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    Process for the preparation of a polyurethane polymer with secondary hydroxyl end groups comprising polyester polyols
    61.
    发明授权
    Process for the preparation of a polyurethane polymer with secondary hydroxyl end groups comprising polyester polyols 有权
    用于制备具有包含聚酯多元醇的仲羟基端基的聚氨酯聚合物的方法

    公开(公告)号：US09139685B2

    公开(公告)日：2015-09-22

    申请号：US13381139

    申请日：2010-06-29

    申请人： Hartmut Nefzger ,  Jörg Hofmann ,  Bert Klesczewski ,  Erika Bauer ,  Klaus Lorenz

    发明人： Hartmut Nefzger ,  Jörg Hofmann ,  Bert Klesczewski ,  Erika Bauer ,  Klaus Lorenz

    IPC分类号： C08G18/00 ,  C08G18/42 ,  C08G18/76 ,  C08G63/91 ,  C08G77/46 ,  C08G101/00

    CPC分类号： C08G18/4291 ,  C08G18/4241 ,  C08G18/4261 ,  C08G18/4263 ,  C08G18/7621 ,  C08G63/916 ,  C08G77/46 ,  C08G2101/0008 ,  C08G2101/005 ,  C08G2101/0083

    摘要： The invention relates to a process for the preparation of a polyurethane polymer, comprising the step of reaction ofA) polyester polyols with secondary hydroxyl end groups, which are obtainable from the reaction of a polyester comprising carboxyl end groups with an epoxide of the general formula (1): wherein R1 represents an alkyl radical or an aryl radical and wherein the polyester comprising carboxyl end groups has an acid number of from ≧25 mg of KOH/g to ≦400 mg of KOH/g and a hydroxyl number of ≦5 mg of KOH/g, with B) polyisocyanates which are chosen from the group comprising toluoylene-diisocyanate, diphenylmethane-diisocyanate, polymeric diphenylmethane-diisocyanate, xylylene-diisocyanate, naphthylene-diisocyanate, hexamethylene-diisocyanate, diisocyanatodicyclohexylmethane and/or isophorone-diisocyanate. The invention furthermore relates to polyurethane polymers prepared by such a process.

    摘要翻译： 本发明涉及一种制备聚氨酯聚合物的方法，包括A）聚酯多元醇与仲羟基端基反应的步骤，其可从包含羧基端基的聚酯与通式 （1）表示：其中R1表示烷基或芳基，其中包含羧基端基的聚酯的酸值为≥25mgKOH / g至＆lt; NlE; 400mg KOH / g，羟值为＆ ; B）多异氰酸酯，其选自甲苯二异氰酸酯，二苯基甲烷二异氰酸酯，聚合二苯基甲烷二异氰酸酯，亚二甲苯基二异氰酸酯，亚萘基二异氰酸酯，六亚甲基二异氰酸酯，二异氰酸二环己基甲烷和/或异佛尔酮 - 二异氰酸酯。 本发明还涉及通过这种方法制备的聚氨酯聚合物。

    Semi-continuous method for producing copolymers
    68.
    发明授权
    Semi-continuous method for producing copolymers 有权
    半连续共聚物的制备方法

    公开(公告)号：US08536285B2

    公开(公告)日：2013-09-17

    申请号：US13133026

    申请日：2009-11-25

    申请人： Reinhard Dorfner ,  Klaus Lorenz ,  Petra Wagner ,  Christian Scholz

    发明人： Reinhard Dorfner ,  Klaus Lorenz ,  Petra Wagner ,  Christian Scholz

    IPC分类号： C08F216/14 ,  C08F2/10 ,  C08F224/00 ,  C04B16/04

    CPC分类号： C08F290/00 ,  C08F265/00 ,  C08F267/00 ,  C08F283/06 ,  C08F290/062 ,  C08F290/142 ,  C08L51/003 ,  C08L2666/02

    摘要： A process for the preparation of a copolymer in semicontinuous operation in a polymerization apparatus including a polymerization reactor connected to a metering device, acid monomer being initially taken in the metering device and polyether macromonomer and water in the polymerization reactor, acid monomer being metered from the metering device via an acid monomer metering line into the polymerization reactor, a portion of the copolymer-containing aqueous medium being passed continuously during the free radical polymerization from the polymerization reactor via a reaction mixture line which is connected via a mixing device to the acid monomer metering line, the discharged copolymer-containing aqueous medium being mixed with the acid monomer in the mixing device during the metering of the acid monomer and being recycled to the polymerization reactor after the mixing via the acid monomer metering line.

    摘要翻译： 一种在包括连接到计量装置的聚合反应器的聚合装置中的半连续操作中制备共聚物的方法，初始计量装置中的酸单体和聚合反应器中的聚醚大分子单体和水，酸单体从 计量装置通过酸性单体计量管线进入聚合反应器，一部分含共聚物的水性介质在自由基聚合期间通过经由混合装置连接到酸单体的反应混合物线从聚合反应器中连续通过 计量管线，在计量酸性单体期间将含有共聚物的含水介质与酸性单体混合在混合装置中，并通过酸性单体计量管道在混合后再循环到聚合反应器中。

    METHOD FOR PRODUCING POLYOLS CONTAINING AMINO GROUPS
    70.
    发明申请
    METHOD FOR PRODUCING POLYOLS CONTAINING AMINO GROUPS 审中-公开
    生产含有氨基团的多元醇的方法

    公开(公告)号：US20120184705A1

    公开(公告)日：2012-07-19

    申请号：US13498772

    申请日：2010-09-27

    申请人： Klaus Lorenz ,  Manfred Schmidt

    发明人： Klaus Lorenz ,  Manfred Schmidt

    IPC分类号： C08G18/32 ,  C07C217/08 ,  C07C213/04

    CPC分类号： C08G65/30 ,  C08G18/10 ,  C08G18/3819 ,  C08G18/5021 ,  C08G18/7664 ,  C08G65/2621

    摘要： The present invention provides a simple method with no processing for producing polyols based on amino group-containing starter compounds. Unless explicitly specified, polyols are understood to be polyether polyols, polyether ester polyols and also polyether ester amide polyols. The invention also provides the polyols obtainable by the method according to the invention and the use of the polyols according to the invention to produce polyurethane materials.

    摘要翻译： 本发明提供了一种基于含氨基起始化合物制备多元醇的方法。 除非另有明确规定，多元醇被理解为聚醚多元醇，聚醚酯多元醇以及聚醚酯酰胺多元醇。 本发明还提供可通过本发明的方法获得的多元醇以及根据本发明的多元醇的用途来生产聚氨酯材料。