公开(公告)号：US09889542B2

公开(公告)日：2018-02-13

申请号：US15379878

申请日：2016-12-15

Applicant: Baker Hughes Incorporated

Inventor： Danny E. Scott ,  Anthony A. DiGiovanni

IPC: B24D18/00 ,  B24D3/14 ,  B24D99/00 ,  B01J3/06 ,  B24D3/06 ,  E21B10/55

CPC classification number: B24D18/0009 ,  B01J3/06 ,  B01J2203/062 ,  B01J2203/0645 ,  B24D3/06 ,  B24D3/14 ,  B24D99/005 ,  E21B10/55

Abstract: Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high-pressure, high-temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.

公开(公告)号：US09868099B2

公开(公告)日：2018-01-16

申请号：US13091660

申请日：2011-04-21

Applicant: Anthony A. DiGiovanni

Inventor： Anthony A. DiGiovanni

IPC: B24D3/02 ,  C09C1/68 ,  C09K3/14 ,  B01J3/06 ,  E21B10/567 ,  F16C33/04

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/0685 ,  E21B10/567 ,  F16C33/043 ,  F16C2352/00

Abstract: Grains of superabrasive material may be infiltrated with a molten metal alloy at a relatively low temperature, and the molten metal alloy may be solidified within interstitial spaces between the grains of superabrasive material to form a solid metal alloy having the grains of superabrasive material embedded therein. The solid metal alloy with the grains of superabrasive material embedded therein may be subjected to a high pressure and high temperature process to form a polycrystalline superabrasive material. A polycrystalline superabrasive material also may be formed by depositing material on surfaces of grains of superabrasive material in a chemical vapor infiltration process to form a porous body, which then may be subjected to a high pressure and high temperature process. Polycrystalline compacts and cutting elements including such compacts may be formed using such methods.

公开(公告)号：US09409280B2

公开(公告)日：2016-08-09

申请号：US13416201

申请日：2012-03-09

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B24D18/00 ,  B28D1/12 ,  B01J3/06 ,  B24D3/06

CPC classification number: B24D18/0009 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B24D3/06 ,  B24D18/0027 ,  B28D1/121 ,  B28D1/127

Abstract: Superabrasive tools and methods for the making thereof are disclosed and described. In one aspect, superabrasive particles are chemically bonded to a matrix support material according to a predetermined pattern by a braze alloy. The brazing alloy may be provided as a powder, thin sheet, or sheet of amorphous alloy. A template having a plurality of apertures arranged in a predetermined pattern may be used to place the superabrasive particles on a given substrate or matrix support material.

公开(公告)号：US20150283674A1

公开(公告)日：2015-10-08

申请号：US14743159

申请日：2015-06-18

Applicant: Baker Hughes Incorporated

Inventor： Danny E. Scott ,  Anthony A. DiGiovanni

IPC: B24D3/14 ,  B24D18/00

CPC classification number: B24D18/0009 ,  B01J3/06 ,  B01J2203/062 ,  B01J2203/0645 ,  B24D3/06 ,  B24D3/14 ,  B24D99/005 ,  E21B10/55

Abstract: Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high-pressure, high-temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.

Abstract translation: 公开了用于形成切割元件的方法，用于形成多晶压块的方法和相关的多晶压块。 对硬质材料的颗粒进行高压高温处理以形成多晶压块。 在另外的平稳温度或压力阶段期间，将系统压力或温度中的至少一个相对较快的尖峰包含在颗粒之间形成颗粒间结合。 高峰阶段的简洁可以避免不必要的晶粒生长。 方法的实施例还可以包括振荡至少一个系统状态（例如，压力，温度）和使晶粒经受超声或机械振动中的至少一个。 所得到的多晶压块可以包括具有最小量的催化剂材料的高密度颗粒间结合的硬质材料，并且可以在使用结合多晶压块的切割元件时提供改善的热稳定性，耐磨性，韧性和性能。

公开(公告)号：US09067304B2

公开(公告)日：2015-06-30

申请号：US13618927

申请日：2012-09-14

Applicant: Danny E. Scott ,  Anthony A. DiGiovanni

Inventor： Danny E. Scott ,  Anthony A. DiGiovanni

IPC: B24D3/00 ,  B24D3/14 ,  B24D18/00 ,  B24D99/00

CPC classification number: B24D18/0009 ,  B01J3/06 ,  B01J2203/062 ,  B01J2203/0645 ,  B24D3/06 ,  B24D3/14 ,  B24D99/005 ,  E21B10/55

Abstract: Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high-pressure, high-temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.

Abstract translation: 公开了用于形成切割元件的方法，用于形成多晶压块的方法和相关的多晶压块。 对硬质材料的颗粒进行高压高温处理以形成多晶压块。 在另外的平稳温度或压力阶段期间，将系统压力或温度中的至少一个相对较快的尖峰包含在颗粒之间形成颗粒间结合。 高峰阶段的简洁可以避免不必要的晶粒生长。 方法的实施例还可以包括振荡至少一个系统状态（例如，压力，温度）和使晶粒经受超声或机械振动中的至少一个。 所得到的多晶压块可以包括具有最小量的催化剂材料的高密度颗粒间结合的硬质材料，并且可以在使用结合多晶压块的切割元件时提供改善的热稳定性，耐磨性，韧性和性能。

公开(公告)号：US20140090307A1

公开(公告)日：2014-04-03

申请号：US14027606

申请日：2013-09-16

Applicant: DIAMOND INNOVATIONS, INC.

Inventor： Shuang Ji ,  Christopher Long ,  Susanne Sowers ,  Kai Zhang

IPC: C09K3/14

CPC classification number: C09K3/1409 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068

Abstract: A superabrasive material and method of making the superabrasive material are provided. The superabrasive material may comprise a superabrasive crystal having an irregular surface. The superabrasive material further comprises a plurality of structure defects within the superabrasive crystal. The plurality of structure defects may cause micro-chipping when used as grinding materials.

Abstract translation: 提供了一种超研磨材料和制造该超级磨料的方法。 超研磨材料可以包括具有不规则表面的超级磨料晶体。 超级磨料材料还包括超研磨晶体内的多个结构缺陷。 当用作研磨材料时，多种结构缺陷可能导致微切削。

公开(公告)号：US20140000177A1

公开(公告)日：2014-01-02

申请号：US13925264

申请日：2013-06-24

Applicant: DIAMOND INNOVATIONS, INC.

Inventor： Kai Zhang

IPC: C09K3/14

CPC classification number: C09K3/1409 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  C01B21/064 ,  C01B21/0648 ,  C01P2004/03 ,  C01P2004/30 ,  C01P2004/61 ,  C01P2004/80 ,  C01P2004/82 ,  C01P2006/21 ,  C04B35/62836 ,  C04B2235/386 ,  C04B2235/5427 ,  C04B2235/5436 ,  C09K3/1436

Abstract: A superabrasive material and method of making the superabrasive material are provided. The superabrasive material may comprise a core and an outgrown region. The core may have a single crystal structure. The outgrown region may also contain a single crystal. The single crystal may extend outwards from the core. The outgrown region may have a lower toughness index than that of the core.

Abstract translation: 提供了一种超研磨材料和制造该超级磨料的方法。 超研磨材料可以包括芯和越野区域。 芯可以具有单晶结构。 超出区域也可以含有单晶。 单晶可以从芯向外延伸。 长出的区域的韧性指数可能低于核心区域。

公开(公告)号：US08529696B2

公开(公告)日：2013-09-10

申请号：US13561695

申请日：2012-07-30

Applicant: Kenji Watanabe ,  Takashi Taniguchi ,  Satoshi Koizumi ,  Hisao Kanda ,  Masayuki Katagiri ,  Takatoshi Yamada ,  Nesladek Milos

Inventor： Kenji Watanabe ,  Takashi Taniguchi ,  Satoshi Koizumi ,  Hisao Kanda ,  Masayuki Katagiri ,  Takatoshi Yamada ,  Nesladek Milos

IPC: C30B9/00

CPC classification number: C30B29/38 ,  B01J3/062 ,  B01J3/065 ,  B01J2203/0645 ,  B01J2203/066 ,  B01J2203/069 ,  C09K11/63 ,  H01S5/32341

Abstract: A method for producing hexagonal boron nitride single crystals including mixing boron nitride crystals with a solvent thereby obtaining a mixture, heating and melting the mixture under high-temperature and high-pressure thereby obtaining a melted mixture, and recrystallizing the melted mixture thereby producing hexagonal boron nitride single crystals, wherein the solvent is boronitride of alkaline earth metal, or boronitride of alkali metal and the boronitride of alkaline earth metal.

Abstract translation: 一种生产六方氮化硼单晶的方法，包括将氮化硼晶体与溶剂混合从而获得混合物，在高温高压下加热熔化混合物，从而获得熔融混合物，并将熔融混合物重结晶，从而产生六方硼 氮化物单晶，其中溶剂是碱土金属的硼氮化物，碱金属的硼氮化物和碱土金属的硼氮化物。

公开(公告)号：US08404010B2

公开(公告)日：2013-03-26

申请号：US12518745

申请日：2007-12-13

Applicant: Steven W. Webb

Inventor： Steven W. Webb

IPC: B24D3/04 ,  B24D3/14 ,  B24D3/34

CPC classification number: B24D3/342 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0685 ,  C09K3/1436 ,  C22C26/00 ,  C22C2026/007 ,  C22C2026/008

Abstract: An abrasive compact may include an ultra-hard phase that may include ultra-hard particles having a Knoop hardness of 5000 KHN or greater, a sinter catalyst, and a reaction phase that may include a catalyst-ceramic compound having a Knoop hardness lower than that of the ultra-hard phase.

公开(公告)号：US20130067825A1

公开(公告)日：2013-03-21

申请号：US13618927

申请日：2012-09-14

Applicant: Danny E. Scott ,  Anthony A. DiGiovanni

Inventor： Danny E. Scott ,  Anthony A. DiGiovanni

IPC: B24D3/04 ,  B24D18/00

CPC classification number: B24D18/0009 ,  B01J3/06 ,  B01J2203/062 ,  B01J2203/0645 ,  B24D3/06 ,  B24D3/14 ,  B24D99/005 ,  E21B10/55

Abstract: Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high pressure, high temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.

Abstract translation: 公开了用于形成切割元件的方法，用于形成多晶压块的方法和相关的多晶压块。 将硬质材料的颗粒进行高压高温处理以形成多晶压块。 在另外的平稳温度或压力阶段期间，将系统压力或温度中的至少一个相对较快的尖峰包含在颗粒之间形成颗粒间结合。 高峰阶段的简洁可以避免不必要的晶粒生长。 方法的实施例还可以包括振荡至少一个系统状态（例如，压力，温度）和使晶粒经受超声或机械振动中的至少一个。 所得到的多晶压块可以包括具有最小量的催化剂材料的高密度颗粒间结合的硬质材料，并且可以在使用结合多晶压块的切割元件时提供改善的热稳定性，耐磨性，韧性和性能。