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公开(公告)号：US08128897B2
公开(公告)日：2012-03-06
申请号：US12151398
申请日：2008-05-06
申请人： Roma Gimelfarb , Kurt John Waatti , Francis Joseph Lipiecki , Stephen Gerard Maroldo , Kenneth Eugene Sloffer
发明人： Roma Gimelfarb , Kurt John Waatti , Francis Joseph Lipiecki , Stephen Gerard Maroldo , Kenneth Eugene Sloffer
IPC分类号： C02F1/00
摘要： A continuous process for purification of brine contaminated with alkaline earth metals. The process comprises combining the brine with an aqueous solution containing at least one of an alkali metal hydroxide and an alkali metal carbonate with efficient mixing by a micro-mixing device.
摘要翻译： 用于净化受碱土金属污染的盐水的连续方法。 该方法包括将盐水与含有碱金属氢氧化物和碱金属碳酸盐中的至少一种的水溶液混合，通过微混合装置有效混合。
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公开(公告)号：US20100143237A1
公开(公告)日：2010-06-10
申请号：US12530427
申请日：2008-03-06
CPC分类号： B01D61/58 , B01D9/0013 , B01D9/005 , B01D9/0059 , B01D61/025 , B01D61/364 , B01D2311/04 , B01D2311/08 , C01D3/06 , C01D3/16 , B01D2311/103 , B01D2311/106 , B01D2311/26
摘要： A method of separating potassium chloride and sodium chloride from a heated solution of these salts, such as a solution obtained from potash ore, to recover potassium chloride from the ore is disclosed. The method includes a combination of steps of (a) extracting water from a heated solution containing potassium chloride and sodium chloride using a membrane system and (b) subsequently cooling the solution discharged from the membrane system, whereby steps (a) and (b) make it possible to selectively recover potassium chloride and sodium chloride from the solution.
摘要翻译： 公开了从这些盐的加热溶液中分离氯化钾和氯化钠的方法，例如从钾盐中获得的溶液，从矿石中回收氯化钾。 该方法包括以下步骤的组合：（a）使用膜系统从含有氯化钾和氯化钠的加热溶液中提取水，和（b）随后冷却从膜系统排出的溶液，由此步骤（a）和（b） 可以从溶液中选择性地回收氯化钾和氯化钠。
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73.发明授权公开(公告)号：US07645386B2
公开(公告)日：2010-01-12
申请号：US11404868
申请日：2006-04-17
申请人： Jan Procida
发明人： Jan Procida
CPC分类号： C01D3/10 , C01D3/00 , C01D3/04 , C01D3/06 , C01D3/14 , C01D3/145 , C01D3/16 , C01F11/24 , C01F11/34 , C01P2002/76 , C01P2004/02 , C22B7/008 , C22B26/00 , Y02P10/234
摘要： Pure halogen salts of alkaline and/or alkaline earth metals or a mixture thereof are prepared by (I) hydrolytically heating a suspension of 1 part by weight of a halogenic, organic waste material in a comminuted state in 1-10 parts by weight of an aqueous medium in the presence of a base to a temperature ranging from 200-300° C. at a pressure sufficient to maintain the water in a liquid state for a period of time sufficient to convert substantially all the organically bound halogen present to inorganic halides, and (II) separating the hydrolysate obtained in step (I) into a solid hydrolysate fraction and a liquid hydrolysate fraction, (III) neutralizing the liquid hydrolysate with hydrohalogenic acid, (IV) adding a flocculent to the neutralized hydrolysate; (V) separating the material from step (IV) into a solid containing fraction and an aqueous solution; and (VI) nanofiltering the aqueous solution to obtain a retentate and a permeate, wherein the permeate is further treated to obtain the pure salts.
摘要翻译： 碱性和/或碱土金属或其混合物的纯卤素盐通过以下步骤制备：（I）将1重量份粉碎状态的有机废物的1重量份的悬浮液水解加热至1-10重量份 水溶液在碱存在下反应至温度范围为200-300℃，其压力足以将水保持在液态，所述时间足以将存在的所有有机结合的卤素转化为无机卤化物， 和（II）将步骤（I）中获得的水解产物分离成固体水解产物级分和液体水解产物级分，（III）用氢卤酸中和液体水解产物，（Ⅳ）向中和的水解产物中加入絮凝物; （V）将来自步骤（IV）的材料分离成含固体部分和水溶液; 和（VI）对所述水溶液进行纳滤，得到渗余物和渗透物，其中进一步处理渗透物以获得纯盐。
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公开(公告)号：US20060118034A1
公开(公告)日：2006-06-08
申请号：US11330473
申请日：2006-01-12
申请人： Oleg Kozyuk
发明人： Oleg Kozyuk
IPC分类号： H01L21/322
CPC分类号： C30B35/00 , B01D9/005 , B01D9/0054 , B01D9/0063 , B01D9/0081 , B01F5/0656 , C01D3/16 , C01D3/24 , C30B7/00 , C30B7/10 , C30B29/60
摘要： A device and process for crystallizing a compound using hydrodynamic cavitation comprising the steps of mixing at least one stream of a solution of such compound to be crystallized with at least one stream of an anti-solvent and passing the mixed streams at an elevated pressure through a local constriction of flow to create hydrodynamic cavitation thereby causing nucleation and the direct production of crystals.
摘要翻译： 一种用于使用流体动力空化使化合物结晶的装置和方法，包括以下步骤：将待结晶的这种化合物的溶液的至少一种流与至少一种抗溶剂流混合，并在高压下通过混合物流 流动的局部收缩以产生流体动力空化，从而引起成核并直接产生晶体。
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公开(公告)号：US20030155301A1
公开(公告)日：2003-08-21
申请号：US10036877
申请日：2002-01-04
IPC分类号： B01D015/00
摘要： A method of purifying gluconate-containing brine is described which comprises first removing transition metal cations and other impurities by passage of the brine through a first ion exchange resin. The brine is then passed through a second ion exchange resin to effect removal of alkaline earth metal cations. In a third step the brine is treated with a carbonaceous adsorbent to remove impurities introduced by the ion exchange resins, as well as to effect removal of quaternary ammonium salts such as chloromethyl triethylammonium chloride. Methods for the regeneration of the carbonaceous adsorbent are described.
摘要翻译： 描述了一种纯化含有葡萄糖酸盐的盐水的方法，其包括首先通过第一离子交换树脂通过盐水来除去过渡金属阳离子和其它杂质。 然后将盐水通过第二离子交换树脂以除去碱土金属阳离子。 在第三步骤中，用碳质吸附剂处理盐水以除去由离子交换树脂引入的杂质，以及除去季铵盐如氯甲基三乙基氯化铵。 描述了碳质吸附剂的再生方法。
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公开(公告)号：US06428677B1
公开(公告)日：2002-08-06
申请号：US08973078
申请日：1998-03-20
IPC分类号： C25B126
CPC分类号： C02F1/4674 , C01D3/14 , C01D3/16 , C02F1/281 , C02F1/283 , C02F2209/06 , C02F2303/185 , C25B1/26
摘要： A chlorination system in which brine is converted to sodium hypochlorite by an electrolyser. Brine (1) fed to the electrolyser (3) is passed through a filter (2) which is capable of adsorbing bromine or hypobromous acid. Some of the sodium hypochlorite produced in an electrolyser (3) is fed back to a point in the brine feed upstream of the filter (2) such that any bromide in the brine is oxidized to bromine or hypobromous acid and therefore adsorbed by the filter (2).
摘要翻译： 盐水通过电解槽转化为次氯酸钠的氯化体系。 进料到电解槽（3）的盐水（1）通过能够吸附溴或次溴酸的过滤器（2）。 在电解器（3）中产生的一些次氯酸钠被反馈到过滤器（2）上游的盐水进料中的一个点，使得盐水中的任何溴化物被氧化成溴或次溴酸，因此被过滤器吸附（ 2）。
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77.发明授权
公开(公告)号：US5814359A
公开(公告)日：1998-09-29
申请号：US730204
申请日：1996-10-15
申请人： Masami Oura , Hironaga Hashiba
发明人： Masami Oura , Hironaga Hashiba
摘要： A soy sauce is produced by mixing a salt solution having a hard component concentration of not more than 20 ppm as calcium with a soy sauce koji, and subjecting the mixture to fermentation and ageing and then compressing it to obtain a crude soy sauce, and heat-treating the crude soy sauce in a plate-type exchanger, thereby the hard component decomposition on the plate surface being lowered and the frequency of washing the plate surface resulting in considerable decrease.
摘要翻译： 将硬质成分浓度为20ppm以下的盐溶液与酱油酱混合制成酱油，并对混合物进行发酵和熟化，然后压缩，得到粗酱油，加热 在平板式交换器中调制粗酱油，从而使板表面上的硬分量分解降低，并且洗涤板表面的频率大大降低。
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78.发明授权
公开(公告)号：US5769906A
公开(公告)日：1998-06-23
申请号：US721658
申请日：1996-09-27
申请人： Mattias Kremer , Georg Wahl , Eberhard Gock , Stefan Wigger , Jorg Kahler
发明人： Mattias Kremer , Georg Wahl , Eberhard Gock , Stefan Wigger , Jorg Kahler
摘要： The process for environmentally acceptable and economical recovery of chloride salts from hardening-shop used salts utilizing the steps of leaching of the used salt, detoxification of the cyanide and selective crystallization of the individual chloride salts. The process is characterized in that all the chloride salts that are present in the hardening-shop used salt are recovered in pure form.
摘要翻译： 使用浸出所用盐的步骤从硬化车间使用的盐中环境可接受和经济地回收氯化物的方法，氰化物的解毒和各种氯化物盐的选择性结晶。 该方法的特征在于，在硬化车间使用的盐中存在的所有氯化物盐以纯的形式回收。
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公开(公告)号：US5536415A
公开(公告)日：1996-07-16
申请号：US319224
申请日：1994-10-06
申请人： Philippe Joubert
发明人： Philippe Joubert
CPC分类号： C01D3/16
摘要： Contaminating amounts of sulfate ions are removed from aqueous saline solutions comprised thereof by (i) contacting such saline solution with a zirconium compound, at an acidic pH, (ii) separating the resulting medium into (a) a saline solution depleted in sulfate ions and (b) a zirconium compound onto which said sulfate ions are sorbed, (iii) desorbing the sulfate ions from the stage (ii) zirconium compound at a basic pH, and (iv) separating the medium of desorption into (1) a basic aqueous solution enriched in sulfate ions and (2) a zirconium compound substantially devoid of sulfate ions, with the proviso that the zirconium compound is a novel hydrated zirconium hydroxide having the formula Zr(OH).sub.4 .multidot.xH.sub.2 O, in which x ranges from 4 to 200, and such zirconium compound comprising an undried gelatinous precipitate thereof.
摘要翻译： （i）在酸性pH下使这种盐溶液与锆化合物接触，（ii）将得到的培养基分离成（a）贫去硫酸根离子的盐水溶液和 （b）在其上吸附所述硫酸根离子的锆化合物，（iii）在碱性pH下从阶段（ii）锆化合物解吸硫酸根离子，和（iv）将解吸介质分离成（1）碱性水溶液 富含硫酸根离子的溶液和（2）基本上不含硫酸根离子的锆化合物，条件是锆化合物是具有式Zr（OH）4×H 2 O的新型水合氢氧化锆，其中x为4至200，以及 这种锆化合物包含未干燥的凝胶状沉淀物。
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公开(公告)号：US5082492A
公开(公告)日：1992-01-21
申请号：US345167
申请日：1989-05-01
CPC分类号： F24J3/085 , C01D3/16 , Y02E10/14 , Y10S423/19
摘要： A method is disclosed for polishing geothermal brines containing iron-rich silica scale and silica particles suspended therein while removing and recovering copper, silver and other precious metals dissolved therein. The method comprises passing brine having a pH just below about 5.0 through a conduit packed with a metal higher in the electromotive series than silver for a time to sufficient for substantially all of the silver and other precious metals therein to precipitate onto the packing. Preferably, the packing comprises coiled zinc-galvanized steel chicken wire mesh packed in a sufficient density to act as a filter for said suspended particles. Dissolving the packing in a suitable acid will leave a precious metal-rich residue behind for subsequent recovery. When the brine is treated this process, the useful life of injection wells used to return cooled brine back to the geothrmal field is extended by at least about 3 times as compared to that observed with untreated brine.
摘要翻译： 公开了一种用于抛光含有富铁二氧化硅垢和悬浮在其中的二氧化硅颗粒的地热盐水的方法，同时除去和回收溶解在其中的铜，银和其它贵金属。 该方法包括将具有低于约5.0的pH的盐水通过填充有高于银的电动系列中的金属的管道一段时间足以使其中的所有银和其它贵金属基本上沉淀到填料上。 优选地，填料包括以足够的密度填充的卷绕的镀锌钢丝鸡丝网，以充当所述悬浮颗粒的过滤器。 将包装溶解在合适的酸中将留下贵重的富含金属的残留物，以便随后的回收。 当这种方法处理盐水时，用于将冷却的盐水返回到地质储层的注入井的使用寿命与未处理的盐水相比，延长至少约3倍。
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