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公开(公告)号：US20060182892A9
公开(公告)日：2006-08-17
申请号：US10248056
申请日：2002-12-13
CPC分类号： C23C28/321 , C21D7/06 , C23C4/18 , C23C8/02 , C23C26/00 , C23C28/345 , C23C28/3455 , Y10T428/12611 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944
摘要： A beta-phase nickel aluminide (NiAl) overlay coating (24) and method for modifying the grain structure of the coating (24) to improve its oxidation resistance. The coating (24) is deposited by a method that produces a grain structure characterized by grain boundaries (44) exposed at the outer coating surface (36). The grain boundaries (44) may also contain precipitates (40) as a result of the alloyed chemistry of the coating (24). During or after deposition, the overlay coating (24) is caused to form new grain boundaries (34) that, though open to the outer surface (36) of the coating (24), are free of precipitates or contain fewer precipitates (40) than the as-deposited grain boundaries (44). New grain boundaries (34) are preferably produced by causing the overlay coating (24) to recrystallize during coating deposition or after deposition as a result of a surface treatment followed by heat treatment.
摘要翻译： β相镍铝化合物（NiAl）覆盖层（24）以及用于改变涂层（24）的晶粒结构以提高其抗氧化性的方法。 通过产生以在外涂层表面（36）处暴露的晶界（44）为特征的晶粒结构的方法沉积涂层（24）。 由于涂层（24）的合金化学，晶界（44）也可含有沉淀物（40）。 在沉积期间或之后，使覆盖涂层（24）形成新的晶粒边界（34），其尽管向涂层（24）的外表面（36）开口，但没有沉淀物或含有较少的沉淀物（40） 比沉积的晶界（44）。 优选通过在涂布沉积期间或沉积后的覆盖涂层（24）进行再结晶，然后进行热处理后的表面处理，来制造新的晶界（34）。
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32.发明申请Thermal barrier coating/environmental barrier coating system for a ceramic-matrix composite (CMC) article to improve high temperature capability 有权陶瓷基复合材料（CMC）制品的隔热涂层/环境屏障涂层系统，以提高高温能力公开(公告)号：US20060121293A1
公开(公告)日：2006-06-08
申请号：US11006292
申请日：2004-12-06
申请人： Brett Boutwell , Irene Spitsberg , Christine Govern , Bangalore Nagaraj , Brian Hazel , Ramgopal Darolia , Curtis Johnson , Yan Gao , Mark Gorman
发明人： Brett Boutwell , Irene Spitsberg , Christine Govern , Bangalore Nagaraj , Brian Hazel , Ramgopal Darolia , Curtis Johnson , Yan Gao , Mark Gorman
CPC分类号： C04B41/009 , C04B41/52 , C04B41/89 , C04B2111/0025 , C23C28/042 , C23C28/322 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/2118 , F05D2300/50211 , F05D2300/611 , C04B41/4527 , C04B41/5096 , C04B41/5035 , C04B41/522 , C04B41/5024 , C04B41/5037 , C04B41/5031 , C04B41/5042 , C04B41/5044 , C04B41/4529 , C04B35/565 , C04B35/584 , C04B35/806
摘要： In accordance with an embodiment of the invention, an article is provided. The article comprises a substrate comprised of silicon containing material, an environmental barrier coating (EBC) overlying the substrate and a thermal barrier coating (TBC) on the environmental barrier coating. The thermal barrier coating comprising a compound having a rhombohedral phase.
摘要翻译： 根据本发明的实施例，提供了一种制品。 该制品包括由含硅材料构成的衬底，覆盖衬底的环境阻挡涂层（EBC）和环境屏障涂层上的热障涂层（TBC）。 该热障涂层包含具有菱面体相的化合物。
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公开(公告)号：US06974637B2
公开(公告)日：2005-12-13
申请号：US10707543
申请日：2003-12-19
申请人： Jeffrey Allan Pfaendtner , Deborah A. Schorr , Ramgopal Darolia , Joseph David Rigney , Irene Spitsberg , William Scott Walston
发明人： Jeffrey Allan Pfaendtner , Deborah A. Schorr , Ramgopal Darolia , Joseph David Rigney , Irene Spitsberg , William Scott Walston
CPC分类号： C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2220/3212 , F05D2300/13 , Y10T428/12611 , Y10T428/12736 , Y10T428/1275 , Y10T428/12875 , Y10T428/12944 , Y10T428/12986
摘要： An article and TBC coating system thereon that in combination exhibit significantly improved spallation resistance. The article comprises a substrate formed of a metal alloy containing ruthenium and one or more refractory elements (e.g., tantalum, tungsten, molybdenum, rhenium, hafnium, etc.). The substrate is protected by a coating system comprising an aluminum-containing bond coat on the surface of the substrate and a ceramic coating bonded to the substrate by the bond coat. The bond coat, preferably an aluminide, is deposited so as to be substantially free of ruthenium, though ruthenium is present in the bond coat as a result of diffusion from the substrate into the bond coat.
摘要翻译： 其上的一种制品和TBC涂层体系组合显示出显着改善的防剥落性。 该制品包括由含有钌和一种或多种难熔元素（例如钽，钨，钼，铼，铪等）的金属合金形成的基材。 基材由包括基材表面的含铝粘合涂层的涂层体系和通过粘合涂层粘合到基材上的陶瓷涂层保护。 沉积粘合涂层，优选铝化物，以便基本上不含钌，尽管由于从基材扩散到粘合涂层中，钌存在于粘合涂层中。
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34.发明申请Ceramic compositions for thermal barrier coatings stabilized in the cubic crystalline phase 审中-公开用于隔热涂层的陶瓷组合物稳定在立方晶相公开(公告)号：US20050142393A1
公开(公告)日：2005-06-30
申请号：US10748517
申请日：2003-12-30
申请人： Brett Boutwell , Mark Gorman , Irene Spitsberg , Ramgopal Darolia , Robert Bruce , Venkat Venkataramani
发明人： Brett Boutwell , Mark Gorman , Irene Spitsberg , Ramgopal Darolia , Robert Bruce , Venkat Venkataramani
IPC分类号： C04B35/486 , C04B37/02 , C23C14/08 , C23C28/00 , C23C30/00 , F01D5/28 , B32B9/00 , C23C16/00
CPC分类号： F01D5/288 , B82Y30/00 , C04B35/486 , C04B2235/3206 , C04B2235/3208 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3251 , C04B2235/3286 , C04B2235/781 , C04B2235/9607 , C23C14/08 , C23C14/083 , C23C28/321 , C23C28/3215 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/2118 , F05D2300/611 , Y10T428/12611 , Y10T428/26
摘要： Zirconia-containing ceramic compositions that are capable of providing thermal barrier coatings wherein the zirconia is stabilized in the cubic crystalline phase. These compositions comprise at least about 50 mole % zirconia and a stabilizing amount up to about 49 mole % of a stabilizer component comprising: (1) a first metal oxide selected from the group consisting of ytterbia, neodymia, mixtures of ytterbia and neodymia, mixtures of ytterbia and lanthana, mixtures of neodymia and lanthana, and mixtures of ytterbia, neodymia and lanthana in an amount of from about 5 to about 49 mole % of the composition; and (2) a second metal oxide selected from the group consisting of yttria, calcia, ceria, scandia, magnesia, india and mixtures thereof in an amount of about 4 mole % or less of the composition. The ceramic composition further comprises one or more of a third metal oxide selected from the group consisting of: (a) hafnia in an amount from about 0.5 to about 40 mole % of the composition; and (b) tantala in an amount of from about 0.5 to about 10 mole % of the composition. These compositions are useful in preparing thermal barrier coatings for an underlying substrate of articles that operate at, or are exposed to, high temperatures.
摘要翻译： 能够提供热障涂层的含氧化锆的陶瓷组合物，其中氧化锆稳定在立方晶体相中。 这些组合物包含至少约50摩尔％的氧化锆和至多约49摩尔％的稳定剂组分的稳定剂组分，其包含：（1）选自下列组的第一金属氧化物：镱，钕，镱和钕的混合物，混合物 镱和镧的混合物，钕和镧的混合物，以及组合物的约5至约49摩尔％的镱，钕和镧的混合物; 和（2）选自组合物的约4摩尔％以下的量的氧化钇，氧化钙，二氧化铈，钪，氧化镁，印度及其混合物的第二金属氧化物。 所述陶瓷组合物还包含选自以下的一种或多种第三金属氧化物：（a）组合物的约0.5至约40摩尔％的量的铪; 和（b）所述组合物的约0.5至约10摩尔％的量的黄铁矿。 这些组合物可用于制备在高温下操作或暴露于其中的制品的下层基材的热障涂层。
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35.发明申请公开(公告)号：US20050136283A1
公开(公告)日：2005-06-23
申请号：US10707543
申请日：2003-12-19
申请人： Jeffrey Pfaendtner , Deborah Schorr , Ramgopal Darolia , Joseph Rigney , Irene Spitsberg , William Walston
发明人： Jeffrey Pfaendtner , Deborah Schorr , Ramgopal Darolia , Joseph Rigney , Irene Spitsberg , William Walston
CPC分类号： C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2220/3212 , F05D2300/13 , Y10T428/12611 , Y10T428/12736 , Y10T428/1275 , Y10T428/12875 , Y10T428/12944 , Y10T428/12986
摘要： An article and TBC coating system thereon that in combination exhibit significantly improved spallation resistance. The article comprises a substrate formed of a metal alloy containing ruthenium and one or more refractory elements (e.g., tantalum, tungsten, molybdenum, rhenium, hafnium, etc.). The substrate is protected by a coating system comprising an aluminum-containing bond coat on the surface of the substrate and a ceramic coating bonded to the substrate by the bond coat. The bond coat, preferably an aluminide, is deposited so as to be substantially free of ruthenium, though ruthenium is present in the bond coat as a result of diffusion from the substrate into the bond coat.
摘要翻译： 其上的一种制品和TBC涂层体系组合显示出显着改善的防剥落性。 该制品包括由含有钌和一种或多种难熔元素（例如钽，钨，钼，铼，铪等）的金属合金形成的基材。 基材由包括基材表面的含铝粘合涂层的涂层体系和通过粘合涂层粘合到基材上的陶瓷涂层保护。 沉积粘合涂层，优选铝化物，以便基本上不含钌，尽管由于从基材扩散到粘合涂层中，钌存在于粘合涂层中。
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公开(公告)号：US06887589B2
公开(公告)日：2005-05-03
申请号：US10249564
申请日：2003-04-18
申请人： Ramgopal Darolia , Joseph David Rigney , William Scott Walston , Jeffrey Allan Pfaendtner , Brett Allen Rohrer Boutwell , Irene Spitsberg , James Anthony Ruud
发明人： Ramgopal Darolia , Joseph David Rigney , William Scott Walston , Jeffrey Allan Pfaendtner , Brett Allen Rohrer Boutwell , Irene Spitsberg , James Anthony Ruud
CPC分类号： C23C28/321 , C23C4/02 , C23C4/12 , C23C14/06 , C23C28/3215 , C23C28/324 , C23C28/345 , C23C28/3455 , Y10T428/12576 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12771 , Y10T428/12806 , Y10T428/12944 , Y10T428/252
摘要： A beta-phase NiAl overlay coating containing a dispersion of ceramic particles and a process for depositing the overlay coating. If the coating is used to adhere a thermal barrier coating (TBC), the TBC exhibits improved spallation resistance as a result of the dispersion of ceramic particles having a dispersion-strengthening effect on the overlay coating. The overlay coating contains at least one reactive element and is deposited so that the some of the reactive element deposits as the ceramic particles dispersed in the overlay coating.
摘要翻译： 含有陶瓷颗粒分散体的β相NiAl覆盖涂层和沉积覆盖层的方法。 如果涂层用于粘附热障涂层（TBC），则由于在覆盖涂层上具有分散强化作用的陶瓷颗粒的分散，TBC显示出改进的抗剥落性。 覆盖层包含至少一个反应性元件并沉积成使得一部分反应性元素沉积为陶瓷颗粒分散在覆盖层中。
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公开(公告)号：US20050064104A1
公开(公告)日：2005-03-24
申请号：US10710112
申请日：2004-06-18
申请人： Ramgopal Darolia , Boris Movchan , Yuriy Rudoy , Leonella Nerodenko , Irene Spitsberg , David Wortman
发明人： Ramgopal Darolia , Boris Movchan , Yuriy Rudoy , Leonella Nerodenko , Irene Spitsberg , David Wortman
CPC分类号： C23C28/3215 , C23C14/06 , C23C28/321 , C23C28/345 , C23C28/3455 , C23C30/00 , F01D5/288 , F05D2300/15 , Y10T428/249954 , Y10T428/249956 , Y10T428/249957 , Y10T428/249976 , Y10T428/24999
摘要： A thermal barrier coating, or TBC, and method for forming the TBC. The TBC is formed of a thermal-insulating material that contains yttria-stabilized zirconia (YSZ) alloyed with at least a third oxide. The TBC is formed to also contain elemental carbon, and may potentially contain carbides and/or a carbon-containing gas that forms from the thermal decomposition of carbon. The TBC is characterized by lower density and thermal conductivity, high temperature stability and improved mechanical properties. To exhibit the desired effect, the third oxide is more particularly one that increases the lattice strain energy of the TBC microstructure as a result of having an ion size that is sufficiently different than a zirconium ion.
摘要翻译： 热障涂层或TBC，以及形成TBC的方法。 TBC由含有与至少第三氧化物合金的氧化钇稳定的氧化锆（YSZ）的绝热材料形成。 TBC形成也含有元素碳，并且可能含有从碳的热分解形成的碳化物和/或含碳气体。 TBC具有较低的密度和导热性，高温稳定性和改善的机械性能。 为了表现出期望的效果，由于具有与锆离子充分不同的离子尺寸的结果，第三氧化物更特别地增加了TBC微结构的晶格应变能。
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公开(公告)号：US08100083B2
公开(公告)日：2012-01-24
申请号：US12883386
申请日：2010-09-16
IPC分类号： C23C16/00
摘要： A process and apparatus for depositing a ceramic coating, such as a thermal barrier coating (TBC) for a gas turbine engine component. The process deposits a coating whose composition includes multiple oxide compounds and a carbon-based constituent, e.g., elemental carbon, carbides, and carbon-based gases. The process uses at least one evaporation source to provide multiple different oxide compounds and at least one carbide compound comprising carbon and an element. The evaporation source is evaporated to produce a vapor cloud that contacts and condenses on the component surface to form the ceramic coating, and particularly so that the coating comprises the oxide compounds, an oxide of the element of the carbide compound, and the carbide compound and/or a carbon-containing gas. The process is carried out with an apparatus comprising a coating chamber in which the evaporation source is present, and a device for evaporating the evaporation source.
摘要翻译： 一种用于沉积陶瓷涂层的方法和装置，例如用于燃气涡轮发动机部件的热障涂层（TBC）。 该方法沉积涂层，其组成包括多种氧化物化合物和碳基组分，例如元素碳，碳化物和碳基气体。 该方法使用至少一个蒸发源来提供多种不同的氧化物化合物和至少一种包含碳和元素的碳化物。 蒸发源被蒸发以产生在组件表面上接触和冷凝以形成陶瓷涂层的蒸汽云，特别是使涂层包含氧化物化合物，碳化物化合物的元素的氧化物和碳化物化合物，以及 /或含碳气体。 该方法使用包括其中存在蒸发源的涂布室和用于蒸发蒸发源的装置的装置进行。
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公开(公告)号：US07824744B2
公开(公告)日：2010-11-02
申请号：US10707469
申请日：2003-12-16
IPC分类号： C23C14/30
摘要： A process and apparatus for depositing a ceramic coating, such as a thermal barrier coating (TBC) for a gas turbine engine component. The process deposits a coating whose composition includes multiple oxide compounds and a carbon-based constituent, e.g., elemental carbon, carbides, and carbon-based gases. The process uses at least one evaporation source to provide multiple different oxide compounds and at least one carbide compound comprising carbon and an element. The evaporation source is evaporated to produce a vapor cloud that contacts and condenses on the component surface to form the ceramic coating, and particularly so that the coating comprises the oxide compounds, an oxide of the element of the carbide compound, and the carbide compound and/or a carbon-containing gas. The process is carried out with an apparatus comprising a coating chamber in which the evaporation source is present, and a device for evaporating the evaporation source.
摘要翻译： 一种用于沉积陶瓷涂层的方法和装置，例如用于燃气涡轮发动机部件的热障涂层（TBC）。 该方法沉积涂层，其组成包括多种氧化物化合物和碳基组分，例如元素碳，碳化物和碳基气体。 该方法使用至少一个蒸发源来提供多种不同的氧化物化合物和至少一种包含碳和元素的碳化物。 蒸发源被蒸发以产生在组件表面上接触和冷凝以形成陶瓷涂层的蒸汽云，特别是使涂层包含氧化物化合物，碳化物化合物的元素的氧化物和碳化物化合物，以及 /或含碳气体。 该方法使用包括其中存在蒸发源的涂布室和用于蒸发蒸发源的装置的装置进行。
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公开(公告)号：US07393416B2
公开(公告)日：2008-07-01
申请号：US10709668
申请日：2004-05-21
CPC分类号： C23C16/52 , C23C14/08 , C23C14/30 , C23C14/564
摘要： An apparatus for depositing a ceramic coating on a component. The apparatus includes an evaporation source containing multiple different oxide compounds, at least one of the oxide compounds having a vapor pressure that is higher than the remaining oxide compounds, to deposit on the component a coating of the multiple oxide compounds. The apparatus further includes a device for introducing the evaporation source into a coating chamber, a device for suspending the component near the evaporation source, a device for projecting a high-energy beam on the evaporation source to melt and form a vapor cloud of the oxide compounds of the evaporation source, a device capable of preventing the vapor cloud from contacting and condensing on the component, and a device for moving the preventing device to allow the vapor cloud to contact and condense on the component.
摘要翻译： 一种用于在组件上沉积陶瓷涂层的装置。 所述装置包括含有多种不同氧化物化合物的蒸发源，所述氧化物化合物中的至少一种具有比剩余的氧化物化合物高的蒸汽压，以在所述组分上沉积所述多种氧化物化合物的涂层。 该装置还包括用于将蒸发源引入涂覆室的装置，用于将部件悬浮在蒸发源附近的装置，用于将高能束投影到蒸发源上以熔化并形成氧化物蒸汽云的装置 蒸发源的化合物，能够防止蒸气云在部件上接触和冷凝的装置，以及用于使防止装置移动以允许蒸汽云接触并冷凝在部件上的装置。
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