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    Perylene derivative synthesis process, perylene derivative and organic EL device
    15.
    发明申请
    Perylene derivative synthesis process, perylene derivative and organic EL device 有权
    苝衍生物合成工艺，苝衍生物和有机EL器件

    公开(公告)号：US20050054852A1

    公开(公告)日：2005-03-10

    申请号：US10959222

    申请日：2004-10-07

    申请人： Tetsuji Fujita ,  Kensuke Ara ,  Tetsushi Inoue

    发明人： Tetsuji Fujita ,  Kensuke Ara ,  Tetsushi Inoue

    IPC分类号： C07C13/62 ,  C07C15/20 ,  C07C17/30 ,  C07C17/35 ,  C07C25/22 ,  C07C25/24 ,  H01L51/00 ,  H01L51/30 ,  H01L51/40 ,  H01L51/50 ,  C07D221/22 ,  C07C15/067 ,  C07D471/02

    CPC分类号： C07C25/24 ,  C07C13/62 ,  C07C15/20 ,  C07C17/30 ,  C07C17/35 ,  C07C25/22 ,  C07C2603/52 ,  C07C2603/54 ,  H01L51/001 ,  H01L51/0052 ,  H01L51/0055 ,  H01L51/0056 ,  H01L51/0058 ,  H01L51/0059 ,  H01L51/0081 ,  H01L51/5012 ,  H01L2251/308 ,  Y10S428/917

    摘要： The invention aims to provide a perylene derivative preparation process featuring satisfactory yields and improved preparation efficiency, a perylene derivative obtained by the process, and an organic EL device using the same. The object is achieved by a perylene derivative preparation process comprising subjecting to coupling reaction a 1,8-dihalogenated naphthalene derivative of the formula (1): wherein X is Cl, Br or I, R1 to R4, R11 and R12 each are hydrogen, alkyl, alkoxy, alkylthio, alkenyl, alkenyloxy, alkenylthio, aralkyl, aralkyloxy, aralkylthio, aryl, aryloxy, and arylthio radicals which may be substituted, amino radical, cyano radical, hydroxyl radical, —COOM1 radical (wherein M1 is hydrogen, alkyl, alkenyl, aralkyl or aryl), —COM2 radical (wherein M2 is hydrogen, alkyl, alkenyl, aralkyl, aryl or amino), or —OCOM3 radical (wherein M3 is alkyl, alkenyl, aralkyl or aryl), and at least two adjoining radicals selected from among R1 to R4, R11 and R12 may bond or fuse together to form a substituted or unsubstituted carbocyclic aliphatic ring, aromatic ring or fused aromatic ring with the carbon atoms on which they substitute, with the proviso that when the carbocyclic aliphatic ring, aromatic ring or fused aromatic ring has substituent radicals, the substituent radicals are the same as R1 to R4, R11 and R12, to thereby synthesize a perylene derivative of the formula (2): wherein R1′ to R4′, R11′ and R12′ are as defined for R1 to R4, R11 and R12 in formula (1), and R1 to R4, R11 and R12 and R1′ to R4′, R11′ and R12′ may be the same or different.

    摘要翻译： 本发明旨在提供一种具有令人满意的产率和提高的制备效率的苝衍生物制备方法，通过该方法获得的苝衍生物和使用其的有机EL器件。 该目的通过苝衍生物制备方法实现，其包括使式（1）的1,8-二卤代萘衍生物与其偶合反应：其中X为Cl，Br或I，R 1至R 4，R 11和R 12各自为氢， 烷基，烷氧基，烷硫基，烯基，烯氧基，烯硫基，芳烷基，芳烷氧基，芳烷硫基，芳基，芳氧基和可被取代的芳硫基，氨基，氰基，羟基，-COOM1基（其中M1是氢，烷基， 烯基，芳烷基或芳基），-COM 2基团（其中M 2是氢，烷基，烯基，芳烷基，芳基或氨基）或-OCOM 3基团（其中M 3是烷基，烯基，芳烷基或芳基），和至少两个相邻的基团 选自R 1至R 4，R 11和R 12可以键合或熔合在一起以形成具有其取代的碳原子的取代或未取代的碳环脂族环，芳香环或稠合芳环，条件是当碳环脂族环， 芳环或f 所使用的芳香环具有取代基，取代基与R 1〜R 4，R 11，R 12相同，合成式（2）所示的苝衍生物：其中R1'至R4'，R11'和R12'如上所定义 对于式（1）中的R 1至R 4，R 11和R 12，并且R 1至R 4，R 11和R 12以及R 1'至R 4'，R 11'和R 12'可以相同或不同。

    Process for the preparation of halohydrocarbons
    16.
    发明授权
    Process for the preparation of halohydrocarbons 失效
    卤代烃的制备方法

    公开(公告)号：US6153803A

    公开(公告)日：2000-11-28

    申请号：US87852

    申请日：1998-06-01

    申请人： Jean-Paul Schoebrechts

    发明人： Jean-Paul Schoebrechts

    IPC分类号： C07B61/00 ,  C07C17/278 ,  C07C19/01 ,  C07C21/18 ,  C07C17/30

    CPC分类号： C07C17/278

    摘要： Halohydrocarbons comprising at least 3 carbon atoms are obtained by reaction between a haloalkane and a haloolefin in the presence of an organonickel compound as catalyst, and optionally in the presence of a solvent. 1,1,1,3,3-Pentachlorobutane can thus be obtained in good yield under mild conditions.

    摘要翻译： 包含至少3个碳原子的卤代烃通过在有机镍化合物作为催化剂的存在下，和任选地在溶剂的存在下，通过卤代烷烃和卤代烯烃之间的反应获得。 因此可以在温和条件下以良好的产率获得1,1,1,3,3-五氯代丁烷。