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89 条记录 (耗时 0.012 秒)

    Apparatus for carrying out chlorinating reactions
    61.
    发明授权
    Apparatus for carrying out chlorinating reactions 失效
    用于进行氯化反应的装置

    公开(公告)号：US4049385A

    公开(公告)日：1977-09-20

    申请号：US644888

    申请日：1975-12-29

    申请人： Josef Bohnenstingl ,  Manfred Laser ,  Gunter Lossmann ,  Helmut Gebhard

    发明人： Josef Bohnenstingl ,  Manfred Laser ,  Gunter Lossmann ,  Helmut Gebhard

    IPC分类号： B01J15/00 ,  B01J19/24 ,  C22B1/08 ,  C22B34/10 ,  C22B60/02 ,  B01J8/08 ,  H05B3/62

    CPC分类号： B01J19/2415 ,  B01J15/00 ,  B01J19/2405 ,  C22B1/08 ,  C22B34/10 ,  C22B60/0213 ,  B01J2219/00135 ,  B01J2219/00155 ,  B01J2219/00159

    摘要： An apparatus for carrying out chlorinating reactions when extracting metalsuch as titanium, zirconium or the like during the extraction of uranium and thorium during the reprocessing of burned-off fuel and/or breeder elements for core reactors and during the purification of coal and graphite. The device comprises a shaft or blast furnace which is heated by a direct flow of current and while being coaxially surrounded by a mantle or shell communicates through a connection or adapter piece with a subsequent condenser of graphite. The device according to the present invention is characterized primarily in that the shell of the furnace and the adapter piece connecting the furnace with the condenser are made of graphite. The shell of the furnace, the condenser and the adapter piece connecting the shell with the condenser are arranged within a steel casing designed in a gas-tight manner.

    摘要翻译： 在用于核反应堆的废燃料和/或增殖元件的后处理期间以及在煤和石墨的净化过程中，在提取铀和钍之前提取金属如钛，锆等时，进行氯化反应的装置。 该装置包括轴或高炉，其通过直流电流加热并同时被套管或壳体包围，通过连接或适配件与后续的石墨冷凝器连通。 根据本发明的装置的特征主要在于炉的外壳和将炉与冷凝器连接的适配件由石墨制成。 炉壳，冷凝器和将壳体与冷凝器连接的适配器片体布置在以气密方式设计的钢壳体内。

    Process for class IV-B metals ore reduction
    62.
    发明授权
    Process for class IV-B metals ore reduction 失效
    IV-B类金属矿石还原工艺

    公开(公告)号：US3948637A

    公开(公告)日：1976-04-06

    申请号：US478345

    申请日：1974-06-10

    申请人： Paul Franklin Taylor

    发明人： Paul Franklin Taylor

    IPC分类号： C22B34/10 ,  C22B1/00

    CPC分类号： C22B34/10

    摘要： Ores containing oxides of Titanium, Zirconium and Hafnium metals are reduced by mixing them in the powdered state with a base hydroxide of one of the Classes I-A or II-A metals of the periodic table of elements and either sugar or starch, mixing them well, then heating the mixture until ignition begins and maintaining the necessary heat until ignition is finished. The remaining residue is then flushed and boiled with water to remove waste chemicals, leached with hydrocarbon solvents, hydrochloric acid, again boiled with water, flushed, dryed, and then smelted to Class IV-B metal powder or ingot.

    摘要翻译： 含有钛，锆和铪金属的氧化物的矿石通过将粉末状态与元素周期表中的IA类或II-A族之一的碱性氢氧化物和糖或淀粉混合，将它们混合而减少， 然后加热混合物，直到点火开始，并保持必要的热量直到点火完成。 然后将剩余的残余物冲洗并用水煮沸以除去废化学品，用烃溶剂，盐酸浸出，再次用水煮沸，冲洗，干燥，然后熔炼成IV-B族金属粉末或锭。

    Process for class iv-b metals ore reduction
    63.
    发明授权
    Process for class iv-b metals ore reduction 失效
    IV-B类金属减少的过程

    公开(公告)号：US3912498A

    公开(公告)日：1975-10-14

    申请号：US47180374

    申请日：1974-05-20

    申请人： TICOA COMPANY INC

    发明人： TAYLOR PAUL FRANKLIN

    IPC分类号： C22B34/12 ,  C22B34/14 ,  C22B1/00 ,  C22B3/00 ,  C22B4/04 ,  C22B34/10

    CPC分类号： C22B34/14 ,  C22B34/124 ,  C22B34/1259 ,  C22B34/1295

    摘要： Ores containing oxides of Titanium, Zirconium and Hafnium metals are reduced by mixing them in the powdered state with a chemical solution formula consisting primarily of phosphoric acid, zinc oxide, and a sulfated surfactant. Calcium carbonate is added to the solution as a catalyst and the mixture is brought to a boil, allowing the volatile materials to vaporize out of the mixture so as to provide either pliable or hard formed residue material. Sodium bicarbonate and water are added to the pliable which reacts chemically with waste chemicals, then is decanted and flushed with water, cleansing agents, etc. and dried. Powder may then be subjected to the plasma arc furnace so as to provide commercially pure and semi-pure powder, sponge-like ingot, or metallized upon other metal surfaces. Or the powder may be leached and cleansed of the phosphide contaminants within it and then smelted. This is accomplished by boiling it within hydroxide bases, molten halogen salts, or burning it within a mixture of hydroxide bases and sugar. Resultant material then sets in repose with added water, boiled, flushed, reacted with hydrochloric acid, again boiled with water, cleansed and rinsed with water, then dried, screened and smelted. Smelting is accomplished by plasma arc furnaces, vacuum-inert furnaces containing molten metal of the Ia or IIa Periodic Table Class groups, or vacuuminert furnaces operating at the respective melting points of the metal. The hard formed residue is pulverized to small particle size, boiled within hydroxide bases, molten halogen salts, or burned within a mixture of hydroxide bases and sugar. Resultant material then stes in repose with added water, boiled, flushed, reacted with hydrochloric acid, again boiled with water, cleansed and rinsed with water, then dried, screened and smelted. Smelting is accomplished by plasma arc furnaces, vacuum-inert furnaces containing molten metal of the Ia or IIa Periodic Table Class groups, or vacuum-inert furnaces operating at the respective melting points of the metal.

    Method for producing refractory metals
    64.
    发明授权
    Method for producing refractory metals 失效
    生产耐火金属的方法

    公开(公告)号：US3736132A

    公开(公告)日：1973-05-29

    申请号：US3736132D

    申请日：1971-12-17

    申请人： STEEL CORP

    发明人： MORSE H H ,  EASTERDAY C L ,  EASTERDAY D E ,  PLOCK L S ,  MORGAN F K

    IPC分类号： C22B34/14 ,  B22F3/10 ,  C22B5/02 ,  C22B34/10 ,  C22B34/12 ,  B22F1/00 ,  C22B53/00 ,  C22B61/02

    CPC分类号： C22B34/10 ,  C22B34/1272

    摘要： A PROCESS FOR THE MANUFACTURE OF TITANIUM FROM TITANIUM TETRACHLORIDE BY REDUCTION WITH SODIUM, IN WHICH A PARTIALLY REDUCED MATERIAL PRINCIPALLY CORRESPONDING TO NA2TICL4 IS CONTINUOUSLY FORMED, IS IMPROVED BY CONTINUOUSLY MIXING THE PARTIALLY REDUCED MATERIAL WITH SODIUM AT A TEMPERATURE BELOW ABOUT 200*C. SO AS TO FORM AN INTERMEDIATE MATERIAL CORRESPONDING TO AT LEAST 15% BY WEIGHT NA3TICL4, COMPACTING THE INTERMEDIATE MATERIAL AT A TEMPERATURE OF LESS THAN 100*C. TO FORM A CONTINUOUS ROD OF THE COMPOSITE MATERIAL WITHOUT SUBSTANTIAL FURTHER REDUCTION OF THE TITANIUM CHLORIDE CONTENT THEREOF AND CONTINUOUSLY HEATING THE ROD FORMED AT TEMTERATURES ABOUT 800*C. TO COMPLETE REDUCTION OF TITANIUM CHLORIDE COMPONENT THEREOF, TO EFFECT SINTERING OF THE RESULTING TITANIUM METAL, AND TTO SIMULTANEOUSLY MELT THE SALT BY-PRODUCT AND THEREBY FACILITATE SEPARATION AND REMOVAL OF THE SALT FROM THE ROD-SHAPED, SINTERED TITANIUM METAL PRODUCT.