via the intermediate product. The single crystals have features such that, depending on a direction in which a magnetic field is applied thereto, an irreversible magnetic field strength becomes equivalent to not less than 95% of a second magnetic field strength, so that adjustment of crystal orientation thereof results in production of a superconductive material excellent in property. Further, it is useful in effecting growth of the single crystals to cause a reducing agent such as Mg and so forth to coexist at the time of the reaction, or to provide a temperature gradient in melt occurring in the course of the reaction.

Abstract translation: 本发明旨在建立用于制造MB2单晶的手段，并且利用其各向异性超导性能来提供有用的超导材料（线棒等）。 通过与保持与六方氮化硼（hBN）接触的Mg和B的混合原料的反应获得的Mg和B的混合原料或含有MgB 2微晶的前体在高温下保持在 1300至1700℃，在3至6GPa的高压下引起反应，形成中间产物，从而通过中间产物生长具有各向异性超导性的MB2单晶。 单晶具有这样的特征：根据施加磁场的方向，不可逆磁场强度等于不小于第二磁场强度的95％，从而导致晶体取向的调整 生产性能优异的超导材料。 此外，在进行单晶生长以使Mg等还原剂在反应时共存，或在反应过程中提供熔融温度梯度是有用的。

公开(公告)号：US09481073B2

公开(公告)日：2016-11-01

申请号：US14929611

申请日：2015-11-02

Applicant: Baker Hughes Incorporated

Inventor： Anthony A. DiGiovanni

IPC: B24D18/00 ,  B24D99/00 ,  E21B10/567 ,  B01J3/06

CPC classification number: B01J3/062 ,  B01J2203/0605 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D18/0009 ,  B24D99/00 ,  E21B10/54 ,  E21B10/56 ,  E21B10/567

Abstract: Methods of forming polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure and a temperature sufficient to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool includes a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.

Abstract translation: 形成多晶金刚石的方法包括将金刚石颗粒和烃物质包封在罐中，并且将包封的金刚石颗粒和烃物质经受足以在金刚石颗粒之间形成颗粒间结合的压力和温度。 用于钻孔工具的切割元件包括通过这种工艺形成的多晶金刚石材料。 钻孔工具包括这样的切割元件。

公开(公告)号：US09205531B2

公开(公告)日：2015-12-08

申请号：US13619210

申请日：2012-09-14

Applicant: Anthony A. DiGiovanni

Inventor： Anthony A. DiGiovanni

IPC: B24D3/02 ,  B24D99/00 ,  B24D18/00 ,  E21B10/567 ,  B01J3/06

CPC classification number: B01J3/062 ,  B01J2203/0605 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D18/0009 ,  B24D99/00 ,  E21B10/54 ,  E21B10/56 ,  E21B10/567

Abstract: Methods of fabricating polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure of at least 5.0 GPa and a temperature of at least 1400° C. to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool includes a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.

Abstract translation: 制造多晶金刚石的方法包括将金刚石颗粒和烃类物质包封在罐中，并将包封的金刚石颗粒和烃物质经受至少5.0GPa的压力和至少1400℃的温度以形成颗粒间结合 在金刚石颗粒之间。 用于钻孔工具的切割元件包括通过这种工艺形成的多晶金刚石材料。 钻孔工具包括这样的切割元件。

公开(公告)号：US08945301B2

公开(公告)日：2015-02-03

申请号：US13204205

申请日：2011-08-05

Applicant: Valery N. Khabashesku ,  Valery A. Davydov ,  Alexandra V. Rakhmanina

Inventor： Valery N. Khabashesku ,  Valery A. Davydov ,  Alexandra V. Rakhmanina

IPC: C30B29/04 ,  C01B31/06 ,  B01J3/06 ,  B82Y30/00 ,  C09K11/65

CPC classification number: C01B31/06 ,  B01J3/062 ,  B01J2203/0605 ,  B01J2203/061 ,  B01J2203/0655 ,  B01J2203/068 ,  B82Y30/00 ,  C01B32/25 ,  C01P2002/60 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/64 ,  C09K11/65

Abstract: A method for producing a diamond material by contacting a fluorinated precursor with a hydrocarbon in a reactor and forming a combination in the absence of a metal catalyst; increasing the pressure of the reactor to a first pressure; heating the combination under pressure to form a material precursor; cooling the material precursor; and forming a diamond material.

Abstract translation: 一种通过在反应器中使含氟前体与烃接触并在不存在金属催化剂的情况下形成组合来生产金刚石材料的方法; 将反应器的压力增加到第一压力; 在压力下加热组合以形成材料前体; 冷却材料前体; 并形成金刚石材料。

公开(公告)号：US20140013672A1

公开(公告)日：2014-01-16

申请号：US13705693

申请日：2012-12-05

Applicant: Abds-Sami Malik ,  Hui Zhang

Inventor： Abds-Sami Malik ,  Hui Zhang

IPC: B24D18/00

CPC classification number: B24D18/00 ,  B01J3/062 ,  B01J2203/0605 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  C04B35/528 ,  C04B35/645 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/5296 ,  C04B2235/5436 ,  C04B2235/6567

Abstract: A method of making diamond including mixing graphene with diamond seed to form a powder mixture, and then sintering the powder mixture, in the absence of a transition metal catalyst, at high pressure and high temperature; and a method of making a polycrystalline diamond compact including mixing graphene in diamond powder to form a powder mixture with less than about 50% graphene by weight, and then sintering the powder mixture, in the absence of a transition metal catalyst, at high pressure and high temperature.

Abstract translation: 一种制造金刚石的方法，包括将石墨烯与金刚石晶种混合以形成粉末混合物，然后在高压和高温下在不存在过渡金属催化剂的情况下烧结粉末混合物; 以及制造多晶金刚石压块的方法，包括在金刚石粉末中混合石墨烯以形成重量小于约50％石墨烯的粉末混合物，然后在不存在过渡金属催化剂的情况下在高压下烧结粉末混合物， 高温。

公开(公告)号：US20130068540A1

公开(公告)日：2013-03-21

申请号：US13619210

申请日：2012-09-14

Applicant: Anthony A. DiGiovanni

Inventor： Anthony A. DiGiovanni

IPC: B24D3/34 ,  B01J3/06 ,  E21B10/46

CPC classification number: B01J3/062 ,  B01J2203/0605 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D18/0009 ,  B24D99/00 ,  E21B10/54 ,  E21B10/56 ,  E21B10/567

Abstract: Methods of fabricating polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure of at least 5.0 GPa and a temperature of at least 1400° C. to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool includes a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.

Abstract translation: 制造多晶金刚石的方法包括将金刚石颗粒和烃类物质包封在罐中，并将包封的金刚石颗粒和烃物质经受至少5.0GPa的压力和至少1400℃的温度以形成颗粒间结合 在金刚石颗粒之间。 用于钻孔工具的切割元件包括通过这种工艺形成的多晶金刚石材料。 钻孔工具包括这样的切割元件。