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    4-(3,3-dihalo-allyloxy) phenol derivatives having pesticidal properties
    21.
    发明授权
    4-(3,3-dihalo-allyloxy) phenol derivatives having pesticidal properties 失效
    具有杀虫特性的4-（3,3-二卤代烯丙氧基）苯酚衍生物

    公开(公告)号：US07608631B2

    公开(公告)日：2009-10-27

    申请号：US10525891

    申请日：2003-08-29

    申请人： Wemer Zambach ,  Arthur Steiger ,  Peter Renold ,  Stephan Trah ,  Roger Graham Hall

    发明人： Wemer Zambach ,  Arthur Steiger ,  Peter Renold ,  Stephan Trah ,  Roger Graham Hall

    IPC分类号： A01N43/40

    CPC分类号： C07D207/325 ,  A01N43/36 ,  A01N43/56 ,  A01N43/653 ,  A01N43/713 ,  A01N43/76 ,  A01N43/78 ,  A01N43/80 ,  A01N43/82 ,  A01N43/90 ,  A01N47/18 ,  A01N47/20 ,  C07D207/333 ,  C07D207/34 ,  C07D231/12 ,  C07D231/22 ,  C07D231/38 ,  C07D249/08 ,  C07D249/10 ,  C07D257/04 ,  C07D261/08 ,  C07D261/10 ,  C07D261/18 ,  C07D263/32 ,  C07D263/34 ,  C07D271/06 ,  C07D271/07 ,  C07D277/24 ,  C07D277/30 ,  C07D277/40 ,  C07D277/48 ,  C07D277/56 ,  C07D285/08 ,  C07D285/12 ,  C07D333/16 ,  C07D333/38 ,  C07D471/04

    摘要： Compounds of formula (I) wherein Ao is a bond or a C1-C6alkylene bridge; A1, A2 and A3 are a C1-C6alkylene bridge; D is CH or N; W is, for example, O, S, SO, S02, —C(═O)—O— or —O—C(═O)—; T is a bond or, for example, O, NH, S, SO or SR2; Q is, for example, O, S, SO or SO2; Y is, for example, O, S, SO or SO2; X1 and X2 are each independently of the other fluorine, chlorine or bromine; R1, R2 and R3 are, for example, H, halogen, OH, SH, CN or nitro; R4 is, for example, H, halogen, OH, SH, CN, nitro or C1-C6alkyl; R5 is, for example, H, CN, OH, C1-C6alkyl or C3-C8cycloalkyl; k is 1, 2 or 3 when D is nitrogen; or is 1, 2, 3 or 4 when D is CH; m is 1 or 2; E is heteroaryl which is unsubstituted or substituted—depending upon the substitutions possible on the ring—by from one to four identical or different substituents selected from R10; and R10 is, for example, halogen, CN, NO2, OH, SH or C1-C6alkyl; and, where applicable, their possible E/Z isomers, E/Z isomeric mixtures and/or tautomers, in each case in free form or in salt form, a process for the preparation of those compounds and their use, pesticidal compositions in which the active ingredient has been selected from those compounds or an agrochemically acceptable salt thereof, a process for the preparation of those compositions and their use, plant propagation material treated with those compositions, and a method of controlling pests.

    摘要翻译： 式（I）的化合物，其中Ao是一个键或C1-C6亚烷基桥; A1，A2和A3是C1-C6亚烷基桥; D是CH或N; W是例如O，S，SO，SO 2，-C（-O）-O-或-O-C（-O） - ; T是键或例如O，NH，S，SO或SR2; Q是例如O，S，SO或SO 2; Y是例如O，S，SO或SO 2; X1和X2各自独立地为氟，氯或溴; R1，R2和R3是例如H，卤素，OH，SH，CN或硝基; R4是例如H，卤素，OH，SH，CN，硝基或C1-C6烷基; R5是例如H，CN，OH，C1-C6烷基或C3-C8环烷基; 当D为氮时，k为1,2或3; 或D为CH时为1,2,3或4; m为1或2; E是未被取代或被取代的杂芳基，这取决于环上通过1-4个相同或不同的选自R 10的取代基取代的取代基; R 10为例如卤素，CN，NO 2，OH，SH或C 1 -C 6烷基; 在适用情况下，它们可能的E / Z异构体，E / Z异构体混合物和/或互变异构体，在每种情况下为游离形式或盐形式，制备这些化合物及其用途的方法，其中 从这些化合物或其农业化学上可接受的盐中选择活性成分，制备这些组合物的方法及其用途，用这些组合物处理的植物繁殖材料以及控制害虫的方法。

    Process for the preparation of pesticides
    26.
    发明授权
    Process for the preparation of pesticides 失效
    农药制备工艺

    公开(公告)号：US6156923A

    公开(公告)日：2000-12-05

    申请号：US762217

    申请日：1996-12-06

    申请人： Saleem Farooq ,  Stephan Trah ,  Hugo Ziegler ,  Rene Zurfluh

    发明人： Saleem Farooq ,  Stephan Trah ,  Hugo Ziegler ,  Rene Zurfluh

    IPC分类号： C07C249/04 ,  C07C249/12 ,  C07C251/48 ,  C07C251/60

    CPC分类号： C07C249/12 ,  C07C251/48 ,  C07C251/60

    摘要： The invention relates to a process for the preparation of compounds of the formula ##STR1## or, if appropriate, a tautomer thereof, in each case in the free form or in salt form, in whichA, X, Y, Z, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.7, R.sub.9 and n are as defined in claim 1 and the C.dbd.N double bond marked with E has the E configuration, which comprisesa1) reacting either a compound of the formula (II) mentioned above with a compound of the formula (III) mentioned above, in which X.sub.1 is a leaving group, ora2) a compound of the formula (IV) mentioned above, if appropriate in the presence of a base, with a compound of the formula (V) mentioned above, orb1) reacting a compound of the formula (VI) mentioned above with a compound of the formula R.sub.7 --A--X.sub.2 (VII), in which X.sub.2 is a leaving group, and either further reacting the compound thus obtainable, of the formula (IV), for example according to method a2), orb2) reacting it with hydroxylamine or a salt thereof, if appropriate in the presence of a basic or acid catalyst, and further reacting the compound thus obtainable, of the formula (II), for example according to method a1), orc) reacting a compound of the formula (VII), mentioned above with a C.sub.1 -C.sub.6 alkyl nitrite and further reacting the compound thus obtainable, of the formula (VI), for example according to method b), the E isomers of the compounds of the formulae (II), (IV) and (VI), a process for their preparation and their use for the preparation of compounds of the formula (I).

    摘要翻译： 本发明涉及一种制备下式的化合物或其合适的互变异构体的方法，其各自为游离形式或盐形式，其中A，X，Y，Z，R 2，R 3，R 4 ，R 5，R 7，R 9和n如权利要求1中所定义，并且用E标记的C = N双键具有E构型，其包括a1）使上述式（II）的化合物与 上述式（III），其中X1是离去基团，或a2）上述式（Ⅳ）化合物，如果合适，在碱的存在下，与上述式（Ⅴ）化合物， 或b1）使上述式（Ⅵ）化合物与式R7-A-X2（Ⅶ）化合物反应，其中X 2为离去基团，并进一步使由此得到的化合物（式（Ⅴ） IV），例如根据方法a2），或b2）如果合适，在碱性或酸性催化剂存在下，使其与羟胺或其盐反应， 进一步使由式（II）得到的化合物，例如按照方法a1）进行反应，或c）使上述式（Ⅶ）化合物与亚硝酸C 1 -C 6烷基酯反应，然后进一步使化合物 式（Ⅵ）化合物的E异构体，其制备方法及其制备方法（Ⅵ）的制备方法及其制备方法 式（I）的化合物。

    Triazoline and isoxazoline bis-oxime derivatives and their use as pesticides
    27.
    发明授权
    Triazoline and isoxazoline bis-oxime derivatives and their use as pesticides 失效
    三唑啉和异恶唑啉双肟衍生物及其作为农药的用途

    公开(公告)号：US5932583A

    公开(公告)日：1999-08-03

    申请号：US981116

    申请日：1997-12-23

    申请人： Hugo Ziegler ,  Stephan Trah ,  Rene Zurfluh ,  Anthony Cornelius O'Sullivan

    发明人： Hugo Ziegler ,  Stephan Trah ,  Rene Zurfluh ,  Anthony Cornelius O'Sullivan

    IPC分类号： A01N43/647 ,  A01N43/653 ,  A01N43/80 ,  C07C251/52 ,  C07C251/58 ,  C07C251/60 ,  C07C265/12 ,  C07C279/18 ,  C07C281/06 ,  C07C331/28 ,  C07C335/18 ,  C07D249/08 ,  C07D249/12 ,  C07D261/10 ,  C07D261/12 ,  C07D401/12 ,  C07D403/12 ,  C07D413/12 ,  C07D417/12 ,  A61K31/41 ,  A61K31/42 ,  C07C249/08

    CPC分类号： C07D261/10 ,  A01N43/647 ,  A01N43/80 ,  C07C251/52 ,  C07C251/58 ,  C07C251/60 ,  C07C265/12 ,  C07C279/18 ,  C07C331/28 ,  C07C335/18 ,  C07D249/12 ,  C07D261/12 ,  C07D401/12 ,  C07D403/12 ,  C07D413/12 ,  C07D417/12

    摘要： Bis-oxime derivatives of the formula I ##STR1## W is oxygen or sulfur, and the other substituents defined as follows: R.sub.1 =hydrogen, C.sub.1 -C.sub.4 alkyl; cyclopropyl;R.sub.2 =hydrogen, C.sub.1 -C.sub.6 alkyl; halo(C.sub.1 -C.sub.6) alkyl; C.sub.2 -C.sub.6 alkoxyalkyl; C.sub.3 -C.sub.6 cycloalkyl; substituted or unsubstituted aryl; substituted or unsubstituted heteroaryl; cyano; C.sub.1 -C.sub.6 alkoxycarbonyl; C.sub.1 -C.sub.6 alkyl-S(O).sub.n ; substituted or unsubstituted aryl-S(O).sub.n ; C.sub.1 -C.sub.6 alkoxy; substituted or unsubstituted aryloxy; substituted or unsubstituted heteroaryloxy; unsubstituted or mono- to trimethyl-substituted heterocyclyl; substituted or unsubstituted aryl-C.sub.1 -C.sub.6 alkyl; substituted or unsubstituted heteroaryl-C.sub.1 -C.sub.6 alkyl;R.sub.3 =hydrogen; C.sub.1 -C.sub.6 alkyl; C.sub.1 -C.sub.6 haloalkyl having 1 to 5 halogen atoms; C.sub.1 -C.sub.4 alkoxy-C.sub.1 -C.sub.2 -alkyl; unsubstituted or mono- to trihalo-substituted C.sub.1 -C.sub.6 alkenyl; C.sub.2 -C.sub.6 alkynyl; unsubstituted or mono- to tetrahalo-substituted C.sub.3 -C.sub.6 cycloalkyl-C.sub.1 -C.sub.4 alkyl;n=0 to 2;R.sub.8 =H, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 haloalkyl, C.sub.3 -C.sub.6 cycloalkyl;X=OR.sub.5, SR.sub.5, NR.sub.6 R.sub.7, halogen (especially Cl);R.sub.6, R.sub.7 =independently of one another H, C.sub.1 -C.sub.4 alkyl, C.sub.3 -C.sub.4 alkenyl, C.sub.3 -C.sub.4 alkynyl;R.sub.5 =C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.3 haloalkyl, are fungicidal, acaricidal and insecticidal active ingredients for agriculture. They can be employed as formulated crop protection compositions.

    摘要翻译： PCT No.PCT / EP96 / 02695 Sec。 371 1997年12月23日第 102（e）1997年12月23日PCT PCT 1996年6月21日PCT公布。 出版物WO97 / 02255 日期1997年1月23日式I W的双肟衍生物是氧或硫，其它取代基定义如下：R1 =氢，C1-C4烷基; 环丙基 R2 =氢，C1-C6烷基; 卤代（C 1 -C 6）烷基; C2-C6烷氧基烷基; C 3 -C 6环烷基; 取代或未取代的芳基; 取代或未取代的杂芳基; 氰基; C1-C6烷氧基羰基; C 1 -C 6烷基-S（O）n; 取代或未取代的芳基-S（O）n; C1-C6烷氧基; 取代或未取代的芳氧基; 取代或未取代的杂芳氧基; 未取代或单 - 三甲基取代的杂环基; 取代或未取代的芳基-C 1 -C 6烷基; 取代或未取代的杂芳基-C 1 -C 6烷基; R3 =氢; C1-C6烷基; 具有1至5个卤素原子的C 1 -C 6卤代烷基; C 1 -C 4烷氧基-C 1 -C 2 - 烷基; 未取代或单 - 三卤代取代的C 1 -C 6烯基; C2-C6炔基; 未取代或单 - 四卤代取代的C 3 -C 6环烷基-C 1 -C 4烷基; n = 0〜2; R8 = H，C1-C4烷基，C1-C4卤代烷基，C3-C6环烷基; X = OR5，SR5，NR6R7，卤素（特别是Cl）; R6，R7 =彼此独立地为H，C1-C4烷基，C3-C4链烯基，C3-C4炔基; R5 = C1-C4烷基，C1-C3卤代烷基，是农业的杀真菌，杀螨和杀虫活性成分。 它们可以用作配制的作物保护组合物。

    Insecticides
    28.
    发明授权
    Insecticides 有权
    杀虫剂

    公开(公告)号：US07812170B2

    公开(公告)日：2010-10-12

    申请号：US10598041

    申请日：2005-03-02

    申请人： David John Hughes ,  James Edward Peace ,  Suzanna Riley ,  Sally Russell ,  Joseph John Swanborough ,  Roger Graham Hall ,  André Jeanguenat ,  Olivier Loiseleur ,  Peter Renold ,  Stephan Trah ,  Jean Wenger

    发明人： David John Hughes ,  James Edward Peace ,  Suzanna Riley ,  Sally Russell ,  Joseph John Swanborough ,  Roger Graham Hall ,  André Jeanguenat ,  Olivier Loiseleur ,  Peter Renold ,  Stephan Trah ,  Jean Wenger

    IPC分类号： C07D401/00

    CPC分类号： C07D401/04 ,  A01N37/46 ,  A01N43/40 ,  A01N43/56 ,  C07D401/14 ,  C07D405/14 ,  C07D409/14 ,  C07D413/14 ,  C07D417/14 ,  C07D491/04 ,  C07D493/08 ,  C07D495/04 ,  C07D513/04

    摘要： Compounds of the formula (I) in which Z, is an oxygen atom; or a sulfur atom; Z2 is an oxygen atom; or a sulfur atom; R, is an aryl or heteroaryl group, which is unsubstituted or substituted; R2 is hydrogen; or an organic substituent; R3 is hydrogen; or an organic substituent; R4 is hydrogen; or an organic substituent; or R3 and R4, taken together, form, together with the nitrogen atom, to which they are attached, a ring, which is unsubstituted or substituted; R5 is hydrogen; or an unsubstituted or substituted alkyl group; or forms, taken together with R8 or with a monovalent substituent attached to that atom of R6, via which atom R6 is directly connected with the carbon atom, shown in the formula I, which carries R5, one additional bond; R6 and R7, taken together, form, together with the two carbon atoms, shown in the formula I, to which atoms they are attached, a bicyclic ring system, which ring system is carbocyclic or heterocyclic, which ring system is substituted, in the manner shown in the formula I, by the four substituents —N(R2)-C(═Z1)-R, —C(═Z2)-N(R3)-R4, R5 and R8, and which ring system is optionally further substituted; and R8 is hydrogen; or an unsubstituted or substituted alkyl group; or forms, taken together with R5 or with a monovalent substituent attached to that atom of R7, via which atom R7 is directly connected with the carbon atom, shown in the formula I, which carries R8, one additional bond, and, where appropriate, tautomers thereof, in each case in free form or in salt form, can be used as agrochemical active ingredients and can be prepared in a manner known per se.

    摘要翻译： 其中Z为氧原子的式（I）化合物; 或硫原子; Z2是氧原子; 或硫原子; R 1是未取代或取代的芳基或杂芳基; R2是氢; 或有机取代基; R3是氢; 或有机取代基; R4是氢; 或有机取代基; 或者R 3和R 4一起与它们所连接的氮原子一起形成未被取代或被取代的环， R5是氢; 或未取代或取代的烷基; 或其形式，与R8一起或与R6的该原子连接的一价取代基，其中原子R6直接与碳原子连接，如式I所示，其携带R5，另外一个键; R6和R7一起与式I中所示的两个碳原子一起形成，其中它们连接的原子是双环系统，该环系是碳环或杂环的，该环系被取代，在 式（I）所示的四种取代基-N（R 2）-C（= Z 1）-R，-C（= Z 2）-N（R 3）-R 4，R 5和R 8， 取代 R8是氢; 或未取代或取代的烷基; 或其形式与R5一起或与R7的原子连接的一价取代基，其中原子R7与碳原子直接连接，如式I所示，其携带R8，一个附加键，并且在适当的情况下， 互变异构体，以游离形式或盐形式，可以用作农业化学活性成分，并且可以以本身已知的方式制备。