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    Reactor for producing a nitrile compound and method for operating the reactor
    12.
    发明申请
    Reactor for producing a nitrile compound and method for operating the reactor 有权
    用于生产腈化合物的反应器和操作反应器的方法

    公开(公告)号：US20050054855A1

    公开(公告)日：2005-03-10

    申请号：US10940652

    申请日：2004-09-15

    申请人： Shuichi Ueno ,  Takuji Shitara ,  Kenichi Nakamura ,  Fumisada Kosuge

    发明人： Shuichi Ueno ,  Takuji Shitara ,  Kenichi Nakamura ,  Fumisada Kosuge

    IPC分类号： B01J8/00 ,  B01J8/18 ,  C07C253/28 ,  C07C255/51 ,  F28D13/00 ,  C07C253/24 ,  C07D213/84

    CPC分类号： F28D13/00 ,  B01J8/0055 ,  B01J8/1836 ,  B01J2208/00132 ,  B01J2208/00725 ,  C07C253/28 ,  C07C255/51

    摘要： A reactor for producing a nitrile compound from a carbon ring or heterocyclic compound having organic substituents by a gas phase reaction using a fluidized catalyst bed with ammonia and a gas containing oxygen. In a cylindrical fluidized catalyst bed having a diameter of 2.0 meters or greater, partial vaporization-type cooling tubes (the cooling medium is partially vaporized in the tubes) and complete vaporization-type cooling tubes (the cooling medium is completely vaporized in the cooling tubes) are disposed in a specific arrangement. Water containing ionic SiO2 in 0.1 ppm or smaller and having an electric conductivity of 5 μS/cm or smaller is used as the cooling medium for the complete vaporization-type cooling tubes. The temperature of the reaction is easily stabilized and uniform distribution of temperature is obtained in the fluidized catalyst bed. Stable continuous operation is achieved for a long time in a commercial scale apparatus.

    摘要翻译： 一种反应器，其由具有有机取代基的碳环或杂环化合物通过气相反应使用流化催化剂床与氨和含氧气体制备。 在直径为2.0米或更大的圆柱形流化催化剂床中，部分气化型冷却管（冷却介质在管中部分蒸发）和完全蒸发式冷却管（冷却介质在冷却管中完全汽化 ）以特定的布置处理。 使用0.1ppm以下的导电率为5μS/ cm以下的离子性SiO 2的水作为完全蒸发式冷却管的冷却介质。 反应的温度容易稳定，在流化催化剂床中得到均匀的温度分布。 在商业规模的设备中长期实现稳定的连续操作。

    Process for producing a nitrile compound
    13.
    发明申请
    Process for producing a nitrile compound 审中-公开
    腈化合物的制造方法

    公开(公告)号：US20030114702A1

    公开(公告)日：2003-06-19

    申请号：US10310908

    申请日：2002-12-06

    发明人： Kenichi Nakamura ,  Shuji Ebata ,  Fumio Tanaka ,  Takuji Shitara

    IPC分类号： C07C253/28

    CPC分类号： B01J27/199 ,  B01J23/002 ,  B01J2523/00 ,  C07C253/28 ,  B01J2523/12 ,  B01J2523/13 ,  B01J2523/305 ,  B01J2523/51 ,  B01J2523/55 ,  B01J2523/67 ,  B01J2523/68 ,  C07C255/51

    摘要： In a process for producing a nitrile compound comprising introducing a carbon ring or heterocyclic compound having organic substituents, ammonia and the air into a reactor and reacting the introduced compounds in the presence of a catalyst, during the reaction, a residual gas obtained after the formed nitrile compound is separated from a reaction gas discharged from the reactor is recycled to the reactor in an amount of 10 to 60% by volume based on the amount of the fresh raw material gas supplied to the reactor and the ratio of the amount by mole of molecular oxygen to the amount by mole of the organic substituent in the carbon ring or heterocyclic compound having organic substituents supplied to the reactor (O2/organic substituent) is kept within 1.5 to 7. The reaction is achieved under an advantageous condition and the nitrile compound can be produced industrially advantageously at a higher yield.

    摘要翻译： 在制备腈化合物的方法中，包括将具有有机取代基的碳环或杂环化合物，氨和空气引入反应器中并在催化剂存在下使引入的化合物反应，在反应过程中获得的残余气体 将从反应器排出的反应气体中分离的腈化合物以供给反应器的新鲜原料气体的量为基准，以10〜60体积％的量循环至反应器， 分子氧与提供给反应器的有机取代基的碳环或杂环化合物（O 2 /有机取代基）中的有机取代基的摩尔比保持在1.5〜7的范围内。在有利条件下进行反应，并且腈化合物 可以以较高的产率在工业上有利地生产。