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    Ink jet ink and recording material
    61.
    发明申请
    Ink jet ink and recording material 审中-公开
    喷墨油墨和记录材料

    公开(公告)号：US20060040074A1

    公开(公告)日：2006-02-23

    申请号：US11114279

    申请日：2005-04-26

    申请人： Mervin Wood ,  Joseph Suhadolnik ,  Paul Kondracki

    发明人： Mervin Wood ,  Joseph Suhadolnik ,  Paul Kondracki

    IPC分类号： C09D11/02 ,  B41M5/00

    CPC分类号： B41M5/52 ,  B41M5/5227 ,  B41M5/5236 ,  B41M5/5245 ,  C09D11/38

    摘要： The present invention relates to an ink jet ink, an ink jet recording material or an ink jet system comprising at least one sterically hindered N-hydroxylamine strong acid salt, for example 1-hydroxy-2,2,6,6-tetramethyl-4-hydroxypiperidinium chloride or bis(1-hydroxy-2,2,6,6-tetramethylpiperidin-4-yl) sebacate dihydrochloride; or comprising at least one dialkyl N-hydroxylamine salt, for example chloride, bisulfate, sulfate, phosphate, nitrate, ascorbate, formate, acetate, benzoate, oxalate, citrate, a carboxylate of ethylenediaminetetraacetic acid or of diethylenetriaminepentaacetic acid or polyacrylate salts of N,N-diethylhydroxylamine, N,N-bis(2-hydroxypropyl)hydroxylamine, N,N-bis(3-hydroxypropyl)hydroxylamine, N,N-dibenzylhydroxylamine or the N,N-di(alkyl)hydroxylamine produced by the direct oxidation of N,N-di(hydrogenated tallow)amine.

    摘要翻译： 本发明涉及一种喷墨油墨，喷墨记录材料或喷墨系统，其包含至少一个空间位阻N-羟胺强酸盐，例如1-羟基-2,2,6,6-四甲基-4 - 羟基哌啶鎓氯化物或双（1-羟基-2,2,6,6-四甲基哌啶-4-基）癸二酸二盐酸盐; 或包含至少一种二烷基N-羟胺盐，例如氯化物，硫酸氢盐，硫酸盐，磷酸盐，硝酸盐，抗坏血酸盐，甲酸盐，乙酸盐，苯甲酸盐，草酸盐，柠檬酸盐，乙二胺四乙酸或二亚乙基三胺五乙酸的羧酸盐或N， N-二乙基羟胺，N，N-双（2-羟丙基）羟胺，N，N-双（3-羟丙基）羟胺，N，N-二苄基羟胺或通过直接氧化生成的N，N-二（烷基）羟胺 N，N-二（氢化牛脂）胺。

    Processes for the preparation of benzotriazole UV absorbers
    63.
    发明授权
    Processes for the preparation of benzotriazole UV absorbers 失效
    制备苯并三唑紫外线吸收剂的方法

    公开(公告)号：US06815550B2

    公开(公告)日：2004-11-09

    申请号：US10315693

    申请日：2002-12-10

    申请人： Mervin G. Wood ,  Deborah DeHessa ,  Joseph Suhadolnik ,  Andrew B. Naughton ,  Jerome Sanders ,  Jacqueline Lau ,  Rong Xiong ,  Joseph Babiarz

    发明人： Mervin G. Wood ,  Deborah DeHessa ,  Joseph Suhadolnik ,  Andrew B. Naughton ,  Jerome Sanders ,  Jacqueline Lau ,  Rong Xiong ,  Joseph Babiarz

    IPC分类号： C07D24920

    CPC分类号： C07D249/20 ,  C07C245/08

    摘要： Provided is a process for preparing 2H-benzotriazole UV absorbers containing a perfluoroalkyl moiety at the 5-position of the benzoic ring, for example a trifluoromethyl group, which involves digitizing the perfluoroalkyl substituted o-nitroaniline using concentrated sulfuric acid plus sodium nitrite or nitrosylsulfuric acid to form the corresponding monoazobenzene intermediate via the diazonium salt intermediate which is reduced to the corresponding 5-perfluoroalkyl substituted 2H-benzotriazole UV absorber compound by conventional reduction means. Also provided is a novel one-pot, multiphase reaction for the preparation of 2(2-nitrophenylazo) substituted phenols, which are precursors for 2H-benzotriazole UV absorbers.

    摘要翻译： 提供了制备在苯甲酸环的5位上含有全氟烷基部分的2H-苯并三唑UV吸收剂的方法，例如三氟甲基，其涉及使用浓硫酸加亚硝酸钠或亚硝酰基硫酸将全氟烷基取代的邻硝基苯胺数字化 通过重氮盐中间体形成相应的单偶氮苯中间体，其通过常规还原方法还原成相应的5-全氟烷基取代的2H-苯并三唑UV吸收剂化合物。 还提供了用于制备2（2-硝基苯基偶氮）取代的酚的新颖的一锅多相反应，其是2H-苯并三唑UV吸收剂的前体。