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    Method for preparing and using a soluble metal pentafluoride-hydrogen fluoride catalyst
    31.
    发明授权
    Method for preparing and using a soluble metal pentafluoride-hydrogen fluoride catalyst 失效
    制备和使用可溶性金属五氟化氢 - 氟化氢催化剂的方法

    公开(公告)号：US4105704A

    公开(公告)日：1978-08-08

    申请号：US758054

    申请日：1976-12-29

    Applicant: Geoffrey R. Say ,  William C. Baird, Jr.

    Inventor： Geoffrey R. Say ,  William C. Baird, Jr.

    IPC: B01J27/12 ,  C07C2/54 ,  C07C5/22 ,  C07C3/52 ,  C07C5/24

    CPC classification number: C07C5/2253 ,  B01J27/12 ,  C07C2/54 ,  C07C2527/1206 ,  C07C2527/133 ,  Y10S585/906

    Abstract: A soluble HF/TaF.sub.5 catalyst is prepared in the absence of an organic solvent according to the steps of:(1) contacting tantalum metal with substantially anhydrous liquid HF to form soluble TaF.sub.5, the amount of HF being sufficient to maintain the TaF.sub.5 thus formed as a homogeneous substantially liquid phase catalyst at a temperature ranging from about 0.degree. to 150.degree. C.,(2) contacting the catalyst thus formed with a hydrocarbon feedstock in a hydrocarbon conversion process to form an acid catalyst phase and a hydrocarbon product phase,(3) stripping HF from said catalyst phase with a gas containing molecular hydrogen thereby reducing the mole ratio of HF to TaF.sub.5, and(4) passing the stripped acid catalyst phase from step (3) to the hydrocarbon conversion process, thereby maintaining the mole ratio of HF to TaF.sub.5 within said process at a level between that obtained in step (1) and step (3).

    Abstract translation: 根据以下步骤在不存在有机溶剂的情况下制备可溶性HF / TaF 5催化剂：

    Desulfurization and hydroconversion of residua with alkaline earth metal compounds and hydrogen
    32.
    发明授权
    Desulfurization and hydroconversion of residua with alkaline earth metal compounds and hydrogen 失效
    残渣与碱土金属化合物和氢的脱硫和加氢转化

    公开(公告)号：US4087348A

    公开(公告)日：1978-05-02

    申请号：US733085

    申请日：1976-10-18

    Applicant: William C. Baird, Jr. ,  Roby Bearden, Jr.

    Inventor： William C. Baird, Jr. ,  Roby Bearden, Jr.

    IPC: C10G45/04 ,  C10G13/04 ,  B01J27/04

    CPC classification number: C10G29/00 ,  C10G45/04

    Abstract: Sulfur-containing petroleum oil feedstocks which include heavy hydrocarbon constituents undergo simultaneous desulfurization and hydroconversion by contacting such feedstocks with alkaline earth metal hydrides or alkaline earth metal oxides, particularly barium hydride or barium oxide, in the presence of hydrogen, and at elevated temperatures. The mixtures of reaction products resulting from the above procedure can be separated to give a petroleum oil product which has been substantially desulfurized and demetallized and significantly upgraded as demonstrated by reduced Conradson carbon content, and increased API gravity and which includes alkaline earth metal sulfide salts from which the alkaline earth metal hydrides or oxides may be regenerated.

    Abstract translation: 包括重质烃成分的含硫石油原料通过在氢气存在下和在升高的温度下接触这些原料与碱土金属氢化物或碱土金属氧化物，特别是氢化钡或氧化钡同时进行脱硫和加氢转化。 由上述程序产生的反应产物的混合物可以分离，得到一种石油产品，其已被基本上脱硫和脱金属化并​​显着升级，如通过减少的康拉逊碳含量和增加的API重力所证明的，并且其包括碱土金属硫化物盐 碱土金属氢化物或氧化物可以再生。

    Selectively suppressed hydrogenation catalyst
    34.
    发明授权
    Selectively suppressed hydrogenation catalyst 有权
    选择性抑制加氢催化剂

    公开(公告)号：US07612012B2

    公开(公告)日：2009-11-03

    申请号：US11234668

    申请日：2005-09-22

    Applicant: Garland B. Brignac ,  Michele S. Touvelle ,  William C. Baird, Jr.

    Inventor： Garland B. Brignac ,  Michele S. Touvelle ,  William C. Baird, Jr.

    IPC: B01J23/44

    CPC classification number: C10G45/10 ,  B01J23/85 ,  B01J31/02 ,  B01J37/18 ,  B01J37/20 ,  C10G45/04 ,  C10G45/08 ,  C10G2400/02

    Abstract: The hydrogenation activity of a heteroatom removal catalyst, having activity for both heteroatom removal and hydrogenation, is selectively suppressed by a treatment which comprises contacting the catalyst with (i) hydrogen, (ii) a selectively deactivating agent that suppresses the catalyst's hydrogenation activity, and (iii) a protective agent, such as CO, that preserves and protects the heteroatom removal activity during the treatment. This may be achieved in a reactor while it is on-line and removing heteroatoms from a hydrocarbon feed.

    Abstract translation: 通过包括使催化剂与（i）氢，（ii）抑制催化剂的氢化活性的选择性钝化剂接触的处理，选择性地抑制具有除去杂原子和加氢两者的活性的杂原子除去催化剂的加氢活性，以及 （iii）在处理期间保留并保护杂原子除去活性的保护剂，例如CO。 这可以在反应器中实现，同时其在线并且从烃进料中除去杂原子。

    High activity, high yield tin modified platinum-iridium catalysts, and reforming process utilizing such catalysts
    38.
    发明授权
    High activity, high yield tin modified platinum-iridium catalysts, and reforming process utilizing such catalysts 失效
    高活性，高含量的改性铂 - 铱催化剂，以及利用这种催化剂的改性方法

    公开(公告)号：US5106809A

    公开(公告)日：1992-04-21

    申请号：US627528

    申请日：1990-12-14

    Applicant: William C. Baird, Jr. ,  George A. Swan, III ,  Joseph P. Boyle

    Inventor： William C. Baird, Jr. ,  George A. Swan, III ,  Joseph P. Boyle

    IPC: B01J23/62 ,  C10G35/09

    CPC classification number: C10G35/09 ,  B01J23/626

    Abstract: Tin modified platinum-iridium catalysts provide high yields of C.sub.5 + liquid reformate in catalytic reforming, concurrent with high activity. In particular, the tin modified platinum-iridium catalysts are of unusually high selectivity, as contrasted with known iridium promoted platinum catalysts. The high selectivity is manifested in reforming a naphtha feed in a reactor charged to capacity with the catalyst, but particularly when used in the dehydrocyclization zone, or tail reactor of a series of reactors, while the lead reactors of the series contain a non tin-containing platinum catalyst, especially a platinum-iridium, or a platinum-rhenium catalyst. The tin modified platinum-iridium catalysts are also highly active, with only moderate loss in the high activity for which iridium stabilized platinum catalysts are known.

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