Method of aerogel synthesis
    61.
    发明授权
    Method of aerogel synthesis 有权
    气凝胶合成方法

    公开(公告)号:US09562141B2

    公开(公告)日:2017-02-07

    申请号:US14950522

    申请日:2015-11-24

    Abstract: The present disclosure provides a method for producing an aerogel, the method comprising reacting at least one acid monomer with at least one diamino monomer in a first solvent under conditions appropriate to form a polyimide polymer; conducting a solvent exchange wherein the first solvent is exchanged for a second solvent, said second solvent having a freezing point, wherein said solvent exchange further comprises (1) submersing the polyimide polymer in the second solvent in a pressure vessel and (2) creating a high pressure environment inside the pressure vessel for a first period of time; cooling the polyimide polymer to a first temperature below the freezing point of the second solvent; and subjecting cooled polyimide polymer to a first vacuum for a second period of time at a second temperature.

    Abstract translation: 本公开提供了一种制备气凝胶的方法,该方法包括使至少一种酸单体与至少一种二氨基单体在第一溶剂中在适于形成聚酰亚胺聚合物的条件下反应; 进行溶剂交换,其中第一溶剂被更换为第二溶剂,所述第二溶剂具有凝固点,其中所述溶剂交换还包括(1)将聚酰亚胺聚合物浸入第二溶剂中的压力容器中,和(2) 压力容器内的高压环境第一个时间段; 将聚酰亚胺聚合物冷却至低于第二溶剂凝固点的第一温度; 并在第二温度下将冷却的聚酰亚胺聚合物经受第一个真空第二个时间段。

    METHOD FOR PRODUCING POROUS CELLULOSE BEADS
    62.
    发明申请
    METHOD FOR PRODUCING POROUS CELLULOSE BEADS 审中-公开
    生产多孔纤维素珠的方法

    公开(公告)号:US20160236171A1

    公开(公告)日:2016-08-18

    申请号:US15028632

    申请日:2014-10-14

    Abstract: The present invention provides a method for easily and efficiently producing cellulose beads which has narrow pore size distribution and pore structure suitable for an adsorbent and of which adsorption performance is excellent without using highly toxic and highly corrosive auxiliary raw material and without industrially disadvantageous cumbersome step. The method for producing porous cellulose beads according to the present invention is characterized in comprising (a) the step of preparing a fine cellulose dispersion by mixing a low temperature alkaline aqueous solution and cellulose, (b) the step of preparing a mixed liquid by adding a water-soluble low molecular organic compound to the fine cellulose dispersion, (c) the step of preparing an emulsion by dispersing the mixed liquid in a dispersion medium, (d) the step of contacting the emulsion with a coagulating solvent.

    Abstract translation: 本发明提供一种容易且有效地制造纤维素珠粒的方法,该纤维素珠粒具有窄的孔径分布和适用于吸附剂的孔结构,并且其吸附性能优异,而不使用高毒性和高腐蚀性的辅助原料,并且在工业上不利的繁琐步骤。 根据本发明的多孔纤维素珠粒的制造方法的特征在于,(a)通过混合低温碱性水溶液和纤维素来制备细纤维素分散液的步骤,(b)通过添加制备混合液体的步骤 (c)通过将混合液体分散在分散介质中制备乳液的步骤,(d)使乳液与凝固溶剂接触的步骤。

    Method of aerogel synthesis
    63.
    发明授权
    Method of aerogel synthesis 有权
    气凝胶合成方法

    公开(公告)号:US09206298B2

    公开(公告)日:2015-12-08

    申请号:US13901453

    申请日:2013-05-23

    Abstract: The present disclosure provides a method for producing an aerogel, the method comprising reacting at least one acid monomer with at least one diamino monomer in a first solvent under conditions appropriate to form a polyimide polymer; conducting a solvent exchange wherein the first solvent is exchanged for a second solvent, said second solvent having a freezing point, wherein said solvent exchange further comprises (1) submersing the polyimide polymer in the second solvent in a pressure vessel and (2) creating a high pressure environment inside the pressure vessel for a first period of time; cooling the polyimide polymer to a first temperature below the freezing point of the second solvent; and subjecting cooled polyimide polymer to a first vacuum for a second period of time at a second temperature.

    Abstract translation: 本公开提供了一种制备气凝胶的方法,该方法包括使至少一种酸单体与至少一种二氨基单体在第一溶剂中在适于形成聚酰亚胺聚合物的条件下反应; 进行溶剂交换,其中第一溶剂被更换为第二溶剂,所述第二溶剂具有凝固点,其中所述溶剂交换还包括(1)将聚酰亚胺聚合物浸入第二溶剂中的压力容器中,和(2) 压力容器内的高压环境第一个时间段; 将聚酰亚胺聚合物冷却至低于第二溶剂凝固点的第一温度; 并在第二温度下将冷却的聚酰亚胺聚合物经受第一个真空第二个时间段。

    Method of Aerogel Synthesis
    64.
    发明申请
    Method of Aerogel Synthesis 有权
    气凝胶合成方法

    公开(公告)号:US20140350134A1

    公开(公告)日:2014-11-27

    申请号:US13901453

    申请日:2013-05-23

    Abstract: The present disclosure provides a method for producing an aerogel, the method comprising reacting at least one acid monomer with at least one diamino monomer in a first solvent under conditions appropriate to form a polyimide polymer; conducting a solvent exchange wherein the first solvent is exchanged for a second solvent, said second solvent having a freezing point, wherein said solvent exchange further comprises (1) submersing the polyimide polymer in the second solvent in a pressure vessel and (2) creating a high pressure environment inside the pressure vessel for a first period of time; cooling the polyimide polymer to a first temperature below the freezing point of the second solvent; and subjecting cooled polyimide polymer to a first vacuum for a second period of time at a second temperature.

    Abstract translation: 本公开提供了一种制备气凝胶的方法,该方法包括使至少一种酸单体与至少一种二氨基单体在第一溶剂中在适于形成聚酰亚胺聚合物的条件下反应; 进行溶剂交换,其中第一溶剂被更换为第二溶剂,所述第二溶剂具有凝固点,其中所述溶剂交换还包括(1)将聚酰亚胺聚合物浸入第二溶剂中的压力容器中,和(2) 压力容器内的高压环境第一个时间段; 将聚酰亚胺聚合物冷却至低于第二溶剂凝固点的第一温度; 并在第二温度下将冷却的聚酰亚胺聚合物经受第一个真空第二个时间段。

    Monolithic organic copolymer
    65.
    发明授权
    Monolithic organic copolymer 有权
    单片有机共聚物

    公开(公告)号:US08586641B2

    公开(公告)日:2013-11-19

    申请号:US11551181

    申请日:2006-10-19

    Abstract: The present invention relates to a monolithic organic copolymer prepared by copolymerization of at least one monomer of the group consisting of styrene, (C1-C3)alkylstyrene, (meth)acrylic acid and esters thereof with a crosslinker in the presence of a macroporogen and a microporogen, wherein a) the sum of said at least one monomer of the group and the crosslinker is 10-20%, preferably 10-15%, by volume of the reaction mixture, with the rest being essentially macroporogen and microporogen, and the degree of said copolymerization is at least 70%, preferably at least 90%, more preferably at least 99%, or b) the sum of said at least one monomer of the group and the crosslinker is 30-50%, preferably 35-45%, by volume of the reaction mixture, with the rest being essentially macroporogen and microporogen, and the degree of said copolymerization is in the range of 25-60%, preferably 35-50%. These copolymers can be used in high-performance liquid chromatography for the separation of biopolymers as well as small molecules.

    Abstract translation: 本发明涉及一种整体式有机共聚物,其通过在大孔原子存在下将苯乙烯,(C1-C3)烷基苯乙烯,(甲基)丙烯酸及其酯与至少一种单体与交联剂共聚而成, 微生物,其中a)所述基团和交联剂的所述至少一种单体的总和为反应混合物的体积的10-20%,优选10-15%,其余基本上为大孔隙和微孔,以及程度 的所述共聚物为至少70%,优选至少90%,更优选至少99%,或b)所述基团和交联剂的所述至少一种单体之和为30-50%,优选35-45% ,反应混合物的体积,其余基本上是大孔原子和微孔,并且所述共聚的程度在25-60%,优选35-50%的范围内。 这些共聚物可用于高效液相色谱分离生物聚合物以及小分子。

    METHOD FOR REMOVING DILUENT FROM AN EXTRUDATE OF A POLYMER SOLUTION
    67.
    发明申请
    METHOD FOR REMOVING DILUENT FROM AN EXTRUDATE OF A POLYMER SOLUTION 有权
    从聚合物溶液中除去稀释液的方法

    公开(公告)号:US20100273032A1

    公开(公告)日:2010-10-28

    申请号:US12747831

    申请日:2008-12-12

    Abstract: The invention relates to a method for removing diluent from a polymer extrudate, especially in connection with a process for producing a microporous membrane. The method involves contacting the extrudate with a second solvent in a first stage; contacting the extrudate from the first stage with a third solvent in a second stage; conducting a first stream away from the first stage and/or conducting a second stream away from the second stage; and cooling at least a portion of the first and/or second stream and separating therefrom at least one of a first phase rich in the second solvent or a second phase rich in the third solvent.

    Abstract translation: 本发明涉及一种用于从聚合物挤出物中除去稀释剂的方法,特别是涉及用于生产微孔膜的方法。 该方法包括在第一阶段使挤出物与第二溶剂接触; 在第二阶段将来自第一阶段的挤出物与第三溶剂接触; 将远离所述第一级的第一流和/或从所述第二级进行第二流的第一流; 以及冷却所述第一和/或第二物流的至少一部分并从其中分离富含第二溶剂的第一相或富含第三溶剂的第二相中的至少一种。

    Porous gelatin material, gelatin structures, methods for preparation of the same and uses thereof
    68.
    发明授权
    Porous gelatin material, gelatin structures, methods for preparation of the same and uses thereof 有权
    多孔明胶材料,明胶结构,其制备方法及其用途

    公开(公告)号:US07404971B2

    公开(公告)日:2008-07-29

    申请号:US10516614

    申请日:2003-05-23

    Applicant: Kjell Nilsson

    Inventor: Kjell Nilsson

    Abstract: The present invention relates to a porous gelatin material in the form of spherical particles with a continuous pore structure and cast, three-dimensional, porous gelatin structures. The invention also comprises methods for preparation of the porous gelatin materials and structures. The method for preparing the porous gelatin material in the form of spheres with a continuous pore structure comprises the steps of preparing a homogenous water-based gelatin solution, adding an emulsifier with an HLD value >9, adding a first composition comprising an organic solvent and an emulsifier with an HLB value >9, adding a second composition comprising an organic solvent and an emulsifier with an HLB value

    Abstract translation: 本发明涉及具有连续孔结构的球形颗粒形式的多孔明胶材料和铸造的三维多孔明胶结构。 本发明还包括制备多孔明胶材料和结构的方法。 制备具有连续孔结构的球形多孔明胶材料的方法包括以下步骤:制备均匀的水基明胶溶液,加入HLD值> 9的乳化剂,加入包含有机溶剂的第一组合物和 HLB值> 9的乳化剂,加入包含HLB值<8的有机溶剂和乳化剂的第二组合物,并使明胶材料固化。 还包括根据本发明的材料的用途。

    Microporous material exhibiting low alkali metal content
    70.
    发明授权
    Microporous material exhibiting low alkali metal content 失效
    显示低碱金属含量的微孔材料

    公开(公告)号:US5583171A

    公开(公告)日:1996-12-10

    申请号:US221203

    申请日:1994-03-31

    Abstract: Microporous material comprising water insoluble thermoplastic organic polymer and particulate amorphous precipitated silica not only exhibits low particulate emissions during handling and use, but also has a low extactable alkali metal content. Microporous material having these characteristics is especially useful in clean rooms where electronic devices such as integrated circuits are manufactured. Such microporous material may be produced by employing amorphous precipitated silica particles having low alkali metal content as all or a substantial proportion of the amorphous precipitated silica particles constituting the microporous material.

    Abstract translation: 包含水不溶性热塑性有机聚合物和颗粒状无定形沉淀二氧化硅的微孔材料在处理和使用过程中不仅表现出低的颗粒排放,而且具有低的可交换的碱金属含量。 具有这些特性的微孔材料在制造诸如集成电路的电子设备的洁净室中特别有用。 这样的微孔材料可以通过使用具有低碱金属含量的无定形沉淀二氧化硅颗粒作为构成微孔材料的全部或相当大比例的无定形沉淀二氧化硅颗粒来制备。

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