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    Start-up method of bubble column slurry bed reactor
    32.
    发明授权
    Start-up method of bubble column slurry bed reactor 有权
    鼓泡塔浆床反应器启动方法

    公开(公告)号：US09376352B2

    公开(公告)日：2016-06-28

    申请号：US14387391

    申请日：2013-03-27

    Applicant: Japan Oil, Gas and Metals National Corporation ,  Inpex Corporation ,  JX Nippon Oil & Energy Corporation ,  Japan Petroleum Exploration Co., Ltd. ,  Cosmo Oil Co., Ltd. ,  Nippon Steel & Sumikin Engineering Co., Ltd.

    Inventor： Kazuhiko Tasaka

    IPC: C07C1/04 ,  C10G2/00

    CPC classification number: C07C1/0485 ,  C10G2/342 ,  C10G2300/4031

    Abstract: A start-up method of a bubble column slurry bed reactor for producing hydrocarbons includes: a first step that fills into a reactor a slurry in which a Fischer-Tropsch synthesis reaction catalyst particles are suspended in a slurry preparation oil with a 5% distillation point of 120 to 270° C., a 95% distillation point of 330 to 650° C., and a sulfur component and an aromatic component of 1 mass ppm or less, and a second step that, in a state where synthesis gas that is primarily hydrogen and carbon monoxide is introduced into the slurry filled into the reactor, raises the temperature of the reactor and starts the Fischer-Tropsch synthesis reaction. As the slurry preparation oil, one containing predetermined components in preset amounts is used. In the first step, the slurry is filled into the reactor in an amount in which airborne droplets do not flow out.

    Abstract translation: 用于生产烃的鼓泡塔淤浆床反应器的启动方法包括：第一步骤，向反应器中填充一种浆料，其中费 - 托合成反应催化剂颗粒悬浮在具有5％蒸馏点的浆料制备油中 120〜270℃，95％蒸馏点为330〜650℃，硫成分和1质量ppm以下的芳香族成分，第二工序为：在合成气为 主要将氢和一氧化碳引入填充到反应器中的浆料中，升高反应器的温度并开始费 - 托合成反应。 作为浆料制备油，使用含有预定量的预定组分的油。 在第一步骤中，将浆料以空气中的液滴不会流出的量装入反应器中。

    START-UP METHOD OF BUBBLE COLUMN SLURRY BED REACTOR
    37.
    发明申请
    START-UP METHOD OF BUBBLE COLUMN SLURRY BED REACTOR 有权
    泡沫柱塞式反应器的启动方法

    公开(公告)号：US20150087730A1

    公开(公告)日：2015-03-26

    申请号：US14387391

    申请日：2013-03-27

    Applicant: Japan Oil, Gas and Metals National Corporation ,  Inpex Corporation ,  JX Nippon Oil & Energy Corporation ,  Japan Petroleum Exploration Co., Ltd. ,  Cosmo Oil Co., Ltd. ,  Nippon Steel & Sumikin Engineering Co., Ltd.

    Inventor： Kazuhiko Tasaka

    IPC: C07C1/04

    CPC classification number: C07C1/0485 ,  C10G2/342 ,  C10G2300/4031

    Abstract: A start-up method of a bubble column slurry bed reactor for producing hydrocarbons includes: a first step that fills into a reactor a slurry in which a Fischer-Tropsch synthesis reaction catalyst particles are suspended in a slurry preparation oil with a 5% distillation point of 120 to 270° C., a 95% distillation point of 330 to 650° C., and a sulfur component and an aromatic component of 1 mass ppm or less, and a second step that, in a state where synthesis gas that is primarily hydrogen and carbon monoxide is introduced into the slurry filled into the reactor, raises the temperature of the reactor and starts the Fischer-Tropsch synthesis reaction. As the slurry preparation oil, one containing predetermined components in preset amounts is used. In the first step, the slurry is filled into the reactor in an amount in which airborne droplets do not flow out.

    Abstract translation: 用于生产烃的鼓泡塔淤浆床反应器的启动方法包括：第一步骤，向反应器中填充一种浆料，其中费 - 托合成反应催化剂颗粒悬浮在具有5％蒸馏点的浆料制备油中 120〜270℃，95％蒸馏点为330〜650℃，硫成分和1质量ppm以下的芳香族成分，第2工序中，在合成气为 主要将氢和一氧化碳引入填充到反应器中的浆料中，升高反应器的温度并开始费 - 托合成反应。 作为浆料制备油，使用预定量的预定组分。 在第一步骤中，将浆料以空气中的液滴不会流出的量装入反应器中。

    Hydrocarbon-reforming catalyst and a method of manufacturing thereof
    38.
    发明申请
    Hydrocarbon-reforming catalyst and a method of manufacturing thereof 有权
    烃重整催化剂及其制造方法

    公开(公告)号：US20040067848A1

    公开(公告)日：2004-04-08

    申请号：US10678288

    申请日：2003-10-03

    Applicant: Japan National Oil Corporation ,  Japan Petroleum Exploration Co., Ltd.

    Inventor： Toshiya Wakatsuki ,  Kiyoshi Inaba ,  Hideyuki Nakajima ,  Eiichi Hosoya

    IPC: B01J023/58

    CPC classification number: B01J23/75 ,  B01J23/755 ,  B01J23/78 ,  B01J35/006 ,  B01J35/0066 ,  B01J35/1009 ,  B01J35/1014 ,  B01J37/0201 ,  C01B3/40 ,  C01B2203/0233 ,  C01B2203/0238 ,  C01B2203/1052 ,  C01B2203/1241 ,  C01B2203/1247 ,  Y02P20/142 ,  Y02P20/52

    Abstract: A porous preform (carrier) is soaked in an impregnating solution, which contains both of a catalytic-activity constituent, e.g. Ni and/or Co, and a carrier-forming constituent, e.g. Mg, Al, Zr, Ti and/or Ca, so as to simultaneously infiltrate the catalytic-activity and carrier-forming constituents into the porous preform. The impregnated preform is dried, calcined at a temperature of 700null C. or higher and then activated at a temperature of 500null C. or higher, whereby fine catalytic-activity particles are distributed on a surface of the porous carrier with high dispersion. Due to finely-distributed catalytic-activity particles, the surface of the catalyst is prevented from deposition of carbonaceous matters during reformation of hydrocarbon and held in an active state over a long term.

    Abstract translation: 将多孔预成型体（载体）浸渍在浸渍溶液中，浸渍溶液含有催化活性成分，例如， Ni和/或Co，以及载体形成成分，例如 Mg，Al，Zr，Ti和/或Ca，以便同时将催化活性和载体形成成分渗透到多孔预制件中。 将浸渍的预成型件干燥，在700℃以上的温度下煅烧，然后在500℃以上的温度下活化，由此精细的催化活性颗粒以高分散性分布在多孔载体的表面上。 由于精细分布的催化活性颗粒，催化剂的表面被阻止在碳氢化合物的改性过程中沉积碳质物质并长期保持在活性状态。

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