摘要:
Dioxane impurities in ether sulfates are removed by using a novel steam stripping technique in which water is neither added to nor removed from ether sulfate. This is possible because the chemical potential of water in the vapor phase is kept at the same value as that of water in the solution phase. In this way, thickening and foaming are avoided while dioxane levels can be reduced to below 10 parts per million by weight in a single pass.
摘要:
A process for the separation of sulphonated paraffins from their sulphonation medium, which comprises neutralization of the sulphuric acid present and separation into two phases, the lower phase containing the sulphate. The neutralization is carried out in such a way that only a part of the sulphuric acid is neutralized. A hydrocarbon is added, which dissolves the sulphonated and non-sulphonated paraffins and forms with water, an azeotropic mixture which is distilled in order to remove all or a part of the water present. The process allows the separation of sulphonates which are purer than in the past and which are poor in sulphates, while the sulphate layer contains only very little sulphonic acid.
摘要:
A method of bleaching olefin sulfonates, which comprises adding more than 0.1% by weight of hydrogen peroxide, with more than 0.1% by weight of phosphate alone or silicate alone or a mixture of the two, to an olefin sulfonate having 12 to 22 carbon atoms, and treating at a temperature in the range of from 30.degree. to 130.degree. C.
摘要:
Sulphonic acids and sulphonates containing olefines and optionally water which improve color and thermal stability and also simplify purification of the acid.
摘要:
A method of purifying crude, oil-soluble sulfonic acids is disclosed, wherein the method comprises contacting a volatile hydrocarbon solution of crude, oil-soluble sulfonic acids with 2methoxyethanol or a mixture of water and 2-methoxyethanol. Primarily, the term ''''purifying'''' means removal of sulfuric acid and sulfur oxides.
摘要:
Stabilized aqueous solutions of aliphatic unsaturated sulfonic acids which contain aliphatic chlorine compounds, and nickelplating baths containing said stabilized aqueous solutions as brighteners.
摘要:
A PROCESS FOR STABILIZIING THE PH OF SULFONATES OBTAINED FROM THE REACTION OF AN OLEFINIC COMPOUND WITH AN ALKALI BISULFITE WHICH INVOLVES CONTACTING AN AQUEOUS SLURRY OF SUCH SULFONATES CONTAINING AN ALKALINE COMPOUND WITH OXYGEN.
摘要:
AN AQUEOUS SOLUTION OF ALKALI PARAFFIN SULPHONATES HAVING A LOW CONTENT OF ALKALI SULPHATE IS OBTAINED FROM SULPHOXIDATION PRODUCTS BY SEPARATING THE MAIN PART OF THE HYDROTROPICALLY DISSOLVED PARAFFIN BY ADDITION OF A LOW MOLECULAR ALCOHOL, NEUTRALIZING THE AQUEOUS-ALCOHOLIC SOLUTION WITH AN ALKALI AND SEPARATING THE PRECIPITATED ALKALI SULPHATE.