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    Cyclic amine based polymers and process for their production
    52.
    发明授权
    Cyclic amine based polymers and process for their production 有权
    循环胺基聚合物及其生产方法

    公开(公告)号：US6111056A

    公开(公告)日：2000-08-29

    申请号：US153307

    申请日：1998-09-15

    申请人： Soren Hildebrandt ,  Elisabeth Kappes ,  Dieter Boeckh ,  Rajan Panandiker ,  Sherri Randall ,  Eugene Paul Gosselink ,  William Conrad Wertz

    发明人： Soren Hildebrandt ,  Elisabeth Kappes ,  Dieter Boeckh ,  Rajan Panandiker ,  Sherri Randall ,  Eugene Paul Gosselink ,  William Conrad Wertz

    IPC分类号： C08G73/02 ,  C08G73/06 ,  C11D3/00 ,  C11D3/22 ,  C11D3/37 ,  C11D3/382 ,  C08G69/00 ,  C08F8/02 ,  C08G12/00 ,  C08L79/02

    CPC分类号： C08G73/0273 ,  C08G73/02 ,  C08G73/022 ,  C08G73/0616 ,  C11D3/0015 ,  C11D3/225 ,  C11D3/227 ,  C11D3/3723 ,  C11D3/3776

    摘要： A cyclic amine containing polymer substantially free of primary and secondary amino groups which is prepared by reacting:a) an amine selected from the group consisting of:i) cyclic amines having at least one nitrogen atom in the ring and at least one primary amino alkyl group bonded to the nitrogen atom of the ring, andii) mixtures of cyclic amines containing at least two nitrogen atoms which react with a cross-linking agent with at least one other amine containing 1-6 nitrogen atoms which react with a cross-linking agent, withb) at least one cross-linker selected from the group consisting of at least one compound containing two groups which react with the primary amino group and said nitrogen atoms and mixtures of at least one compound containing two groups which react with the primary amino group and said nitrogen atoms with at least one compound containing at least three groups which react with the primary amino group and said nitrogen atoms in a molar ratio of (a):(b) of from 2.5:1 to 1:1.5 thereby forming a cyclic amine containing polymer containing primary or secondary amino groups and reacting said cyclic amine based polymer, withc) an alkylating agent selected from the group consisting of epoxides, alkyl halides, arylalkyl halides, dimethyl sulfate, diethyl sulfate, mixtures of formic acid and an aldehyde, and mixtures of formic acid and a ketone, to convert more than 80% of the primary and secondary nitrogen groups into tertiary nitrogen groups.

    摘要翻译： 一种基本上不含伯和仲氨基的含环胺的聚合物，其通过以下方法制备：a）选自以下的胺：i）环中具有至少一个氮原子的环胺和至少一个伯氨基烷基 基团与环的氮原子键合，以及ii）含有至少两个氮原子的环状胺的混合物，其与交联剂与至少一种含有1-6个氮原子的其它胺反应，其与交联反应 其中b）至少一个选自至少一种含有两个与伯氨基和所述氮原子反应的基团的化合物的交联剂以及至少一种含有两个与主要氨基反应的基团的化合物的混合物 氨基和所述氮原子与至少一种含有至少三个与伯氨基和所述氮原子反应的化合物，其摩尔比为（a）：（b）为2 1.5:1至1:1.5，由此形成含有伯胺或仲氨基的含环胺的聚合物，并使所述环胺基聚合物与c）选自环氧化物，烷基卤，芳烷基卤化物，二甲基 硫酸盐，二乙基硫酸盐，甲酸和醛的混合物，以及甲酸和酮的混合物，将80％以上的初级和次级氮基团转化为叔氮基团。

    Use of polycationic condensation products as an additive for detergents or detergent after treatment agents in order to inhibit running of colors and to reduce color loss
    53.
    发明授权
    Use of polycationic condensation products as an additive for detergents or detergent after treatment agents in order to inhibit running of colors and to reduce color loss 有权
    使用聚阳离子缩合产物作为洗涤剂或洗涤剂后处理剂的添加剂，以抑制颜色的运行并减少色差

    公开(公告)号：US6025322A

    公开(公告)日：2000-02-15

    申请号：US284479

    申请日：1999-04-21

    申请人： Dieter Boeckh ,  Hans-Ulrich Jager ,  Jurgen Alfred Lux

    发明人： Dieter Boeckh ,  Hans-Ulrich Jager ,  Jurgen Alfred Lux

    IPC分类号： D06L1/02 ,  C11D3/00 ,  C11D3/37 ,  C11D3/30 ,  C11D1/835

    CPC分类号： C11D3/3723 ,  C11D3/0021 ,  C11D3/3776

    摘要： Polycationic condensates obtainable by condensing(a) piperazine, 1-alkylpiperazines having 1 to 25 carbon atoms in the alkyl group, 1,4-dialkylpiperazines having 1 to 25 carbon atoms in the alkyl group, 1,4-bis(3-aminopropyl)piperazine, 1-(2-aminoethyl)piperazine, 1-(2-hydroxyalkyl)piperazines having 2 to 25 carbon atoms in the alkyl group, imidazole, C.sub.1 -C.sub.25 -alkylimidazoles or mixtures of said compounds with(b) alkylene dihalides, epihalohydrins and/or bisepoxidesin the molar ratio from 1:0.8 to 1:1.1 and, where appropriate, quaternization of the condensates with C.sub.4 -C.sub.25 -alkylating agents or by heating triethanolamine or triisopropanolamine in the presence of acidic catalysts and quaternizing the condensates with C.sub.4 -C.sub.25 -alkylating agents as color-fixing additive to detergents and fabric conditioners, and detergents which comprise(i) 1-50% by weight of at least one nonionic surfactant,(ii) 0-4.0% by weight of an anionic surfactant and(iii) 0.05-2.5% by weight of the polycationic condensateare used as color transfer inhibiting and color release reducing additive, and fabric conditioners which comprise a fabric softener, a nonionic surfactant and 0.1-2.5% by weight of said polycationic condensates.

    摘要翻译： PCT No.PCT / EP97 / 05606 Sec。 371 1999年4月21日第 102（e）1999年4月21日PCT PCT 1997年10月10日PCT公布。 公开号WO98 / 17762 日期：1998年04月30日通过缩合（a）在烷基中具有1至25个碳原子的哌嗪，1-烷基哌嗪，在烷基中具有1至25个碳原子的1,4-二烷基哌嗪，1,4-双 （3-氨基丙基）哌嗪，1-（2-氨基乙基）哌嗪，烷基中具有2至25个碳原子的1-（2-羟烷基）哌嗪，咪唑，C 1 -C 25烷基咪唑或所述化合物与（b ）亚烷基二卤化物，表卤代醇和/或双过氧化物，摩尔比为1:0.8至1:1.1，并且在适当时，缩合物与C 4 -C 25烷基化试剂季铵化或通过在酸性催化剂存在下加热三乙醇胺或三异丙醇胺，和 用C4-C25-烷基化剂作为着色固定添加剂对洗涤剂和织物调理剂季铵化缩合物，以及洗涤剂，其包含（i）1-50重量％的至少一种非离子表面活性剂，（ii）0-4.0重量％ 的阴离子表面活性剂和（iii）0.05-2.5重量％的t 使用聚阳离子缩合物作为转色抑制和减色添加剂，以及包含织物柔软剂，非离子表面活性剂和0.1-2.5重量％所述聚阳离子缩合物的织物调理剂。

    Process for preparing fine-particle mixtures of amphiphilic polymers and inorganic solids
    55.
    发明授权
    Process for preparing fine-particle mixtures of amphiphilic polymers and inorganic solids 失效
    制备两亲聚合物和无机固体的微粒混合物的方法

    公开(公告)号：US5834548A

    公开(公告)日：1998-11-10

    申请号：US836205

    申请日：1997-05-16

    申请人： Hans-Ulrich Jager ,  Dieter Boeckh ,  Ulrich Brockel ,  Frank Muller ,  Gunnar Schornick

    发明人： Hans-Ulrich Jager ,  Dieter Boeckh ,  Ulrich Brockel ,  Frank Muller ,  Gunnar Schornick

    IPC分类号： C11D3/02 ,  C08J3/20 ,  C08K7/00 ,  C11D3/37 ,  C11D11/00 ,  C08G63/20

    CPC分类号： C11D11/0082 ,  C08J3/201 ,  C08K7/00 ,  C11D3/046 ,  C11D3/3715 ,  C11D3/3788

    摘要： Finely divided mixtures of 97-10% by weight of at least one amphiphilic polymer whose softening point is above 35.degree. C., and 3-90% by weight of at least one inorganic solid with a particle size not exceeding 500 .mu.m are prepared by heating the two components to a temperature which is above the softening point of the polymer, mixing the components, dispersing the melt and rapidly cooling to a temperature at which virtually no inhomogeneity occurs and, where appropriate, further comminuting the particles at temperatures below 50.degree. C. to a particle size of from 50 .mu.m to 5 mm, and are used as additive to detergents.

    摘要翻译： PCT No.PCT / EP95 / 04373 Sec。 371日期：1997年5月16日 102（e）日期1997年5月16日PCT提交1995年11月7日PCT公布。 公开号WO96 / 16149 日期：1996年5月30日将至少一种软化点高于35℃的至少一种两亲性聚合物和3-90重量％至少一种粒度不超过500的无机固体的97-10重量％ 通过将两种组分加热到高于聚合物软化点的温度，混合组分，分散熔体并迅速冷却至几乎不发生不均匀性的温度，并在适当情况下进一步粉碎颗粒， 在50℃以下，粒度为50〜5mm，用作洗涤剂的添加剂。

    Preparation of polycondensates of citric acid and use thereof in detergents and cleaners
    56.
    发明授权
    Preparation of polycondensates of citric acid and use thereof in detergents and cleaners 失效
    柠檬酸缩聚物的制备及其在洗涤剂和清洁剂中的应用

    公开(公告)号：US5652330A

    公开(公告)日：1997-07-29

    申请号：US515806

    申请日：1995-08-16

    申请人： Dieter Boeckh ,  Angelika Funhoff ,  Alexander Kud ,  Richard Baur ,  Volker Schwendemann ,  Gunnar Schornick

    发明人： Dieter Boeckh ,  Angelika Funhoff ,  Alexander Kud ,  Richard Baur ,  Volker Schwendemann ,  Gunnar Schornick

    IPC分类号： C02F5/12 ,  C08G63/06 ,  C08G69/44 ,  C11D3/37 ,  C08F6/00 ,  C08J3/00

    CPC分类号： C02F5/12 ,  C08G63/06 ,  C08G69/44 ,  C11D3/3757

    摘要： Process for preparing polycondensates of citric acid and/or isocitric acid, by converting(a) citric acid, isocitric acid or mixtures thereof in an organic solvent in the presence of a water-withdrawing agent at least partially into the anhydride form and then condensing the reaction mixture, if desired after addition of two cocondensable compounds selected from the group consisting of(b) other hydroxycarboxylic acids and/or(c) amino acids, alcohols, amines and/or at least dibasic carboxylic acids other than carboxylic acids (a) and (b), at temperatures of at least 80.degree. C. to form polycarboxylates which have an average molecular weight of at least 500, polycondensates of citric acid and/or isocitric acid obtainable thereby, anduse of said polycondensates as ingredients in phosphate-free and reduced-phosphate detergents and cleaners, and also detergents and cleaners which contain at least one surfactant and optionally builders and other customary constituents with from 0.1 to 30% by weight of an abovementioned polyestercarboxylate.

    摘要翻译： 通过在吸水剂存在下，在有机溶剂中将（a）柠檬酸，异柠檬酸或其混合物至少部分转化成酸酐形式，然后将（a）柠檬酸和/或异柠檬酸的缩聚物 （b）其它羟基羧酸和/或（c）氨基酸，醇，胺和/或除羧酸以外的至少二元羧酸（a）中的两种可共缩合化合物，如果需要， 和（b）中，在至少80℃的温度下形成平均分子量至少为500的聚羧酸酯，由此得到的柠檬酸和/或异柠檬酸的缩聚物，以及所述缩聚物作为磷酸盐 - 游离和还原磷酸盐洗涤剂和清洁剂，以及含有至少一种表面活性剂和任选的助洗剂和其它常规组分的洗涤剂和清洁剂，其含量为0.1-30％ 重量的上述聚酯羧酸酯。

    Water-soluble copolymers, their preparation and their use
    58.
    发明授权
    Water-soluble copolymers, their preparation and their use 失效
    水溶性共聚物，其制备及其用途

    公开(公告)号：US4952655A

    公开(公告)日：1990-08-28

    申请号：US183611

    申请日：1988-04-19

    申请人： Hans-Peter Seelmann-Eggebert ,  Dieter Boeckh ,  Heinrich Hartmann ,  Wolfgang Trieselt ,  Alexander Kud

    发明人： Hans-Peter Seelmann-Eggebert ,  Dieter Boeckh ,  Heinrich Hartmann ,  Wolfgang Trieselt ,  Alexander Kud

    IPC分类号： A01N25/26 ,  C08F2/10 ,  C08F20/10 ,  C08F220/04 ,  C08F220/20 ,  C08F290/00 ,  C08F299/00 ,  C08L101/16

    CPC分类号： C08F220/04 ,  A01N25/26

    摘要： Water-soluble copolymers having a K value of from 15 to 120 (determined on the sodium salt according to H. Fikentscher in aqueous solution at 25.degree. C., a pH of 7 and a polymer concentration of the Na salt of 1% by weight) contain, in the polymerized form,(a) from 99.5 to 80 mol % of one or more monoethylenically unsaturated C.sub.3 -C.sub.6 -monocarboxylic acids and(b) from 0.5 to 20 mol % of one or more comonomers which possess two or more ethylenically unsaturated, non-conjugated double bonds, are derived from esters and are obtainable by esterification of(b1) monoethylenically unsaturated C.sub.3 -C.sub.6 -monocarboxylic acids with(b2) polyhydric alcohols of 2 to 6 carbon atoms, polyalkylene glycols, polyglycerols, polyvinyl alcohol and monohydric, monoethylenically unsaturated C.sub.3 -C.sub.6 -alcohols and(c) from 0 to 30 mol % of other water-soluble, monoethylenically unsaturated monomers which are copolymerizable with (a) and (b),the copolymers containing polymer segments which consist of units of the monomers (a) and (c), have a weight average molecular weight of not more than 15,000 and are bonded to one another via units of (b).

    摘要翻译： K值为15〜120的水溶性共聚物（根据H.Fikentscher的钠盐在25℃的水溶液中测定，pH为7，Na盐的聚合物浓度为1重量％ ）包含（a）99.5-80mol％的一种或多种单烯属不饱和C 3 -C 6 - 单羧酸和（b）0.5至20摩尔％的一种或多种具有两个或多个烯键式的共聚单体的共聚单体 不饱和的非共轭双键衍生自酯，可通过（b1）单烯属不饱和C3-C6-单羧酸与（b2）2至6个碳原子的多元醇酯，聚亚烷基二醇，聚甘油，聚乙烯醇和 一元，单烯属不饱和C 3 -C 6醇和（c）0至30摩尔％可与（a）和（b）共聚的其它水溶性单烯属不饱和单体，所述共聚物含有聚合物链段， monom （a）和（c）的重均分子量不大于15,000，通过（b）单元彼此结合。

    Detergents containing water-soluble copolymers containing as copolymerized units monomers having two or more ethylenically unsaturated double bonds
    59.
    发明授权
    Detergents containing water-soluble copolymers containing as copolymerized units monomers having two or more ethylenically unsaturated double bonds 失效
    含有含有共聚单元的含有两个或更多个烯属不饱和双键的单体的水溶性共聚物的洗涤剂

    公开(公告)号：US4897220A

    公开(公告)日：1990-01-30

    申请号：US191979

    申请日：1988-05-10

    申请人： Wolfgang Trieselt ,  Richard Baur ,  Ekhard Winkler ,  Paul Diessel ,  Hans-Peter Seelmann-Eggebert ,  Dieter Boeckh ,  Heinrich Hartmann

    发明人： Wolfgang Trieselt ,  Richard Baur ,  Ekhard Winkler ,  Paul Diessel ,  Hans-Peter Seelmann-Eggebert ,  Dieter Boeckh ,  Heinrich Hartmann

    IPC分类号： C08L33/02 ,  C08F20/10 ,  C08F220/04 ,  C08F220/06 ,  C08F222/16 ,  C11D3/37

    CPC分类号： C11D3/3761

    摘要： A surfactant-based detergent contains water-soluble copolymers which contain(a) from 99.5 to 15 mol % of one or more monoethylenically unsaturated C.sub.3 - to C.sub.6 -monocarboxylic acids,(b) from 0.5 to 20 mol % of one or more comonomers which contain two or more ethylenically unsaturated nonconjugated double bonds and have one or more --CO--OX groups where X is hydrogen, an alkali metal, one equivalent of an alkaline earth metal or ammonium,(c) from 0 to 84.5 mol % of one or more monoethylenically unsaturated C.sub.4 - to C.sub.6 -dicarboxylic acids,(d) from 0 to 20 mol % of one or more hydroxyalkyl esters of monoethylenically unsaturated C.sub.3 - to C.sub.6 -carboxylic acids and(e) from 0 to 30 mol % of other water-soluble monoethylenically unsaturated monomers copolymerizable with (a) to (d)as copolymerized units, with the proviso that the sum of the mol % ages (a) to (e) is always 100 and which have a Finkentscher K value of from 8 to 120.

    摘要翻译： 基于表面活性剂的洗涤剂含有水溶性共聚物，其含有（a）99.5〜15摩尔％的一种或多种单烯属不饱和C3〜C6-一元羧酸，（b）0.5〜20摩尔％的一种或多种共聚单体， 含有两个或多个烯键式不饱和非共轭双键，并且具有一个或多个-CO-OX基团，其中X为氢，碱金属，1当量碱土金属或铵，（c）0至84.5摩尔％ 更多的单烯属不饱和C 4 -C 6 - 二羧酸，（d）0至20摩尔％的一种或多种单烯属不饱和C 3 -C 6羧酸的羟烷基酯和（e）0至30摩尔％ 可与（a）至（d）共聚的可溶性单烯属不饱和单体作为共聚单元，条件是mol％年龄（a）至（e）的总和始终为100，Finkentscher K值为8至120 。