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公开(公告)号：US06395912B1
公开(公告)日：2002-05-28
申请号：US08481105
申请日：1995-06-07
申请人： Stephen Neal Falling
发明人： Stephen Neal Falling
IPC分类号： C07D30728
CPC分类号： C07D307/28 , B01J21/08 , B01J23/06 , B01J31/0239 , B01J31/0268 , B01J31/122 , B01J31/26 , B01J2231/52
摘要： Disclosed are processes for the isomerization of epoxyalkenes to dihydrofurans by contacting an epoxyalkene with a catalyst comprising a quaternary organic onium iodide compounds, optionally deposited on a non-acidic support and/or in combination with a Lewis acid co-catalyst The catalyst may comprise a supported catalyst, an unsupported catalyst or a solution of the catalytically-active components in an inert, organic solvent.
摘要翻译： 公开了将环氧烯烃异构化为二氢呋喃的方法，该方法是将环氧烯烃与任选沉积在非酸性载体上和/或与路易斯酸助催化剂组合的季铵有机碘鎓化合物的催化剂接触。催化剂可以包含 负载型催化剂，无载体催化剂或催化活性组分在惰性有机溶剂中的溶液。
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公开(公告)号：US09114328B2
公开(公告)日：2015-08-25
申请号：US13473126
申请日：2012-05-16
CPC分类号： B01D3/009 , C07C29/149 , C07C51/12 , C07C51/44 , C07C67/08 , C07C67/54 , Y02P20/127 , C07C69/675 , C07C59/06 , C07C31/202 , C07C69/67
摘要： Disclosed is a process for producing glycolate ester oligomers. The process comprises reacting ethylene glycol and glycolic acid to produce a stream of glycolate ester oligomers and glycolic acid oligomers while simultaneously removing water. The stream of glycolate ester oligomers and glycolic acid oligomers has a low concentration of water and glycolic acid-ends, and thus is useful in a subsequent hydrogenation reaction to produce ethylene glycol.
摘要翻译： 公开了一种生产乙醇酸酯低聚物的方法。 该方法包括使乙二醇和乙醇酸反应以产生乙醇酸酯低聚物和乙醇酸低聚物流同时除去水。 乙醇酸酯低聚物和乙醇酸低聚物的水具有低浓度的水和乙醇酸末端，因此可用于随后的氢化反应以生产乙二醇。
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公开(公告)号：US06555595B1
公开(公告)日：2003-04-29
申请号：US09974010
申请日：2001-10-10
IPC分类号： C08F246
CPC分类号： C09D151/08 , C08F255/10 , C08F283/065 , C08F290/04 , C08F290/062 , C08F290/142 , C09D151/06 , Y10T428/31511 , Y10T428/31855
摘要： Disclosed are radiation-curable or photopolymerizable compositions, processes for applying and curing the compositions and articles bearing a cured coating of the compositions utilizing radiation-curable compositions which contain, in addition to the typical components of radiation-curable compositions, a polymer derived from 3,4-epoxy-1-butene.
摘要翻译： 公开了可辐射固化的或可光聚合的组合物，使用可辐射固化组合物施用和固化组合物和固化的组合物固化涂层的方法，除了可辐射固化组合物的典型组分外，还含有衍生自3 ，4-环氧-1-丁烯。
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24.发明授权Coating compositions based on polyether alcohols prepared from 3,4-epoxy-1-butene 失效基于由3,4-环氧-1-丁烯制备的聚醚醇的涂料组合物公开(公告)号：US06451926B1
公开(公告)日：2002-09-17
申请号：US09564860
申请日：2000-05-04
申请人： Thauming Kuo , Edward Enns McEntire , Stephen Neal Falling , Yao-Ching Liu , William Anthony Slegeir
发明人： Thauming Kuo , Edward Enns McEntire , Stephen Neal Falling , Yao-Ching Liu , William Anthony Slegeir
IPC分类号： C08L7102
CPC分类号： C09D163/00 , C08G65/14 , C08G65/2609 , C09D171/02 , C08L2666/02
摘要： EpB polyether alcohols were prepared by reacting 3,4-epoxy-1-butene with water or an alcohol such as methanol, butanol or ethylene glycol. Polyether alcohols thus prepared were found to have utility as reactive diluents for oxidatively curable coatings. In addition to this application, 3,4-epoxy-1-butene oligomers can also function as a resin, a chain extender, a monomer, and an additive for various oxidatively curable coating systems including alkyds, unsaturated polyesters, (meth)acrylate functional resins, urethanes, and latexes.
摘要翻译： 通过使3,4-环氧-1-丁烯与水或醇如甲醇，丁醇或乙二醇反应制备EpB聚醚醇。 发现由此制备的聚醚醇可用作氧化可固化涂料的反应性稀释剂。 除了该应用之外，3,4-环氧-1-丁烯低聚物还可用作树脂，扩链剂，单体和用于各种可氧化固化的涂料体系的添加剂，包括醇酸树脂，不饱和聚酯，（甲基）丙烯酸酯官能 树脂，聚氨酯和胶乳。
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公开(公告)号：US06201138B1
公开(公告)日：2001-03-13
申请号：US08481096
申请日：1995-06-07
IPC分类号： C07D30728
CPC分类号： C07D307/28 , B01J21/08 , B01J23/06 , B01J31/0239 , B01J31/0268 , B01J31/122 , B01J31/26 , B01J2231/52 , C07D307/08
摘要： Disclosed are processes for the isoberization of epoxyalkenes to dihydrofurans by contacting an epovyalkene with a catalyst comprising a quaternary organic onium iodide compounds, optionally deposited on a non-acidic support and/or in combination with a Lewis acid co-catalyst. The catalyst may comprise a supported catalyst, an unsupported catalyst or a solution of the catalytically-active components in an inert, organic solvent.
摘要翻译： 公开了通过使环戊烯与含有任选沉积在非酸性载体上和/或与路易斯酸助催化剂组合的季铵有机碘化铱化合物的催化剂使环氧烯烃与二氢呋喃类化合的方法。 催化剂可以包含负载型催化剂，无载体催化剂或催化活性组分在惰性有机溶剂中的溶液。
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公开(公告)号：US5693833A
公开(公告)日：1997-12-02
申请号：US701932
申请日：1996-08-26
CPC分类号： B01J31/122 , B01J31/4015 , C07D307/28 , C07F7/2216 , B01J2231/52 , B01J2531/42 , B01J27/08 , Y02P20/584
摘要： Disclosed is a process for converting an iodine-free organotin (IV) compound resulting from the decomposition of an organotin (IV) iodide during the catalytic isomerization of .gamma.,.delta.-epoxyalkenes to 2,5-dihydrofurans to the corresponding, catalytically active organotin (IV) iodide by intimately contacting a catalyst mixture comprising (i) an organotin (IV) iodide, (ii) an iodine-free organotin (IV) compound resulting from the decomposition of the organotin (IV) iodide of component (i), and (iii) a solvent selected from hydrocarbons and chlorocarbons with aqueous hydrogen iodide.
摘要翻译： 本发明公开了一种在γ，δ-环氧乙烷催化异构化至2,5-二氢呋喃期间将碘化有机锡（Ⅳ）分解产生的无碘有机锡（Ⅳ）化合物转化为相应的催化活性有机锡（ IV）碘化物，其通过紧密接触催化剂混合物，所述催化剂混合物包含（i）碘化有机锡（IV），（ii）由组分（i）的有机锡（IV）碘化物分解得到的无碘有机锡（IV）化合物和 （iii）选自烃和氯代烃的溶剂与碘化氢水溶液。
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公开(公告)号：US06342614B1
公开(公告)日：2002-01-29
申请号：US08194655
申请日：1994-02-10
申请人： Stephen Neal Falling
发明人： Stephen Neal Falling
IPC分类号： C07D30728
CPC分类号： C07D307/28 , B01J21/08 , B01J23/06 , B01J31/0239 , B01J31/0268 , B01J31/122 , B01J31/26 , B01J2231/52
摘要： Disclosed are processes for the isomerization of epoxyalkenes to dihydrofurans by contacting an epoxyalkene with a catalyst comprising a quaternary organic onium iodide compounds, optionally deposited on a non-acidic support and/or in combination with a Lewis acid co-catalyst. The catalyst may comprise a supported catalyst, an unsupported catalyst or a solution of the catalytically-active components in an inert, organic solvent.
摘要翻译： 公开了将环氧烯烃异构化为二氢呋喃的方法，其通过使环氧烯烃与包含季铵有机鎓碘化物的催化剂接触，任选地沉积在非酸性载体上和/或与路易斯酸助催化剂组合。 催化剂可以包含负载型催化剂，无载体催化剂或催化活性组分在惰性有机溶剂中的溶液。
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公开(公告)号：US06201139B1
公开(公告)日：2001-03-13
申请号：US08481103
申请日：1995-06-07
IPC分类号： C07D30728
CPC分类号： C07D307/28 , B01J21/08 , B01J23/06 , B01J31/0239 , B01J31/0268 , B01J31/122 , B01J31/26 , B01J2231/52 , C07D307/08
摘要： Disclosed are processes for the isomerization of epoxyalkenes to dihydrofurans by contacting an epoxyalkene with a catalyst comprising a quaternary organic onium iodide compounds, optionally deposited on a non-acidic support and/or in combination with a Lewis acid co-catalyst. The catalyst may comprise a supported catalyst, an unsupported catalyst or a solution of the catalytically-active components in an inert, organic solvent.
摘要翻译： 公开了将环氧烯烃异构化为二氢呋喃的方法，其通过使环氧烯烃与包含季铵有机鎓碘化物的催化剂接触，任选地沉积在非酸性载体上和/或与路易斯酸助催化剂组合。 催化剂可以包含负载型催化剂，无载体催化剂或催化活性组分在惰性有机溶剂中的溶液。
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29.发明授权Continuous process for the conversion of 2,5-dihydrofuran to 2,3-dihydrofuran 失效将2,5-二氢呋喃转化为2,3-二氢呋喃的连续方法
公开(公告)号：US5681969A
公开(公告)日：1997-10-28
申请号：US642544
申请日：1996-05-03
申请人： Timothy Richard Nolen , Stephen Neal Falling , David Martin Hitch , Jerry Lynn Miller , Daniel Latham Terrill
发明人： Timothy Richard Nolen , Stephen Neal Falling , David Martin Hitch , Jerry Lynn Miller , Daniel Latham Terrill
IPC分类号： C07B61/00 , C07D307/28 , C07D315/00
CPC分类号： C07D307/28
摘要： Disclosed is a process for the continuous production and recovery of 2,3-dihydrofuran (2,3-DHF) by the isomerization of 2,5-dihydrofuran (2,5-DHF) which contains certain impurities to 2,3-dihydrofuran in yields exceeding 95%. The process utilizes, in order, an isomerization zone containing one or more beds of a supported, palladium or platinum catalyst, a product recovery zone comprising a distillation column, a high boiler removal zone and means for feeding the 2,5-DHF component of the bottoms stream from the product recovery zone to the isomerization zone.
摘要翻译： 公开了通过将含有某些杂质的2,5-二氢呋喃（2,5-DHF）异构化为2,3-二氢呋喃的2,3-二氢呋喃（2,3-DHF）连续制备和回收2,3-二氢呋喃的方法， 产量超过95％。 该方法依次使用含有一个或多个载体，钯或铂催化剂床的异构化区，产物回收区，包含蒸馏塔，高锅炉去除区和用于将2,5-DHF组分进料的装置 底部物流从产物回收区到异构化区。
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公开(公告)号：US5663422A
公开(公告)日：1997-09-02
申请号：US609698
申请日：1996-03-01
CPC分类号： C07C67/26 , Y02P20/582
摘要： A process for the preparation of a 1,2-diacetoxy ester comprises acetylation of an epoxide with an acetic anhydride in the presence of a quaternary phosphonium acetate catalyst or its complex with acetic acid.
摘要翻译： 1,2-二乙酰氧基酯的制备方法包括在乙酸季鏻催化剂或其与乙酸的络合物存在下，用乙酸酐乙酰化环氧化物。
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