Cyclic ether copolymer, coating resin composition, optical devices, and process for production of the devices
    72.
    发明申请
    Cyclic ether copolymer, coating resin composition, optical devices, and process for production of the devices 审中-公开
    环状醚共聚物,涂料树脂组合物,光学元件以及器件生产工艺

    公开(公告)号:US20060189788A1

    公开(公告)日:2006-08-24

    申请号:US10552684

    申请日:2004-03-31

    IPC分类号: C08G65/34

    摘要: This invention provides a cyclic ether copolymer such as a cyclic ether copolymer excellent in solubility in solvents and easy to form uniform thin films therefrom. The present invention relates to a cyclic ether copolymer obtained from a 1,3-dioxole ring structure-containing compound represented by the following general formula (I) and an ethylenically unsaturated monomer: (wherein R1 and R2 are the same or different and each represents F, H, Cl or a perfluoroalkyl group containing 1 to 5 carbon atoms and X1 and X2 are the same or different and each represents F, H, Cl or —OR3, and R3 represents a perfluoroalkyl group containing 1 to 5 carbon atoms, provided that at least one of R1 and R2 is F or a perfluoroalkyl group containing 1 to 5 carbon atoms), which compolymer has a glass transition point of 100 to 135° C. and an intrinsic viscosity of 0.01 to 0.4 dl/g as determined at 35° C. in perfluoro-2-butyltetrahydrofuran.

    摘要翻译: 本发明提供了一种环状醚共聚物,例如在溶剂中溶解性优异的环状醚共聚物,并且易于形成均匀的薄膜。 本发明涉及由以下通式(I)表示的含1,3-二氧杂环环结构的化合物和烯属不饱和单体(其中R 1和R 2)和R 2个相同或不同,各自表示F,H,Cl或含有1至5个碳原子的全氟烷基,X 1和X 2 2 >相同或不同,各自表示F,H,Cl或-OR 3,并且R 3表示含有1至5个碳原子的全氟烷基,条件是在 R 1和R 2中的至少一个为F或含有1至5个碳原子的全氟烷基),该共聚物的玻璃化转变点为100至135℃。 并且在35℃下在全氟-2-丁基四氢呋喃中测定的特性粘度为0.01至0.4dl / g。

    Method of forming thin film
    73.
    发明申请
    Method of forming thin film 失效
    薄膜形成方法

    公开(公告)号:US20060014912A1

    公开(公告)日:2006-01-19

    申请号:US11231992

    申请日:2005-09-22

    IPC分类号: C08F114/18

    摘要: There is provided a method of forming a thin film of vinylidene fluoride homopolymer having crystal form I which is applicable to various substrates in relatively easy way (coating conditions, application method, etc.), a process for preparing a vinylidene fluoride homopolymer having crystal form I efficiently at high purity, and novel vinylidene fluoride homopolymers which can give a thin film being excellent in ferroelectricity. The method of forming a thin film of vinylidene fluoride homopolymer comprises (i) a step for preparing a green powder product of vinylidene fluoride homopolymer comprising crystal form I alone or as main component by subjecting vinylidene fluoride to radical polymerization in the presence of a bromine compound or iodine compound having 1 to 20 carbon atoms which contains at least one moiety represented by —CRf1Rf2X1, wherein X1 is iodine atom or bromine atom; Rf1 and Rf2 are the same or different and each is selected from fluorine atom or perfluoroalkyl groups having 1 to 5 carbon atoms and (ii) a step for forming a thin film on a substrate surface by using vinylidene fluoride homopolymer which comprises crystal form I alone or as main component and is obtained from the green powder product of vinylidene fluoride homopolymer comprising crystal form I alone or as main component.

    摘要翻译: 提供一种以相对容易的方式(涂布条件,涂布方法等)形成可以适用于各种基材的结晶形式I的偏二氟乙烯均聚物的薄膜的方法,制备具有结晶形式的偏二氟乙烯均聚物 我高效率地得到高纯度的新型偏二氟乙烯均聚物,可以得到铁电性优异的薄膜。 形成偏氟乙烯均聚物薄膜的方法包括(i)通过在溴化合物的存在下使偏二氟乙烯进行自由基聚合,制备单晶或单体晶形的偏二氟乙烯均聚物的生粉产物的步骤 或具有1〜20个碳原子的碘化合物,其含有至少一个由-CR 1,...,R 2,...,X 1表示的部分,其中X 1 是碘原子或溴原子; Rf 1和Rf 2相同或不同,各自选自具有1至5个碳原子的氟原子或全氟烷基,和(ii)形成薄的 通过使用包含单晶晶体I或主要成分的偏二氟乙烯均聚物在基材表面上形成薄膜,并且由包含单晶晶体I或主要组分的偏二氟乙烯均聚物的绿色粉末产品获得。

    Fluorine-containing optical material and fluorine-containing copolymer
    74.
    发明申请
    Fluorine-containing optical material and fluorine-containing copolymer 审中-公开
    含氟光学材料和含氟共聚物

    公开(公告)号:US20060009599A1

    公开(公告)日:2006-01-12

    申请号:US10538266

    申请日:2003-11-28

    IPC分类号: C08F18/20

    摘要: There is provided a fluorine-containing optical material and a fluorine-containing copolymer which have excellent heat resistance and flexibility in addition to optical characteristics, particularly a material suitable as a clad material for heat resistant plastic optical fiber. The fluorine-containing optical material comprises from 15 to 62% by mole of a structural unit (a) derived from hexafluoroneopentyl methacrylate, from 12 to 70% by mole of a structural unit (b) derived from methyl methacrylate and from 1 to 40% by mole of a structural unit (c) which is derived from a fluorine-containing monomer and is copolymerizable therewith, and is used as various optical materials, and is useful particularly as a clad material for heat resistant optical fiber.

    摘要翻译: 提供除了光学特性以外还具有优异的耐热性和柔性的含氟光学材料和含氟共聚物,特别是适合作为耐热塑料光纤的复合材料的材料。 含氟光学材料包含15至62摩尔%的衍生自甲基丙烯酸六氟戊烯酯的结构单元(a),12至70摩尔%的衍生自甲基丙烯酸甲酯的结构单元(b)和1至40% 的由含氟单体衍生的结构单元(c),可与其共聚,作为各种光学材料使用,特别适用于耐热光纤的复合材料。

    Molding material
    75.
    发明授权
    Molding material 有权
    成型材料

    公开(公告)号:US06635717B1

    公开(公告)日:2003-10-21

    申请号:US09530515

    申请日:2000-07-05

    IPC分类号: C08F25900

    CPC分类号: C08F293/00 C09K3/1009

    摘要: According to the present invention, it is possible to provide a molding material, for example, a sealing material for semiconductor-related production apparatuses which comprises a fluorine-containing multi-segment polymer being excellent in mechanical properties (particularly at high temperature), abrasion resistance and transparency and ensuring reduced contamination and reduced gas permeation while maintaining inherent characteristics of a fluorine-containing elastomer such as flexibility, elasticity, sealing property, chemical resistance and heat resistance. A molding material comprising a fluorine-containing multi-segment polymer having an elastomeric fluorine-containing polymer chain segment and a non-elastomeric fluorine-containing polymer chain segment, in which the elastomeric fluorine-containing polymer chain segment imparts flexibility to the whole polymer and has perhaloolefin units as a recurring unit in an amount of not less than 95% by mole.

    摘要翻译: 根据本发明,可以提供一种成型材料,例如,用于半导体相关生产设备的密封材料,其包括机械性能(特别是在高温下)具有优异的含氟多段聚合物,耐磨性 电阻和透明度,并且确保减少污染和降低气体渗透,同时保持含氟弹性体的固有特性,例如柔性,弹性,密封性,耐化学性和耐热性。 一种包含具有弹性体含氟聚合物链段和非弹性含氟聚合物链段的含氟多段聚合物的模塑材料,其中弹性体含氟聚合物链段赋予整个聚合物柔性, 具有不低于95摩尔%的重复单元的全卤代烯烃单元。

    Nickel powder, method for preparation thereof and conductive paste
    76.
    发明授权
    Nickel powder, method for preparation thereof and conductive paste 有权
    镍粉,其制备方法和导电膏

    公开(公告)号:US06632265B1

    公开(公告)日:2003-10-14

    申请号:US09869970

    申请日:2001-10-09

    IPC分类号: C22B2300

    摘要: The nickel powder is characterized in that the rate of the nickel particles whose particle size is not less than 1.2 time the average particle size as determined by the observation with an SEM is not more than 5% of the total number of nickel particles and that the rate of nickel particles whose particle size is not more than 0.8 time the average particle size is not more than 5% of the total number of nickel particles. The nickel powder is produced by bringing a slurry, containing nickel hydroxide, which is prepared by adding an aqueous solution of a nickel salt to an aqueous solution of an alkali metal hydroxide, into contact with a hydrazine reducing agent under the temperature conditions of not less than 55° C. to reduce the nickel hydroxide.

    摘要翻译: 镍粉的特征在于,通过用SEM观察确定的粒径不小于平均粒径的1.2倍的镍粒子的速度不超过镍粒子总数的5%,并且 粒径不超过平均粒径的0.8倍的镍粒子的速率不超过镍粒子总数的5%。 通过将含有镍盐的水溶液加入到碱金属氢氧化物的水溶液中而制备的含有氢氧化镍的浆料与肼还原剂接触,在不低于 比55℃还原氢氧化镍

    Platform monitoring system
    77.
    发明授权
    Platform monitoring system 有权
    平台监控系统

    公开(公告)号:US06559760B2

    公开(公告)日:2003-05-06

    申请号:US09865535

    申请日:2001-05-29

    IPC分类号: B60Q100

    CPC分类号: B61L23/00 B61C17/00 H04N7/181

    摘要: A platform monitoring system includes a camera for capturing a situation on a platform. An image captured by the camera is transmitted from a light emitter on the ground side as an optical signal and also transmitted from a transmission antenna on the ground side as a radio wave signal. These signals are received by an optical receiver and a reception antenna, respectively, mounted in a leading end portion of a vehicle. When the vehicle is positioned in a region around a stopping position, an image carried by the optical signal is selectively displayed on a monitor disposed near an operator's seat in the vehicle. When the vehicle is positioned out of the region around the stopping position, an image carried by the radio wave signal is selectively displayed on the monitor near the operator's seat in the vehicle.

    摘要翻译: 平台监视系统包括用于捕获平台上的情况的相机。 由摄像机拍摄的图像作为光信号从地面侧的发光体发送,并且作为无线电波信号从地面侧的发送天线发送。 这些信号分别由安装在车辆的前端部的光接收器和接收天线接收。 当车辆位于围绕停止位置的区域中时,由安装在车辆上的操作者座椅附近的监视器上选择性地显示由光信号承载的图像。 当车辆位于围绕停止位置的区域之外时,由无线电波信号携带的图像被选择性地显示在车辆上操作者座位附近的监视器上。

    Nickel powder and conductive paste
    78.
    发明授权
    Nickel powder and conductive paste 有权
    镍粉和导电胶

    公开(公告)号:US06494931B1

    公开(公告)日:2002-12-17

    申请号:US09889149

    申请日:2001-10-17

    IPC分类号: B22F100

    摘要: The present invention relates to nickel powder characterized in that the rate of the nickel particles whose particle size is not less than 1.2 time the average particle size as determined by the observation with an SEM is not more than 5% of the total number of nickel particles, that the rate of nickel particles whose particle size is not more than 0.8 time the average particle size is not more than 5% of the total number of nickel particles and that the tap density of the nickel powder is not less than 2.5 g/cm3, as well as a conductive paste for use in making a multilayer ceramic capacitor. The nickel powder of the present invention has a narrow particle size distribution and an excellent packing ability in a conductive paste and is particularly suitably used for forming a thin and uniform inner electrode for a multilayer ceramic capacitor, without being accompanied by the formation of any crack and/or the generation of any delamination.

    摘要翻译: 本发明涉及镍粉,其特征在于,通过用SEM观察确定的粒径不小于平均粒径的1.2倍的镍粒子的速率不超过镍粒子总数的5% 粒径不大于平均粒径的0.8倍的镍粒子的速率不超过镍粒子总数的5%,并且镍粉的振实密度不小于2.5g / cm 3 ,以及用于制造多层陶瓷电容器的导电浆料。 本发明的镍粉末具有窄的粒度分布和在导电浆料中的优异的填充能力,特别适用于形成薄且均匀的多层陶瓷电容器的内部电极,而不伴随任何裂纹的形成 和/或产生任何分层。

    Method for preparing nickel fine powder
    79.
    发明授权
    Method for preparing nickel fine powder 失效
    镍微粉制备方法

    公开(公告)号:US6120576A

    公开(公告)日:2000-09-19

    申请号:US112361

    申请日:1998-07-09

    IPC分类号: B22F1/00 B22F9/24

    摘要: A method for preparing nickel fine powder is herein disclosed, which comprises the steps of mixing an aqueous sodium hydroxide solution comprising, on the basis of the total weight of the sodium hydroxide present in the aqueous solution, 75 to 85% by weight of liquid caustic soda as specified in JIS K 1203 and 25 to 15% by weight, in total, of at least one of sodium hydroxide as specified in JIS K 8576 and solid caustic soda as specified in JIS K 1202, with an aqueous solution of nickel sulfate to form nickel hydroxide, then reducing the resulting nickel hydroxide with hydrazine and recovering nickel fine powder produced. The nickel fine powder prepared by the method has an average particle size of the primary particles ranging from 0.1 to 0.9 .mu.m, a D.sub.90 value of not more than 2.1 .mu.m and a tap density of not less than 3.5 g/cc. The nickel fine powder has a low degree of aggregation, a narrow particle size distribution and a high tap density and therefore, the powder is quite suitably used as a material for producing an internal electrode for a laminated ceramic condenser.

    摘要翻译: 本文公开了一种制备镍微粉的方法,其包括以下步骤:将氢氧化钠水溶液混合,所述氢氧化钠水溶液基于存在于水溶液中的氢氧化钠的总重量为75至85重量%的液体苛性碱 按照JIS K 1203中规定的苏打水,以及JIS-8576中规定的氢氧化钠中的至少一种和JIS K 1202中规定的固体苛性钠中的至少一种的25〜15重量%的硫酸镍水溶液 形成氢氧化镍,然后用肼还原所得的氢氧化镍并回收生产的镍细粉。 通过该方法制备的镍微粉末,其一次粒子的平均粒径为0.1〜0.9μm,D90值不大于2.1μm,振实密度为3.5g / cc以上。 镍微粉末具有低聚集度,窄粒度分布和高振实密度,因此该粉末非常适合用作制备用于层压陶瓷冷凝器的内部电极的材料。