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    METHOD FOR PRODUCING ETHANOLAMINES AND/OR ETHYLENEAMINES
    62.
    发明申请
    METHOD FOR PRODUCING ETHANOLAMINES AND/OR ETHYLENEAMINES 审中-公开

    公开(公告)号：US20200079725A1

    公开(公告)日：2020-03-12

    申请号：US16469782

    申请日：2017-12-07

    Applicant: BASF SE

    Inventor： Marie Katrin SCHROETER ,  Alvaro GORDILLO ,  Andrei-Nicolae PARVULSCU ,  Johann-Peter MELDER ,  Carlos LIZANDARA PUEYO ,  Juergen BECHTEL ,  Thomas HEIDEMANN ,  Stephan A. SCHUNK ,  Ulrich MUELLER

    IPC: C07C209/16 ,  C07C213/02 ,  B01J23/80 ,  B01J37/03

    Abstract: The present invention relates to a process for preparing ethanolamines and/or ethyleneamines in the gas phase by reacting ethylene glycol with ammonia in the presence of an amination catalyst. It is a characteristic feature of the process that the amination catalyst is prepared by reducing a calcined catalyst precursor comprising an active composition, where the active composition comprises one or more active metals selected from the group consisting of the elements of groups 8, 9, 10 and 11 of the Periodic Table of the Elements and optionally one or more added catalyst elements selected group consisting of the metals and semimetals of groups 3 to 7 and 12 to 17, the element P and the rare earth elements. It is a further characteristic feature of the process that a catalyst precursor having low basicity is used, the low basicity being achieved in that a) the catalyst precursor is prepared by coprecipitation and the active composition additionally comprises one or more basic elements selected from the group consisting of the alkali metals and alkaline earth metals; or b) the catalyst precursor, as well as the active composition, additionally comprises a support material and is prepared by impregnating the support material or precipitative application onto the support material and the support material comprises one or more basic elements selected from the group consisting of the alkali metals, Be, Ca, Ba and Sr or one or more minerals selected from the group consisting of hydrotalcite, chrysotile and sepiolite; or c) the catalyst precursor, as well as the active composition, additionally comprises a support material and is prepared by impregnating the support material or precipitative application onto the support material and the active composition of the catalyst support comprises one or more basic elements selected from the group consisting of the alkali metals and the alkaline earth metals; or d) the catalyst precursor is calcined at temperatures of 600° C. or more; or e) the catalyst precursor is prepared by a combination of variants a) and d) or by a combination of variants b) and d) or by a combination of variants c) and d).

    A PROCESS FOR PREPARING ETHENE OXIDE
    64.
    发明申请
    A PROCESS FOR PREPARING ETHENE OXIDE 审中-公开

    公开(公告)号：US20190330171A1

    公开(公告)日：2019-10-31

    申请号：US16310645

    申请日：2017-07-12

    Applicant: BASF SE

    Inventor： Andrei-Nicolae PARVULESCU ,  Ulrich MUELLER ,  Joaquim Henrique TELES ,  Dominic RIEDEL ,  Markus WEBER ,  Yan LI

    IPC: C07D301/12 ,  B01J29/70

    Abstract: A process for preparing ethene oxide comprising providing a liquid feed stream comprising ethene, hydrogen peroxide, and a solvent; passing the liquid feed stream into an epoxidation zone comprising a catalyst comprising a titanium zeolite comprising zinc and having framework type MWW, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising ethene oxide, water, and the solvent; removing an effluent stream from the epoxidation zone, the effluent stream comprising ethene oxide, water and the solvent.

    PROCESS FOR A CONTINUOUS SYNTHESIS OF ZEOLITIC MATERIALS
    67.
    发明申请
    PROCESS FOR A CONTINUOUS SYNTHESIS OF ZEOLITIC MATERIALS 审中-公开

    公开(公告)号：US20190144290A1

    公开(公告)日：2019-05-16

    申请号：US16308928

    申请日：2017-06-14

    Applicant: BASF SE

    Inventor： Stefan MARX ,  Stefanie CLADE ,  Lena ARNOLD ,  Uwe DIEHLMANN ,  Ulrich MUELLER

    IPC: C01B39/48 ,  B01J19/18 ,  B01J19/00 ,  B01J29/70

    Abstract: The present invention relates to a continuous process for preparing a zeolitic material comprising (i) preparing a mixture comprising a source of YO2, optionally a source of X2O3, and a liquid solvent system; (ii) continuously feeding the mixture prepared in (i) into a continuous flow reactor at a liquid hourly space velocity in the range of from 0.3 to 20 h−1 for a duration of at least 1 h; and (iii) crystallizing the zeolitic material from the mixture in the continuous flow reactor, wherein the mixture is heated to a temperature in the range of from 100 to 300° C.; wherein the volume of the continuous flow reactor is in the range of from 150 cm3 to 75 m3, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.

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