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    METHODS AND SYSTEMS FOR PROCESSING CELLULOSIC BIOMASS
    21.
    发明申请
    METHODS AND SYSTEMS FOR PROCESSING CELLULOSIC BIOMASS 审中-公开
    用于处理细胞生物质的方法和系统

    公开(公告)号：US20160184795A1

    公开(公告)日：2016-06-30

    申请号：US14980375

    申请日：2015-12-28

    Applicant: SHELL OIL COMPANY

    Inventor： Joseph Broun POWELL ,  Glenn Charles KOMPLIN ,  Juben Nemchand CHHEDA

    IPC: B01J19/24 ,  B01D3/14

    CPC classification number: B01J19/24 ,  B01D3/148 ,  B01J2219/24 ,  C10G1/002 ,  C10G1/065 ,  C10G1/083 ,  C10G3/50 ,  C10G2300/1014 ,  D21C3/20 ,  D21C3/222 ,  D21C11/0007 ,  D21C11/0042 ,  Y02P30/20

    Abstract: Separation of a product of digestion of cellulosic biomass solids may be challenging due to the various components contained therein. Methods and systems for processing cellulosic biomass, particularly a reaction product of a hydrothermal reaction containing lignin-derived products, such as phenolics, comprise providing the reaction product to a separation zone comprising a liquid-liquid phase separation unit. The liquid-liquid phase separation unit can provide an aqueous portion and a non-aqueous portion, where these portions can be separated into various fractions individually. For example, desirable compounds in the aqueous portion and non-aqueous portion can be recovered from the portions individually and optionally combined to be further processed into a fuels product. Heavier components in the aqueous portion and non-aqueous portion can be recovered from the portions individually and used in the process, such as phenolics that can be used as a digestion solvent.

    Abstract translation: 纤维素生物质固体的消化产物的分离可能是由于其中所含的各种组分而具有挑战性的。 用于处理纤维素生物质的方法和系统，特别是含有木质素衍生产物如酚醛的水热反应的反应产物包括将反应产物提供到包含液 - 液相分离单元的分离区。 液 - 液相分离装置可以提供水分和非水部分，其中这些部分可分别分成各种馏分。 例如，水性部分和非水部分中的期望的化合物可以从这些部分单独回收并任选地组合以进一步加工成燃料产物。 水性部分和非水部分中的较重组分可以单独回收并在该方法中使用，例如可用作消化溶剂的酚类。

    HYDROTHERMAL HYDROCATALYTIC TREATMENT OF BIOMASS USING WATER TOLERANT CATALYSTS
    23.
    发明申请
    HYDROTHERMAL HYDROCATALYTIC TREATMENT OF BIOMASS USING WATER TOLERANT CATALYSTS 有权
    使用耐水催化剂的生物质的氢热水解处理

    公开(公告)号：US20140165456A1

    公开(公告)日：2014-06-19

    申请号：US14133704

    申请日：2013-12-19

    Applicant: Shell Oil Company

    Inventor： Joseph Broun POWELL ,  Glenn Charles KOMPLIN ,  John Anthony SMEGAL ,  Kimberly Ann JOHNSON

    IPC: C10L1/18

    CPC classification number: C10L1/1802 ,  B01J21/04 ,  B01J23/86 ,  B01J23/88 ,  B01J23/882 ,  B01J35/0046 ,  B01J35/026 ,  B01J35/1009 ,  B01J35/1014 ,  B01J35/1066 ,  B01J37/0201 ,  B01J37/20 ,  C10G1/065 ,  C10G3/46 ,  C10G3/48 ,  C10G3/50 ,  C10G2300/1014 ,  Y02E50/13 ,  Y02P30/20

    Abstract: A method of hydrothermal hydrocatalytic treating biomass is provided. Lignocellulosic biomass solids is provided to a hydrothermal digestion unit in the presence of a digestive solvent, and a supported hydrogenolysis catalyst containing (a) sulfur, (b) Mo or W, and (c) Co, Ni or mixture thereof, incorporated into an alumina support, which support is predominantly alpha alumina; (ii) heating the lignocellulosic biomass solids and digestive solvent in the presence of hydrogen, and supported hydrogenolysis catalyst thereby forming a product solution containing plurality of oxygenated hydrocarbons, said alumina support having a specific surface area of up to about 30 m2/g and said catalyst retaining a crush strength of at least 50% after being subjected to an aqueous phase stability test compared with before the aqueous phase stability test or a crush strength of at least 0.25 kg after being subjected to an aqueous phase stability test.

    Abstract translation: 提供了一种水热催化处理生物质的方法。 将木质纤维素生物质固体在消化溶剂存在下提供给水热消解装置，以及负载的氢解催化剂，其包含（a）硫，（b）Mo或W，和（c）Co，Ni或其混合物， 氧化铝载体，其主要是α氧化铝; （ii）在氢气存在下加热木质纤维素生物质固体和消化溶剂，以及负载的氢解催化剂，由此形成含有多个含氧烃的产物溶液，所述氧化铝载体的比表面积高达约30m 2 / g，所述 在进行水相稳定性试验后，与水相稳定性试验相比，在进行水相稳定性试验后，在进行水相稳定性试验后，将至少50％的压碎强度保持在至少0.25kg的压碎强度。

    BIOMASS CONVERSION SYSTEMS AND METHODS FOR USE THEREOF
    25.
    发明申请
    BIOMASS CONVERSION SYSTEMS AND METHODS FOR USE THEREOF 审中-公开
    生物量转换系统及其使用方法

    公开(公告)号：US20140096764A1

    公开(公告)日：2014-04-10

    申请号：US14045262

    申请日：2013-10-03

    Applicant: SHELL OIL COMPANY

    Inventor： Glenn Charles KOMPLIN ,  Joseph Broun Powell

    IPC: C08B1/00

    CPC classification number: C08B1/00 ,  B01J3/008 ,  B01J2208/0053 ,  B01J2208/00557 ,  B01J2219/00038 ,  B01J2219/0004 ,  C10G1/002 ,  C10G1/065 ,  C10G3/44 ,  C10G2300/4081 ,  Y02P30/20

    Abstract: Digestion of cellulosic biomass solids to form a hydrolysate may be accompanied by decomposition if the soluble carbohydrates produced from the biomass under hydrothermal digestion conditions are not transformed into a more stable reaction product. Biomass conversion systems may be configured to address this issue and others. Biomass conversion systems can comprise: a hydrothermal digestion unit; a first catalytic reduction reactor unit fluidly coupled to the hydrothermal digestion unit along its height by two or more fluid inlet lines and two or more fluid return lines, the first catalytic reduction reactor unit containing a catalyst capable of activating molecular hydrogen; and a fluid circulation loop comprising the hydrothermal digestion unit and a second catalytic reduction reactor unit that contains a catalyst capable of activating molecular hydrogen.

    Abstract translation: 如果在水热消解条件下从生物质产生的可溶性碳水化合物不转化为更稳定的反应产物，则消化纤维素生物质固体以形成水解产物可伴随着分解。 生物量转换系统可能被配置为解决这个问题和其他问题。 生物质转化系统可包括：水热消解单元; 第一催化还原反应器单元，其通过两个或更多个流体入口管线和两个或更多个流体返回管线沿其高度流体耦合到水热消解单元，第一催化还原反应器单元含有能够活化分子氢的催化剂; 以及包含水热消解单元和含有能够活化分子氢的催化剂的第二催化还原反应器单元的流体循环回路。

    BIOMASS CONVERSION SYSTEMS CONTAINING A MOVING BED CATALYST FOR STABILIZATION OF A HYDROLSATE AND METHODS FOR USE THEREOF
    26.
    发明申请
    BIOMASS CONVERSION SYSTEMS CONTAINING A MOVING BED CATALYST FOR STABILIZATION OF A HYDROLSATE AND METHODS FOR USE THEREOF 审中-公开
    含有水解稳定剂的移动床催化剂的生物质转化体系及其使用方法

    公开(公告)号：US20140031599A1

    公开(公告)日：2014-01-30

    申请号：US13949936

    申请日：2013-07-24

    Applicant: Shell Oil Company

    Inventor： Glenn Charles KOMPLIN ,  Joseph Broun POWELL

    IPC: C10G1/00 ,  B01J8/04

    CPC classification number: C10G1/002 ,  B01J8/025 ,  B01J8/04 ,  B01J8/228 ,  B01J2208/00283 ,  B01J2208/003 ,  B01J2219/00006 ,  B01J2219/0004 ,  C10G1/065 ,  C10G1/083 ,  C10G3/44 ,  C10G3/52 ,  C10G2300/1011 ,  C10G2300/1014 ,  Y02P30/20

    Abstract: Digestion of cellulosic biomass solids to form a hydrolysate may be conducted with in situ catalytic reduction to transform soluble carbohydrates in the hydrolysate into a more stable reaction product. Biomass conversion systems for performing such a transformation can comprise: a hydrothermal digestion unit that also contains a first catalyst capable of activating molecular hydrogen, the first catalyst being fluidly mobile within the hydrothermal digestion unit; an optional hydrogen feed line that is operatively connected to the hydrothermal digestion unit; a fluid circulation loop comprising the hydrothermal digestion unit and a catalytic reduction reactor unit that contains a second catalyst capable of activating molecular hydrogen; and a catalyst transport mechanism external to the hydrothermal digestion unit, the catalyst transport mechanism being capable of conveying at least a portion of the first catalyst to another location from a catalyst collection zone located within the hydrothermal digestion unit.

    Abstract translation: 纤维素生物质固体的消化以形成水解产物可以通过原位催化还原进行，以将水解产物中的可溶性碳水化合物转化为更稳定的反应产物。 用于进行这种转化的生物量转化系统可以包括：水热消解单元，其还含有能够活化分子氢的第一催化剂，所述第一催化剂在所述水热消解单元内是可流动的; 可操作地连接到水热消解单元的氢供给管线; 流体循环回路，其包含水热消解单元和催化还原反应器单元，其包含能够活化分子氢的第二催化剂; 以及在所述水热消解单元外部的催化剂输送机构，所述催化剂输送机构能够将所述第一催化剂的至少一部分从位于所述水热消解单元内的催化剂收集区域输送到另一位置。

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