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    POLYCRYSTALLINE COMPACTS HAVING MATERIAL DISPOSED IN INTERSTITIAL SPACES THEREIN, CUTTING ELEMENTS AND EARTH-BORING TOOLS INCLUDING SUCH COMPACTS, AND METHODS OF FORMING SUCH COMPACTS
    71.
    发明申请
    POLYCRYSTALLINE COMPACTS HAVING MATERIAL DISPOSED IN INTERSTITIAL SPACES THEREIN, CUTTING ELEMENTS AND EARTH-BORING TOOLS INCLUDING SUCH COMPACTS, AND METHODS OF FORMING SUCH COMPACTS 有权
    具有在其间隔空间中切割材料的切割元件和包括这样的混合物的接地工具的多晶体化合物以及形成这样的混合物的方法

    公开(公告)号：US20110061942A1

    公开(公告)日：2011-03-17

    申请号：US12558184

    申请日：2009-09-11

    Applicant: Anthony A. DiGiovanni

    Inventor： Anthony A. DiGiovanni

    IPC: B24D3/04 ,  E21B10/46 ,  E21B10/55

    CPC classification number: B24D3/06 ,  B24D3/10 ,  B24D99/005 ,  C01C3/06 ,  C04B35/52 ,  C04B2235/427 ,  C04B2235/783 ,  E21B10/55 ,  E21B10/567

    Abstract: Polycrystalline compacts include smaller and larger hard grains that are interbonded to form a polycrystalline hard material. The larger grains may be at least about 150 times larger than the smaller grains. An interstitial material comprising one or more of a boride, a carbide, a nitride, a metal carbonate, a metal bicarbonate, and a non-catalytic metal may be disposed between the grains. The compacts may be used as cutting elements for earth-boring tools such as drill bits, and may be disposed on a substrate. Methods of making polycrystalline compacts include coating smaller hard particles with a coating material, mixing the smaller particles with larger hard particles, and sintering the mixture to form a polycrystalline hard material including interbonded smaller and larger grains. The sizes of the smaller and larger particles may be selected to cause the larger grains to be at least about 150 times larger than the smaller grains.

    Abstract translation: 多晶压块包括较小和较大的硬质颗粒，其相互键合以形成多晶硬质材料。 较大的颗粒可以比较小的颗粒大至少约150倍。 可以在晶粒之间设置包含硼化物，碳化物，氮化物，金属碳酸盐，金属碳酸氢盐和非催化金属中的一种或多种的间隙材料。 压块可以用作钻头等钻孔工具的切削元件，并且可以设置在基板上。 制造多晶压块的方法包括用涂料涂覆较小的硬颗粒，将较小的颗粒与较大的硬颗粒混合，并烧结该混合物以形成多晶硬质材料，包括粘结的较小和较大的颗粒。 可以选择较小和较大颗粒的尺寸以使较大的颗粒比较小的颗粒大至少约150倍。

    Superabrasive cutting elements with cutting edge geometry having enhanced durability and cutting efficiency and drill bits so equipped
    77.
    发明授权
    Superabrasive cutting elements with cutting edge geometry having enhanced durability and cutting efficiency and drill bits so equipped 有权
    具有切削刃几何形状的超级磨料切削元件具有增强的耐久性和切削效率以及如此装备的钻头

    公开(公告)号：US09371700B2

    公开(公告)日：2016-06-21

    申请号：US13116936

    申请日：2011-05-26

    Applicant: Anthony A. DiGiovanni

    Inventor： Anthony A. DiGiovanni

    IPC: E21B10/36 ,  E21B10/567

    CPC classification number: E21B10/5673 ,  E21B10/5676

    Abstract: A superabrasive cutting element including a diamond or other superabrasive material table having a peripheral cutting edge defined by at least one chamfer between a cutting face and a side surface of the table, an arcuate surface extending between the cutting face and an innermost chamfer of the at least one chamfer and a sharp, angular transition between an outermost chamfer of the at least one chamfer and the side surface. Methods of producing such superabrasive cutting elements and drill bits equipped with such superabrasive cutting elements are also disclosed.

    Abstract translation: 一种超级磨料切割元件，包括金刚石或其它超级磨料材料台，其具有由切割面和台面的侧表面之间的至少一个倒角限定的周边切割边缘，在切割面和在该切割面的最内侧倒角之间延伸的弧形表面 在所述至少一个倒角的最外倒角和所述侧表面之间的至少一个倒角和尖锐的角度过渡。 还公开了生产这种超研磨切割元件的方法和配备有这种超级磨料切割元件的钻头。

    Methods of forming polycrystalline compacts having material disposed in interstitial spaces therein, cutting elements and earth-boring tools including such compacts
    78.
    发明授权
    Methods of forming polycrystalline compacts having material disposed in interstitial spaces therein, cutting elements and earth-boring tools including such compacts 有权
    形成具有设置在其间隙空间中的材料的多晶压块的方法，切割元件和包括这种压块的钻孔工具

    公开(公告)号：US09085946B2

    公开(公告)日：2015-07-21

    申请号：US13619931

    申请日：2012-09-14

    Applicant: Anthony A. DiGiovanni

    Inventor： Anthony A. DiGiovanni

    IPC: B24D3/00 ,  B01J3/06 ,  E21B10/55 ,  B24D99/00 ,  E21B10/567 ,  B24D3/10

    CPC classification number: B24D3/06 ,  B24D3/10 ,  B24D99/005 ,  C01C3/06 ,  C04B35/52 ,  C04B2235/427 ,  C04B2235/783 ,  E21B10/55 ,  E21B10/567

    Abstract: Polycrystalline compacts include smaller and larger hard grains that are interbonded to form a polycrystalline hard material. The larger grains may be at least about 150 times larger than the smaller grains. An interstitial material comprising one or more of a boride, a carbide, a nitride, a metal carbonate, a metal bicarbonate, and a non-catalytic metal may be disposed between the grains. The compacts may be used as cutting elements for earth-boring tools such as drill bits, and may be disposed on a substrate. Methods of making polycrystalline compacts include coating smaller hard particles with a coating material, mixing the smaller particles with larger hard particles, and sintering the mixture to form a polycrystalline hard material including interbonded smaller and larger grains. The sizes of the smaller and larger particles may be selected to cause the larger grains to be at least about 150 times larger than the smaller grains.

    Abstract translation: 多晶压块包括较小和较大的硬质颗粒，其相互键合以形成多晶硬质材料。 较大的颗粒可以比较小的颗粒大至少约150倍。 可以在晶粒之间设置包含硼化物，碳化物，氮化物，金属碳酸盐，金属碳酸氢盐和非催化金属中的一种或多种的间隙材料。 压块可以用作钻头等钻孔工具的切削元件，并且可以设置在基板上。 制造多晶压块的方法包括用涂料涂覆较小的硬颗粒，将较小的颗粒与较大的硬颗粒混合，并烧结该混合物以形成多晶硬质材料，包括粘结的较小和较大的颗粒。 可以选择较小和较大颗粒的尺寸以使较大的颗粒比较小的颗粒大至少约150倍。

    Methods of forming polycrystalline compacts
    79.
    发明授权
    Methods of forming polycrystalline compacts 有权
    形成多晶压块的方法

    公开(公告)号：US09067304B2

    公开(公告)日：2015-06-30

    申请号：US13618927

    申请日：2012-09-14

    Applicant: Danny E. Scott ,  Anthony A. DiGiovanni

    Inventor： Danny E. Scott ,  Anthony A. DiGiovanni

    IPC: B24D3/00 ,  B24D3/14 ,  B24D18/00 ,  B24D99/00

    CPC classification number: B24D18/0009 ,  B01J3/06 ,  B01J2203/062 ,  B01J2203/0645 ,  B24D3/06 ,  B24D3/14 ,  B24D99/005 ,  E21B10/55

    Abstract: Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high-pressure, high-temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.

    Abstract translation: 公开了用于形成切割元件的方法，用于形成多晶压块的方法和相关的多晶压块。 对硬质材料的颗粒进行高压高温处理以形成多晶压块。 在另外的平稳温度或压力阶段期间，将系统压力或温度中的至少一个相对较快的尖峰包含在颗粒之间形成颗粒间结合。 高峰阶段的简洁可以避免不必要的晶粒生长。 方法的实施例还可以包括振荡至少一个系统状态（例如，压力，温度）和使晶粒经受超声或机械振动中的至少一个。 所得到的多晶压块可以包括具有最小量的催化剂材料的高密度颗粒间结合的硬质材料，并且可以在使用结合多晶压块的切割元件时提供改善的热稳定性，耐磨性，韧性和性能。

    Methods of forming diamond particles having organic compounds attached thereto and compositions thereof
    80.
    发明授权
    Methods of forming diamond particles having organic compounds attached thereto and compositions thereof 有权
    形成附着有有机化合物的金刚石颗粒及其组合物的方法

    公开(公告)号：US08936659B2

    公开(公告)日：2015-01-20

    申请号：US13275872

    申请日：2011-10-18

    Applicant: Soma Chakraborty ,  Gaurav Agrawal ,  Anthony A. DiGiovanni

    Inventor： Soma Chakraborty ,  Gaurav Agrawal ,  Anthony A. DiGiovanni

    IPC: C09K3/14 ,  B01J3/06 ,  B82Y30/00 ,  B24D99/00

    CPC classification number: C09K3/1436 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D99/005 ,  B82Y30/00 ,  C01B32/28 ,  Y10T428/2982

    Abstract: A substance includes diamond particles having a maximum linear dimension of less than about 1 μm and an organic compound attached to surfaces of the diamond particles. The organic compound may include a surfactant or a polymer. A method of forming a substance includes exposing diamond particles to an organic compound, and exposing the diamond particles in the presence of the organic compound to ultrasonic energy. The diamond particles may have a maximum linear dimension of less than about 1 μm. A composition includes a liquid, a plurality of diamond nanoparticles dispersed within the liquid, and an organic compound attached to surfaces of the diamond nanoparticles. A method includes mixing a plurality of diamond particles with a solution comprising a liquid solvent and an organic compound, and exposing the mixture including the plurality of diamond nanoparticles and the solution to ultrasonic energy.

    Abstract translation: 物质包括具有小于约1μm的最大线性尺寸的金刚石颗粒和附着到金刚石颗粒表面的有机化合物。 有机化合物可以包括表面活性剂或聚合物。 形成物质的方法包括将金刚石颗粒暴露于有机化合物，并将有机化合物存在下的金刚石颗粒暴露于超声波能量。 金刚石颗粒可以具有小于约1μm的最大线性尺寸。 组合物包括液体，分散在液体内的多个金刚石纳米颗粒和附着到金刚石纳米颗粒表面的有机化合物。 一种方法包括将多个金刚石颗粒与包含液体溶剂和有机化合物的溶液混合，并将包括多个金刚石纳米颗粒和溶液的混合物暴露于超声波能量。

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