公开(公告)号：US20190152847A1

公开(公告)日：2019-05-23

申请号：US16189242

申请日：2018-11-13

Applicant: Corning Incorporated

Inventor： Douglas Clippinger Allan ,  Konstantin Sergeevich Koreshkov ,  Christopher Lee Timmons

IPC: C03C21/00

Abstract: A method for ion exchanging glass articles is provided. The method includes ion exchanging a plurality of lots in steps within an ion exchange salt bath, wherein each of the plurality of lots comprises at least one glass article, and wherein the ion exchange salt bath comprises molten salt and, after removing the last lot from the ion exchange salt bath, removing substantially the entire volume of molten salt from the ion exchange salt bath. The method further includes maintaining steady state conditions in the ion exchange salt bath prior to removing substantially the entire volume of salt from the ion exchange salt bath such that at least one of the compressive stress and the central tension of substantially all of the glass articles varies from at least one of the compressive stress and the central tension of any other of the glass articles by less than about 20%.

公开(公告)号：US10034816B2

公开(公告)日：2018-07-31

申请号：US15374338

申请日：2016-12-09

Applicant: Corning Incorporated

Inventor： Andrei Gennadyevich Fadeev ,  Theresa Chang ,  Dana Craig Bookbinder ,  Santona Pal ,  Chandan Kumar Saha ,  Steven Edward DeMartino ,  Christopher Lee Timmons ,  John Stephen Peanasky

IPC: A61J1/14 ,  C03C17/00 ,  C03C17/42 ,  C03C17/30 ,  C03C17/32 ,  C03C21/00 ,  B65D25/34 ,  B65D65/42 ,  B65D23/08 ,  C09D179/08

CPC classification number: A61J1/1468 ,  A61J1/00 ,  B65D23/0814 ,  B65D23/0821 ,  B65D25/14 ,  B65D25/34 ,  B65D65/42 ,  C03C17/005 ,  C03C17/30 ,  C03C17/32 ,  C03C17/42 ,  C03C21/002 ,  C03C2217/78 ,  C03C2218/111 ,  C09D179/08 ,  Y10T428/1321 ,  Y10T428/24942

Abstract: A pharmaceutical package may include a glass body enclosing an inner volume and having an exterior surface. The glass body may be formed from a borosilicate glass that meets the Type 1 criteria according to USP or an alkali aluminosilicate glass having a Class HGA 1 hydrolytic resistance when tested according to the ISO 720-1985 testing standard. A coupling agent layer having a first thickness less than or equal to 100 nm may be disposed on the exterior surface of the glass body. A polymer layer having a second thickness of less than 50 nm may be positioned over the coupling agent layer. The exterior surface of the glass body with the coupling agent layer and the polymer layer may have a coefficient of friction less than or equal to 0.7.

公开(公告)号：US20170341812A1

公开(公告)日：2017-11-30

申请号：US15610048

申请日：2017-05-31

Applicant: CORNING INCORPORATED

Inventor： Steven Edward DeMartino ,  Daniel Warren Hawtof ,  Ming-Jun Li ,  Anping Liu ,  John Stephen Peanasky ,  Christopher Lee Timmons ,  Qi Wu

IPC: B65D23/00 ,  B23K26/53 ,  B23K26/0622 ,  C03C15/00 ,  B23K26/00 ,  B23K103/00

Abstract: A glass container including a body having a delamination factor less than or equal to 10 and at least one marking is described. The body has an inner surface, an outer surface, and a wall thickness extending between the outer surface and the inner surface. The marking is located within the wall thickness. In particular, the marking is a portion of the body having a refractive index that differs from a refractive index of an unmarked portion of the body. Methods of forming the marking within the body are also described.

公开(公告)号：US20170334604A1

公开(公告)日：2017-11-23

申请号：US15656721

申请日：2017-07-21

Applicant: CORNING INCORPORATED

Inventor： Kaveh Adib ,  Dana Craig Bookbinder ,  Theresa Chang ,  Paul Stephen Danielson ,  Steven Edward DeMartino ,  Melinda Ann Drake ,  Andrei Gennadyevich Fadeev ,  James Patrick Hamilton ,  Robert Michael Morena ,  Santona Pal ,  John Stephen Peanasky ,  Chandan Kumar Saha ,  Robert Anthony Schaut ,  Susan Lee Schiefelbein ,  Christopher Lee Timmons

IPC: B65D23/08 ,  B32B17/06 ,  C08G73/10 ,  B65D1/40 ,  C03C21/00 ,  B65D25/14 ,  C03C17/34 ,  C03C17/32 ,  C03C17/30 ,  C03C17/00 ,  C03C3/087 ,  C09D179/08 ,  C03C17/42

Abstract: Disclosed herein are delamination resistant glass pharmaceutical containers which may include an aluminosilicate glass having a Class HGA 1 hydrolytic resistance when tested according to ISO 720-1985 testing standard. The glass containers may also have a compressive stress layer with a depth of layer of greater than 25 μm. A surface compressive stress of the glass containers may be greater than or equal to 350 MPa. The delamination resistant glass pharmaceutical containers may be ion exchange strengthened and the ion exchange strengthening may include treating the delamination resistant glass pharmaceutical container in a molten salt bath for a time less than or equal to 5 hours at a temperature less than or equal to 450° C.

公开(公告)号：US20170320773A1

公开(公告)日：2017-11-09

申请号：US15656634

申请日：2017-07-21

Applicant: CORNING INCORPORATED

Inventor： Dana Craig Bookbinder ,  Theresa Chang ,  Paul Stephen Danielson ,  Steven Edward DeMartino ,  Andrei Gennadyevich Fadeev ,  Robert Michael Morena ,  Santona Pal ,  John Stephen Peanasky ,  Robert Anthony Schaut ,  Christopher Lee Timmons ,  Natesan Venkataraman ,  Ronald Luce Verkleeren

IPC: C03C17/42 ,  B65D1/02 ,  C09D179/08 ,  A61J1/14 ,  B32B17/06 ,  C03C17/32 ,  C03C17/30 ,  C03C17/00 ,  C03C15/02 ,  B65D65/42 ,  B65D25/34 ,  B65D25/14 ,  B65D23/08 ,  B65D23/02 ,  B65D1/40 ,  C03C21/00 ,  C03C17/34

CPC classification number: C03C17/42 ,  A61J1/1468 ,  B32B17/06 ,  B65D1/0207 ,  B65D1/0215 ,  B65D1/40 ,  B65D23/02 ,  B65D23/0814 ,  B65D23/0821 ,  B65D25/14 ,  B65D25/34 ,  B65D65/42 ,  C03C15/02 ,  C03C17/00 ,  C03C17/005 ,  C03C17/30 ,  C03C17/32 ,  C03C17/3405 ,  C03C21/002 ,  C03C2217/78 ,  C03C2218/111 ,  C09D179/08 ,  Y10T428/13 ,  Y10T428/131 ,  Y10T428/1317 ,  Y10T428/315

Abstract: In embodiments, a delamination resistant glass pharmaceutical package includes a glass body formed from a Type 1 Class glass composition according to ASTM Standard E438-92, the glass body having a wall portion with an inner surface and an outer surface. The glass body may have at least a class A2 base resistance or better according to ISO 695, at least a type HGB2 hydrolytic resistance or better according to ISO 719 and Type 1 chemical durability according to USP . An interior region of the glass body may extend from about 10 nm below the inner surface and having a persistent layer homogeneity. The glass body may also have a surface region extending over the inner surface and having a persistent surface homogeneity such that the glass body is resistant to delamination.

公开(公告)号：US09775775B2

公开(公告)日：2017-10-03

申请号：US14812902

申请日：2015-07-29

Applicant: Corning Incorporated

Inventor： Andrei Gennadyevich Fadeev ,  Theresa Chang ,  Dana Craig Bookbinder ,  Santona Pal ,  Chandan Kumar Saha ,  Steven Edward DeMartino ,  Christopher Lee Timmons ,  John Stephen Peanasky

IPC: A61J1/00 ,  B65D65/42 ,  B65D23/08 ,  B65D25/14 ,  C03C17/30 ,  C03C17/32 ,  C09D179/08 ,  C03C17/00 ,  C03C17/42 ,  C03C21/00 ,  A61J1/14

CPC classification number: A61J1/1468 ,  A61J1/00 ,  B65D23/0814 ,  B65D23/0821 ,  B65D25/14 ,  B65D25/34 ,  B65D65/42 ,  C03C17/005 ,  C03C17/30 ,  C03C17/32 ,  C03C17/42 ,  C03C21/002 ,  C03C2217/78 ,  C03C2218/111 ,  C09D179/08 ,  Y10T428/1321 ,  Y10T428/24942

Abstract: Coated pharmaceutical packages are disclosed. In embodiments, a coated pharmaceutical package includes a glass body comprising a first surface. A low-friction coating may be positioned on at least a portion of the first surface of the glass body. The low-friction coating may include a polymer chemical composition. A light transmission through the coated pharmaceutical package may be greater than or equal to about 55% of a light transmission through an uncoated pharmaceutical package for wavelengths from about 400 nm to about 700 nm. The low-friction coating may have a mass loss of less than about 5% of its mass when heated from a temperature of 150° C. to 350° C. at a ramp rate of about 10° C./minute.

公开(公告)号：US20170036950A1

公开(公告)日：2017-02-09

申请号：US15331113

申请日：2016-10-21

Applicant: Corning Incorporated

Inventor： Andrei Gennadyevich Fadeev ,  Theresa Chang ,  Dana Craig Bookbinder ,  Santona Pal ,  Chandan Kumar Saha ,  Steven Edward DeMartino ,  Christopher Lee Timmons ,  John Stephen Peanasky

IPC: C03C17/42 ,  C03C17/30 ,  B65D65/42 ,  C03C21/00 ,  A61J1/14 ,  C03C17/00 ,  C03C17/32

CPC classification number: A61J1/1468 ,  A61J1/00 ,  B65D23/0814 ,  B65D23/0821 ,  B65D25/14 ,  B65D25/34 ,  B65D65/42 ,  C03C17/005 ,  C03C17/30 ,  C03C17/32 ,  C03C17/42 ,  C03C21/002 ,  C03C2217/78 ,  C03C2218/111 ,  C09D179/08 ,  Y10T428/1321 ,  Y10T428/24942

Abstract: A coated glass pharmaceutical package may include a body formed from a Type 1 Class glass according to ASTM Standard E438-92. The body may have an interior surface and an exterior surface. The body may also have at least a class A2 base resistance or better according to ISO 695, at least a type HGB2 hydrolytic resistance or better according to ISO 719 and a Type 1 chemical durability according to USP . A coating having a thickness of ≦100 microns may be positioned on at least a portion of the exterior surface. The portion of the exterior surface with the coating may have a coefficient of friction that is at least 20% less than an uncoated glass pharmaceutical package and the coefficient of friction does not increase by more than 30% after undergoing a depyrogenation.

Abstract translation: 涂覆玻璃药物包装可以包括由根据ASTM标准E438-92的1型玻璃制成的主体。 身体可以具有内表面和外表面。 根据ISO 695，本体还可以具有至少A2级耐碱性或更好，根据ISO 719至少一种HGB2型耐水解性或更好，以及根据USP <660>的1型化学耐久性。 厚度≤100微米的涂层可以位于外表面的至少一部分上。 具有涂层的外表面的部分可以具有比未涂覆的玻璃药物包装小至少20％的摩擦系数，并且在进行去热原后摩擦系数不会增加超过30％。

公开(公告)号：US20160251260A1

公开(公告)日：2016-09-01

申请号：US15153295

申请日：2016-05-12

Applicant: Corning Incorporated

Inventor： John Frederick Bayne ,  Kyle Christopher Hoff ,  Jamie Lynne Morley ,  Christopher Lee Timmons

IPC: C03C17/30 ,  B65D23/08 ,  B65D1/09

Abstract: Embodiments of the present disclosure are directed to coated glass articles which reduce glass particle formation caused by glass to glass contact in pharmaceutical glass filling lines.

Abstract translation: 本公开的实施方案涉及在药物玻璃填充线中减少由玻璃与玻璃接触引起的玻璃颗粒形成的涂覆玻璃制品。

公开(公告)号：US09034442B2

公开(公告)日：2015-05-19

申请号：US14052048

申请日：2013-10-11

Applicant: Corning Incorporated

Inventor： Theresa Chang ,  Steven Edward DeMartino ,  Andrei Gennadyevich Fadeev ,  John Stephen Peanasky ,  Robert Anthony Schaut ,  Christopher Lee Timmons

IPC: C08L83/00 ,  C03C15/02 ,  B65D25/14 ,  B65D23/08 ,  C03C17/00 ,  B65D1/02 ,  B65D25/34 ,  B32B17/06 ,  B65D1/40 ,  C03C17/30 ,  C03C17/32 ,  C03C17/42 ,  C03C21/00 ,  C09D179/08 ,  B65D23/02

CPC classification number: C03C17/42 ,  A61J1/1468 ,  B32B17/06 ,  B65D1/0207 ,  B65D1/0215 ,  B65D1/40 ,  B65D23/02 ,  B65D23/0814 ,  B65D23/0821 ,  B65D25/14 ,  B65D25/34 ,  B65D65/42 ,  C03C15/02 ,  C03C17/00 ,  C03C17/005 ,  C03C17/30 ,  C03C17/32 ,  C03C17/3405 ,  C03C21/002 ,  C03C2217/78 ,  C03C2218/111 ,  C09D179/08 ,  Y10T428/13 ,  Y10T428/131 ,  Y10T428/1317 ,  Y10T428/315

Abstract: According to one embodiment, a glass container may include a body formed from a Type I, Class B glass composition according to ASTM Standard E438-92. The body may have an inner surface, an outer surface and a wall thickness extending between the outer surface and the inner surface. The body may also include a compressively stressed layer extending into the wall thickness from at least one of the outer surface and the inner surface. A lubricous coating may be positioned on at least a portion of the outer surface of the body, wherein the outer surface of the body with the lubricous coating has a coefficient of friction less than or equal to 0.7.

Abstract translation: 根据一个实施例，玻璃容器可以包括由根据ASTM标准E438-92的I型B类玻璃组合物形成的主体。 主体可以具有在外表面和内表面之间延伸的内表面，外表面和壁厚。 主体还可以包括从外表面和内表面中的至少一个延伸到壁厚中的压应力层。 润滑涂层可以位于主体的外表面的至少一部分上，其中具有润滑涂层的主体的外表面具有小于或等于0.7的摩擦系数。

公开(公告)号：US20150085365A1

公开(公告)日：2015-03-26

申请号：US14386583

申请日：2013-03-26

Applicant: Corning Incorporated

Inventor： John Claude Cadotte, JR. ,  John Stephen Peanasky ,  Christopher Lee Timmons ,  Srinivasa Rao Vaddiraju ,  Nikhil Baburam Vasudeo ,  Tyler Wezner

IPC: G02B5/18

CPC classification number: G02B5/1852 ,  G01N21/23 ,  G01N21/253 ,  G01N21/4133 ,  G01N21/7743 ,  G02B5/18

Abstract: A resonant waveguide article, including: a polymeric substrate having at least one integral grating region, wherein the article has a low birefringence property of for example, from about 5 to 270 nm/cm, as defined herein. Also disclosed is a microplate including the resonant waveguide article, and an integral well plate bonded to the sensor article, as defined herein. Also disclosed are methods of making a sensor article, and a method of making and using the microplate including the sensor article, as defined herein.

Abstract translation: 一种谐振波导制品，包括：具有至少一个整体光栅区域的聚合物基材，其中该制品具有如本文所定义的例如约5至270nm / cm的低双折射性质。 还公开了包括谐振波导制品和结合到传感器制品的整体井板的微板，如本文所定义的。 还公开了制造传感器制品的方法，以及制造和使用如本文所定义的包括传感器制品的微孔板的方法。